ZnO-SnO2透明导电薄膜的制备及性能研究

采用二步成胶工艺制备ZnO-SnO₂透明导电薄膜,应用X射线衍射、原子力显微镜、紫外-可见分光光度计、薄膜分析仪及四探针仪等对薄膜的结构、表面微观形貌、透过率和导电性能进行表征.结果表明,锌锡摩尔比为9/12,退火温度为500 ℃时,薄膜的透过率达90%,电阻率为3.15×10-3 Ω·cm.与其它工艺相比,二步成胶工艺所制备出的ZnO-SnO₂透明导电薄膜性能优异.     

Investigation of scatter from out of the field of view and multiple scatter in PET using Monte Carlo simulations

In fully three-dimensional (3D) positron emission tomography (PET) imaging, the scatter fraction (SF) is about 40%-60%, which may degrade the imaging quality severely. Scatter correction is important for high quality image reconstruction. Model-based scatter correction has been proved to be accurate and available in clinical PET. However, it does not correct the scatter from out of the field of view (OFOV) and multiple scatters. In this study, we demonstrate the radial and axial distribution of scatters from OFOV when the source is located in different radial positions. In order to apply the above conclusions to different PET systems, we characterize the scatters from OFOV as a function of the ratio of the scanner diameter to the length of the axial field of view (AFOV) by modeling several typical whole-body and micro PET systems. The proportions of true events (S_0-0), single scatter of one photon (S_1-0) , single scatter of both photons (S_1-1) , double scatter of one photon (S_2-0) and multiple scatter (S_m) are also calculated and compared. Here the 3D-PET Monte Carlo simulations are performed with the Geant4 Application for Tomography Emission (GATE). In summary, the scatters from OFOV tend to be recorded on the lines of response (LOR) far away from the source. They have a much more serious impact on whole-body PET than micro PET depending on the ratio of scanner diameter to the length of AFOV. In whole-body PET, twice scatters including single scatter of both photons (S_1-1) and double scatter of one photon (S_2-0) add up to about 12% so that twice scatter correction must be taken into account to acquire a high quality reconstruction image.     

固相萃取-超高效液相色谱法同时测定乳制品中6种有机酸

建立了固相萃取-超高效液相色谱(UPLC)同时测定乳制品中苹果酸、酒石酸、乳酸、乙酸、柠檬酸、富马酸等6种有机酸的分析方法。样品用体积分数1%氨水溶液提取,调节至中性后经MAX柱净化,用Acquity UPLC HSS T3色谱柱(2.1 mm×100 mm,1.8μm)分离,以乙腈和0.02 mol/L KH2PO4缓冲溶液(pH 2.0)作为流动相进行梯度洗脱,二极管阵列检测器检测。6种有机酸在其相应范围内(0.05~5000 mg/L)线性关系良好(r2≥0.999),方法的定量限(信噪比为10)为0.05~25.0 mg/kg,3个不同水平的添加浓度回收率为80.1%~103.2%,相对标准偏差(n=8)在1.9%~11%之间。方法适合于乳制品中6种有机酸的同时检测。     

凝胶色谱-气相色谱-串联质谱法筛查茶叶中27种禁用农药

建立了茶叶中27种国家禁用农药的气相色谱-串联质谱分析方法。以27种国家禁用农药为目标分析物,样品经环己烷-乙酸乙酯超声提取、凝胶渗透色谱净化后进行定性和定量分析。方法检出限为0.02~2.82μg/kg,方法定量限为0.07~9.40μg/kg,在0.01~0.20 mg/L范围内方法线性相关系数均大于0.991,75%以上的农药的回收率在70%~110%之间,相对标准偏差在0.53%~7.1%之间。方法适用于茶叶中多种农药残留的检测分析。     

多用非经典光场产生系统的实验研究

由α-切割KTP晶体组成的半整块非简并光学参量振荡腔，以倍频Nd:YAP激光器作抽运源，可在不同运转条件下获得两类非经典光场.低于振荡阈值，该系统输出最大压缩度为3.7dB的双模正交压缩真空态；高于阈值，产生强度差压缩度为7dB的量子相关孪生光子对.系统能在锁定状态下持续稳定运转半小时以上. 关键词：     

用可调探深的电子能量损失谱研究Sn/Si界面

用可调探测深度的电子能量损失谱辅以俄歇电子能谱和低能电子衍射,研究Sn/Si系统的界面反应。结果表明:当Sn蒸镀量大于两个原子单层,退火温度由400℃到700℃,在Sn/Si(111)界面Sn与Si发生互混,形成几个原子层厚的Sn/Si互混层,该互混层的特征体峰在15.5eV。在相同温度范围退火,Sn/Si(001)界面无可察觉的互混,仍有Sn岛存在,长时间在550℃退火低能电子衍射图形上出现(113)小晶面的衍射斑。 关键词：     

灰色聚类法在三峡库区城市江段水质综合评价中的应用

应用灰色聚类法对三峡库区城市江段13个监测断面水质质量进行综合评价,获得较好的结果,能客观反映三峡库区城市江段质的类别及水体实际污染的状况.通过与模糊综合评价方法进行比较,灰色聚类法具有计算简便的优点,是一种较好的评价方法.     

乡村投递员问题的多面体

设 G=(V,E)是以 V 为顶点集,E 为边集合的连通无向图.对任意的 E′(?)E,以G[E′]记 G 的由 E′中的边所组成的子图,称之为边集 E′导出的子图.称边序列 w=〈(i_0,i_1,),(i_1,i_2),…,(i_(k-1),i_k)〉为连接 i_0和 i_k 的路,其中 i_j∈V,(i_j,i_(j+1)∈E,0≤j≤k-1.如果 i_0=i_k,则称 w 为一个闭路.如果 w 中 i_s(?)i_t,对任意0≤s,t≤k,     

高频圆电流磁场中导体环所受电磁悬浮力的实验测量

利用扭秤的高灵敏度和稳定性测量了高频圆电流对导体的电磁悬浮力。通过对与高频圆电流同轴细导体环距高频圆电流平面不同高度所受电磁悬浮力的测量，得到了导体环表面单位面积受纵向电磁悬浮力的分布。与理论计算结果进行对比分析，结果表明，在导体环与圆电流平面距离较大时实验曲线与理论曲线相吻合，从而为电磁悬浮实验提供了一种简便而准确的测量手段。