ZrO_2 films with variable refractive index by glancing angle deposition

When optical film is deposited at oblique angle incidences, the film becomes porously, and the film effective refractive index will decrease. Six porous ZrO2 films are fabricated by the glancing angle deposition (GLAD) technique with the different incidence angles. By changing the substrate tilt angle from 0° to 85°. the film refractive index varies from 1.92 to 1.27.     

冷空气蒸馏分离酸滴定法测定复合肥中铵态氮

提出了用冷空气蒸馏分离酸滴定法在多种形态氮共存时测定复合肥料中铵态氮含量的方法。取适量复合肥料样品于蒸馏瓶中,与550g.L-1碳酸钾溶液60mL反应,溶液总体积以不宜超过110mL。通过空气在流量为3L.min-1和不加热条件下蒸馏8h,生成的氨馏出并先后吸收于相互连接的3个吸收瓶中,每一吸收瓶中预置硼酸吸收溶液50mL,用0.05mol.L-1盐酸标准溶液滴定3溶液至指示剂呈暗红色,记录所耗盐酸标准溶液的总量。将吸收瓶重新按装在蒸馏系统中继续蒸馏1h后再进行滴定,以所耗盐酸标准溶液量不超过0.03mL认为测定完成。根据滴定所耗盐酸标准溶液的总量计算样品中铵态氮的含量。根据3个样品各5次测定结果计算,得到方法的回收率在99.7%～100.1%之间,相对标准偏差在0.12%～0.55%之间。     

修饰铋盘电极吸附伏安法测定痕量钴的研究

研究了利用丁二酮肟修饰铋电极测定钴的吸附伏安分析方法。在0.4 mol/L NH3.H2O-NH4Cl缓冲溶液(pH=9.0)中,Co(Ⅱ)与铋盘电极表面修饰的丁二酮肟形成螯合物。并于-1.20 V附近产生一个灵敏的还原峰。富集时间分别为60 s和280 s时,峰电流与钴的质量浓度在0.01~25μg/mL和0.002~2μg/mL范围内呈线性关系。该还原峰与采用汞电极时的峰形相似、电位相近、灵敏度相当。优化了实验条件,拟订了样品分析的步骤,利用该法测定了合金、维生素B12针剂样品中的微量钴。     

Green Output of 1.5 W from a Diode-Pumped Intracavity Frequency-Doubled Self-Q-Switched and Mode-Locked Cr,Nd：YAG Laser

We report a diode-pumped intracavity frequency-doubled self-Q-switched and mode-locked Cr,Nd：YAG/KTP green laser with a Z-type cavity, which produces 1.5 W of average power at 532nm with incident pump power 14.2 W. The individual mode-locked green pulse duration is about 560ps with 149 MHz repetition rate. Almost 100% modulation depth of the mode-locked green pulses is achieved at an incident pump power of 4.13 W. The maximum energy of Q-switched green pulse is 19.8μJ. The experimental results of pulse duration and pulse energy of Q-switched green pulse agree well with the theoretical calculations.     

Design of single-material guided-mode resonance filter

In this letter, a guided-mode resonance （GMR） filter with the same material for both the grating layer and the waveguide layer is designed, and its optical properties are investigated. The GMR filter owns almost 100% reflection at the resonance wavelength of 800 nm with the full-width at half-maximum （FWHM） of 20 nm, and its sideband reflection from 700 to 1000 nm is less than 5%. As the resonance wavelength is influenced by more than one parameter during the fabrication process, GMR filter with the same resonance wavelength can be obtained by adjusting other parameters or even one parameter to deviate from the design value.     

基于Vague集的建设项目综合评标

把Vague集应用于建设项目评标,从正向、反向和不确定多个方面描述投标文件的信息,为招标人客观评价和选择投标人提供了更充分的依据,应用综合评价值对投标人进行排序,从而选出最优投标人,使评标工作更加趋于全面、快捷,实例说明该方法的有效性.     

Form Birefringence in Thin Films with Oblique Columnar Structures

Effective medium theory is useful for designing optical elements with form birefringent subwavelength structures. Thin films fabricated by oblique deposition are similar to the two-dimensional surface relief subwavelength gratings. We use the effective medium theory to calculate the anisotropic optical properties of the thin films with oblique columnar structures. The effective refractive indices and the directions are calculated from effective medium theory. It is shown that optical thin films with predetermined refractive indices and birefringence may be engineered.     

一种基于马赫-曾德干涉仪的全光纤传感器双参数测量技术

提出一种干涉式全光纤传感器,能够同时实现对折射率和轴向拉力或温度进行双参数测量。传感器由一个微腔和一个纤芯失配衰减器组成。其中微腔结构是由飞秒激光加工光纤纤芯形成,直径和深度分别是6μm和2.5μm。该干涉式传感器可以获得20dB的高品质干涉对比度。传感器透射谱波长为1496.68nm和1533.18nm的两个衰减峰对应的折射率灵敏度分别为-29.91nm/RIU和-16.72nm/RIU,拉力灵敏度分别为-1.55pm/με和-0.31pm/με。实验结果表明,传感器通过灵敏度矩阵可以同时测量折射率和轴向拉力或温度两个参数。     

空间（Lμ^p）^m的弱Banach-Saks性质

证明了由m个Lμp空间产生的Banach向量空间（Lμp）m的弱Banach-Saks性质,其中m是自然数, 1 p 〈＋∞.当m= 1时,这就是著名的Banach-Saks-Szlenk定理.运用该性质,还给出了定义在向量空间Rm的一个凸集上的非负连续凸函数与取值在空间（Lpμ）m的一个弱紧子集中的向量值函数的复合函数的积分不等式.当这些向量值函数属于由m个Lμ∞空间产生的积空间（Lμ∞）m的一个弱＊紧子集时,类似的积分不等式还是成立的.     

Spectroscopic investigation of a new crystal： Nd^3＋,Yb^3＋：YVO4

The absorption and emission spectra of the YVO4 single crystal co-doped with 1 at.% Nd^3＋ and 1 at.% Yb^3＋ are investigated. The efficient Nd^3＋ → Yb^3＋ energy transfer and the back transfer （Yb^3＋ → Nd^3＋） are observed at room temperature. The fluorescence lifetime of the 4F3/2 level of Nd^3＋ in Nd,Yb：YVO4 is measured under 808 nm laser light excitation. The efficiency of Nd^3＋ → Yb^3＋ energy transfer in YVO4 is determined to be about 34%.