FeCuCrVSiB多层膜巨磁阻抗效应的研究

研究了结构为 (FM/SiO₂)₃/Ag/(SiO₂/FM)₃ 多层膜的巨磁阻抗(GMI)效应（这里的F M≡FeCuCrVSiB）．多层膜采用射频溅射法沉积在单晶Si衬底上，沉积过程中，沿膜面长方 向施加约72kA/m的磁场，然后在不同的温度下对样品进行了退火处理．结果表明，该多层膜 样品即使在沉积态便具有相当好的软磁性能和GMI效应，在7MHz的频率下，最大纵向和横向 巨磁阻抗比分别为45%和44%．在230℃下经90min退火处理后的样品具有最佳的GMI效应，在85MHz的频率下，最大纵向和横向巨磁阻抗比分别达到251%和277%．与磁性层总厚度相同的FeCuCrVSiB/Ag/FeCuCrVSiB三层膜相比较，在这种多层结构中出现的GMI效应更强． 关键词： 多层膜 巨磁阻抗效应 趋肤效应 有效磁导率     

TbDyFe薄膜对三明治膜巨磁阻抗效应的影响

将600℃退火后的超磁致伸缩材料(Tb0.27Dy_0.73)_0.3Fe_0.7薄膜作为Ni_80.2Fe_14.1Si_0.2Mn_0.4Mo_5.1三明治膜的基底，制备出四层膜.结果表明：附加的磁致伸缩并没有减小材料的巨磁阻抗(GMI)效应，而由于磁场下磁致伸缩材料的应力效应影响了三明治膜中的各向异性场，使三明治膜的GMI效应增大了4倍.再将制备态的四层膜在280℃下真空退火，退火态四层膜也增大了三明治膜的GMI效应，但可能由于磁致伸缩向磁性层中的扩散，其GMI效应相对于制备态四层膜则有所降低. 关键词： 巨磁阻抗(GMI)效应 三明治膜 TbDyFe薄膜 各向异性场     

FeCuNbSiB单层膜和三明治膜的磁特性与巨磁阻抗效应

用射频溅射法制备了Fe_73.5Cu₁Nb₃Si_13.5B₉单层膜和 Cu或Ag作为中间层的三明治膜.溅态膜为非晶态结构.磁畴观察结果表明,单层膜在380℃退火后,呈现均匀磁化的纳米晶结构,该样品软磁特性最佳,其巨磁阻抗效应最大,在13MHz,最大磁阻抗比纵向为18％,横向为14％.溅态三明治膜具有较大的巨磁阻抗效应,在13MHz,Cu夹层三明治膜的最大磁阻抗比纵向为32％,横向为11％,Ag夹层三明治膜的最大磁阻抗比纵向为47％,横向为57％.Cu夹层三明治膜经250℃退火后,在低频下表现为巨磁电感效应,在100kHz,最大磁电感比为1733％. 关键词：     

81NiFe/Cr多层膜磁电阻单向各向异性与交换耦合

采用电子束蒸发法制备的８１ＮｉＦｅ／Ｃｒ多层膜具有单向各向异性，磁滞回线非轴对称，相当存在１Ｏｅ数量级的交换偏场。磁电阻回线的上升和下降两枝差别明显，其中以横向磁电阻回线最为显著。有的试样上升枝与下降枝相应的最大横向磁电阻率之差已高达０．７８％，其最大各向异性磁电阻率（Ｒ_ｍａｘ－Ｒ_ｍｉｎ）／Ｒ为４．７２％，甚高于Ｍｉｙａｚａｋｉ等^[１］的优质８２ＮｉＦｅ合金单层膜的报道值３％。可以认为这类多层膜的磁电阻效应除主要来源于自旋－轨道耦合机制外， 关键词：     

多层膜［Co85Cr15/Pt］20的磁性、垂直磁记录特性和微结构的关系

采用磁控溅射法制备了性能优良的以Pt为缓冲层的［Co85₈₅Cr15_{15/Pt］2020 多层膜，研究了溅射气压对［Co8585Cr1515/Pt］2020多层膜微结构和磁性的 影响.研究结果表明，Ar溅射气压对［Co8585Cr1515/Pt］2020多层膜的微结构 、垂直磁各向异性和矫顽力有重要的影响 关键词： 溅射气压 多层膜 垂直磁各向异性 有效磁各向异性常数}     

利用FePt/Au多层膜结构制备垂直磁记录L10-FePt薄膜

利用磁控溅射方法在100℃的MgO单晶基片上制备了［FePt/Au］₁₀多层膜,并研究了采用FePt/Au多层膜结构对FePt薄膜的有序化温度、矫顽力（H_C）、垂直磁各向异性、晶粒尺寸以及颗粒间磁交换耦合作用的影响.磁性测试结果表明：FePt/Au多层膜在退火后具有较高的H_C、良好的垂直磁各向异性、较小的晶粒尺寸且无磁交换耦合作用.截面高分辨电镜分析表明：Au可以缓解MgO和FePt之间较大的晶格错配,从而促进薄 关键词： 0-FePt薄膜')" href="#">L1₀-FePt薄膜 有序化温度 垂直磁各向异性 磁交换耦合作用     

退火对Co35(SiO2)65颗粒膜巨磁电阻效应的影响

采用多靶离子束溅射镀膜机制备了一系列不同退火温度的Co₃₅(SiO₂)₆₅（体积百分数）颗粒膜样品,发现样品的巨磁电阻效应随着退火温度T_a的升高而单调下降.应用磁力显微镜对样品的磁结构进行了观测,发现随着退火温度的升高,近邻的Co颗粒的磁矩倾向于平行排列,形成磁畴结构,从而导致Co₃₅(SiO₂)₆₅颗粒膜巨磁电阻效应单调下降. 关键词：     

用脉冲激光方法在Si(100)上沉积的Cox-C1-x颗粒膜及其磁电阻效 应

利用脉冲激光沉积方法在Si(100)上制备了Co_x-C_1-x颗粒膜，并研 究了其正磁电阻 效应.实验结果表明，样品在室温下的正磁电阻效应要远远高于低温下的正磁电阻效应；Co _0.02-C_0.98样品具有最大的室温正磁电阻效应，在外加磁场B=1T时 ，其磁电阻 率MR=22%；随着Co含量的增加，Co_x-C_1-x颗粒膜的正磁电阻效应呈 减小趋势.样品 的MR-B的曲线与传统的多 关键词： 正磁电阻效应 x-C_1-x颗粒膜')" href="#">Co_x-C_1-x颗粒膜 脉冲激光沉积     

退火对IrMn基磁隧道结多层膜热稳定性的影响

采用磁控溅射方法制备了结构为IrMn/CoFe/AlO_x/CoFe的磁性隧道结多层膜,样品置于真空磁场中进行退火处理. 将在不同温度退火的磁隧道结结构多层膜置于负饱和场中等待,研究退火温度对样品热稳定性的影响. 结果表明:退火提高了多层膜反铁磁层的单轴各向异性能,增加了样品的交换偏置;随着负饱和场等待时间的延长,被钉扎层的磁滞回线向正场偏移,交换偏置单调减小,但退火减弱了这种趋势. 关键词： 磁隧道结 交换偏置 磁化反转     

射频溅射功率对FeZrBCu软磁合金薄膜巨磁阻抗效应的影响

用射频溅射法制备了FeZrBCu软磁合金薄膜.研究了不同溅射功率对FeZrBCu薄膜软磁特性和巨磁阻抗效应的影响.用电子探针显微镜测量发现，当溅射功率为240W时，薄膜样品中Fe的原子含量为8732%，Cu的原子含量为29%.这种样品的矫顽力最小，为68A/m，饱和磁化强度约为111×105⁵A/m，软磁性能最佳，巨磁阻抗效应最大，溅态膜在 13MHz最大巨磁阻抗比纵向为17%，横向为11%.重点分析了阻抗的电阻、电感分量及横向有 效磁导率随频率的变化，得到在低频下主要是磁电感 关键词： 铁基合金 薄膜 巨磁阻抗效应     

外磁场与带轴夹角对非晶FeSiB/Cu/FeSiB三明治薄带巨磁阻抗特性的影响

采用层间胶合方法制备了淬态非晶FeSiB/Cu/FeSiB三明治薄带,研究了同尺寸单层薄带和三明治薄带的巨磁阻抗(giant magneto-impedance, GMI)随外磁场与带轴夹角β的变化特性.结果表明,FeSiB单层薄带在7.0 MHz最佳响应频率下,GMI仅约30%,外磁场与带轴夹角对单层薄带GMI几乎没有影响;三明治薄带的GMI效应则十分显著,在0.6 MHz最佳响应频率下,纵、横向GMI比分别达到272%和464%, GMI随β的增大而增强;所有β角的三明治薄带GMI曲线都出现各向异性峰,各向异性峰随β的增大而展宽.根据磁畴转动模型推导了薄带横向磁导率与各向异性场及β之间的函数关系式.结果显示,三明治薄带GMI随夹角β变化的特性与理论推算的横向磁导率变化有较好的一致性,而单层薄带则不然.该磁畴转动模型能定性解释三明治薄带GMI随外磁场方向变化特性.     

电流退火铁基薄带巨磁阻抗效应的影响

研究了电流退火工艺对铁基非晶合金Fe₈₄Zr₈Nb_3.5B_3.5Cu_{1〈/sub>薄带巨磁阻抗效应的影响.实验结果表明,该铁基合金的巨磁阻抗ΔZ/Z随退火电流的增加而增强,当电流为820mA时,ΔZ/Z达到最大值62％,阻抗变化灵敏度可达约0.23％（A/m)^-1.结合此合金在电流退火燧后电性能和软磁性能的演变,讨论了材料的巨磁阻抗效应借助趋肤效应与交流频率和外加纵向磁场的关系. 关键词：}     

Evolution of magnetic permeability and magneto-impedance effect in composite wires with insulator layer

CuBe/Insulator/NiCoP composite wire was prepared by electroless deposition on an insulated CuBe core with a diameter of 90 μm. The conversion relationship between the magneto-impedance and effective magnetic permeability of the composite wire was derived from an energy conversion model. The evolution of the magnetic permeability and the giant magneto-impedance (GMI) effect were investigated. The results show that a distinct GMI effect can be obtained at relatively low frequency. The largest GMI ratio is 240% at 600 kHz, and the maximal field sensitivity is 34%/Oe.     

Cytotoxicity and GMI bio-sensor detection of maghemite nanoparticles internalized into cells

In this work we determine conditions to produce cell samples for imaging with detection of the modification of the magnetic field by maghemite (Fe₂O₃) nanoparticles acting as a high sensitivity magnetic bio-sensor based on the giant magneto-impedance (GMI) effect. Mat Ly Lu cells are grown for 24 h with various maghemite nanoparticles concentrations (from 0 to 6 mg/ml). The percentage of viable cells is determined by counting labeled cells with trypan blue under an optical microscope. The quantity of nanoparticles internalized into the cells is evaluated by X-ray fluorescence analysis and expressed in iron moles per cell. The GMI bio-sensor was tested with the various samples. We observed that the best sensitivity of the GMI bio-sensor was obtained at a frequency of 1 MHz. To confirm these results in the presence of cell samples, four measurement frequencies were pre-selected (from 1 to 100 MHz) and tested. Cell growth conditions compatible with an acceptable percentage of cell viability for various concentrations of nanoparticles were also determined. These experiments allow us to conclude that cell growth with 0.1 mg/ml of nanoparticles for 24 h shows modifications of the magnetic field detectable optimally at 1 MHz frequency.     

Giant magneto-impedance effect in CoMnSiB amorphous microwires

The giant magneto-impedance (GMI) ratio, ΔZ/Z=[(Z(H)−Z(H_max)]/Z(H_max), in a nearly zero magnetostrictive Co_68.5Mn_6.5Si₁₀B₁₅ amorphous microwire has been investigated for the frequency range 0.5–10 MHz, driving current amplitude of 0.5–2.5 mA, bias DC magnetic field up to 2400 A/m and under applied tensile stress up to 132 MPa. A maximum relative change in the GMI ratio up to around 130% is observed at a frequency of 10 MHz, magnetic DC field of about 180 A/m, driving current amplitude of 1 mA and under tension of 60 MPa. The tensile stress dependence of the magnetic field, H_m, corresponding to the maximum ΔZ/Z ratio allows to estimate the magnetostriction constant (λ_s≈−2×10⁻⁷) to be in good agreement with λ_s values estimated by different methods and in amorphous alloys with similar compositions.     

非晶CoFeNiNbSiB合金的巨磁阻抗效应

研究了非晶Co₇₀Fe_4.5Ni₄Nb₁Si_12.5B₈合金薄带的巨磁阻抗效应.实验表明,在一定频率范围内提高测试频率,磁阻抗效应有明显提高;适当温度的退火也有助于磁阻抗效应的提高.制备态非晶合金样品在频率为5MHz下达120%左右,经过退火处理的非晶样品5MHz下的效应可达400%左右. 关键词：     

Giant magnetoimpedance in amorphous (Co0.93Fe0.7)63Ni10Si11B16 glass-coated microwire

Giant magnetoimpedance (GMI) effect has been measured in a glass-coated amorphous (Co_0.93Fe_0.7)₆₃Ni₁₀Si₁₁B₁₆ microwire as a function of DC magnetic field and up to the frequency of 11 MHz. The sample shows single peak GMI characteristics within the whole range of frequency. The domain structure of the above sample has been changed by applying tensile stresses up to 603 MPa and current annealing with a DC current of 50 mA for various time durations, and the corresponding effect on GMI has been studied in detail. A maximum change of 8.85% in MI of the as-quenched sample has been observed around a frequency of 5.05 MHz. Application of an external tensile stress reduces the GMI value by increasing the inner core domain, whereas heat treatment of the sample enhances the same. The square-shaped magnetic hysteresis loop of the as-quenched sample helps us understanding the MI results.