HIRFL-CSRe二极铁积分磁场测量

 介绍了兰州重力加速器冷却储存环实验环二极磁铁积分长线圈测磁装置的构成，描述了实验环二极铁的分散性测量、横向分布测量、传递函数等测量内容及测量方法。实验环二极铁采用不断地加减硅钢铁片垫补和加调整线圈电流的方法来调整二极磁铁的有效长度来改变分散性。通过垫补和测量，二极磁铁的分散性在优化磁场时达到±2×10^-4。同时给出了二极铁的横向分布和传递函数的测量结果。对二极铁的设计和加工进行了修正。     

CSR60°二极C型铁磁场特性的研究

兰州重离子加速器冷却储存环主环注入线二极C型磁铁首次采用了磁极头中埋置垫补线圈调整磁场均匀度的设计.在其磁场测量中,使用了点测和积分测量的方法对其各方面特性参数进行了测量,并对积分场的测量结果以及内置垫补线圈对均匀场的垫补效果进行了详细的非线性分析.     

冷却储存环主环注入线二极磁铁测量

 介绍了兰州重离子加速器冷却储存环工程主环注入线二极磁铁的测磁系统和测磁结果。着重分析了垫补线圈和极头削斜两种手段对C型弯曲二极磁铁积分磁场径向分布均匀度的调节效果。并且分析了TOSCA三维磁场计算程序与实际测量结果之间的误差及其产生的原因。     

强流回旋加速器综合试验装置的磁场测量与垫补

强流回旋加速器综合试验装置的主体是一台紧凑型回旋加速器,加速器主磁铁材料的不均匀性,磁铁加工和安装的非理想因素将引起中心平面的磁场的非理想分布,因此有必要对其中心平面的磁场进行测量和垫补.本文主要讲述该综合试验装置的霍尔感应磁场测量系统的设计和使用;通过磁场测量数据分析进行镶条的再加工,最终实现对等时性磁场和束流的纵向聚焦的垫补;研究与实践了一种对磁场一次谐波进行垫补的方法,垫补的结果满足了设计的要求.     

强流回旋加速器综合试验装置的磁场测量与垫补

强流回旋加速器综合试验装置的主体是一台紧凑型回旋加速器, 加速器主磁铁材料的不均匀性, 磁铁加工和安装的非理想因素将引起中心平面的磁场的非理想分布, 因此有必要对其中心平面的磁场进行测量和垫补. 本文主要讲述该综合试验装置的霍尔感应磁场测量系统的设计和使用;通过磁场测量数据分析进行镶条的再加工, 最终实现对等时性磁场和束流的纵向聚焦的垫补;研究与实践了一种对磁场一次谐波进行垫补的方法, 垫补的结果满足了设计的要求.     

冷却储存环主环注入线四极磁铁测量

 介绍了兰州重离子加速器冷却储存环工程主环注入线四极磁铁谐波测磁系统和谐波磁场测量结果。分析了磁铁误差产生的原因以及磁铁加工存在的问题和注意事项。     

CSRe储存环等时性模式转变能洛伦兹因子曲线的测量与校正

综述了兰州冷却储存环CSRe上转变能洛伦兹因子的测量与校正的最新进展,详细阐述了基于等时性质谱仪实验数据测量储存环的转变能洛伦兹因子的方法,以及利用CSRe二极、四极、六极磁铁校正转变能洛伦兹因子曲线的结果。实验结果表明,二极磁铁和四极磁铁可以平移转变能洛伦兹因子曲线,六极磁铁可以旋转转变能洛伦兹因子曲线。通过校正CSRe的转变能洛伦兹因子曲线,将CSRe对目标离子的质量分辨能力R=m/△m=3.15（9）×104（FWHM）（回旋周期相对误差σT/T=7.3（2）×10-6）提高到1.72（4）×105（FWHM）（σT/T=1.34（3）×10-6）。     

二极铁均匀场修正

HI-13串列加速器升级工程中的ISOL高质量分辨谱仪要求20000的质量分辨率, 分析磁铁磁场均匀性要求好于1×10-5。 要达到这样高的磁场均匀性, 必须对磁铁进行垫补。 介绍了二极铁表面线圈垫补均匀场的设计方法和制作工艺, 并且基于现有的一块C型二极铁对表面线圈垫补均匀场的方法进行了实验研究。 实验结果表明, 采用表面线圈垫补后, 场均匀性提高了一个数量级, 积分场的均匀性从5×10-4提高到3×10-5。 The mass resolving power of ISOL’s spectrometer for Beijing Radioactive Ion beam Facilities project is 20000, which requires the field uniformity of the magnet better than 1×10-5. To achieve such a high uniformity field,field optimize is indispensable. This paper presents the design method,manufacture techniques and experiment results of surface coils,which are set on pole face of a dipole to improve the magnetic field homogeneity. The integral field uniformity with surface coil is optimized to 3×10-5 from 5×10-4,which is improved roughly an order of magnitude.     

兰州重离子冷却储存环二极磁铁设计

介绍了兰州重离子冷却储存环主环(CSRm)的改进W型二极磁铁和实验环(CSRe)C型二极磁铁的磁场计算和物理设计,在降低了磁铁造价和运行费用的前提下设计参数达到或超过了物理要求.根据样机的加工和检测结果来看,所有的磁场计算和物理设计的结果是可靠的.Magnetic field calculation and design of CSRm modified W-type dipoles and of CSRe C-type dipoles are presented in this paper. Under the condition of lower cost, all of the designed parameters are better than required values. Now the prototype has been fabricated and also the magnetic field measurement has been done. According to the measured results, all the calculation and design are very reliable.     

光学速调管改造后辐射段磁场垫补和测量

 合肥国家同步辐射实验室正在开展储存环相干谐波自由电子激光研究，并对原来的光学速调管进行了改造。磁场的垫补和测量方法由原来的整体测量改为分段进行，垫补的使用使各段积分场及位相误差都尽可能小。详述了合肥储存环的光学速调管辐射段磁场垫补的三种方式，测量了垫补前后不同间隙下积分场分布、位相误差及横向均匀度，各项指标都达到了要求。同样的方法将用于色散段和调制段磁场垫补与测量中，为相干谐波自由电子激光研究提供实验保障。     

混合物物态方程的计算

 在采用体积相加原理计算混合物物态方程的基础上,建立了一种物理模型确定混合物温度。根据混合物中各组分温度和压强平衡条件,采用压强-密度迭代方法计算给出混合物物态方程,编制了两种组分的混合物物态方程计算程序。为检验建立的温度模型的合理性及程序的有效性,分析了不同密度、温度状态的氢（H2）和钨（W）组成的混合物状态参量,计算了以下情形及其组合情形的混合物物态方程：H₂和W以不同质量比混合;质量比固定,单组分状态不同;温度区间和密度区间不同。研究表明:实际应用中在建立的混合物温度模型基础上确定的混合物物态方程是合理的。     

分子费米共振拉曼光谱强度分析

测量了CCl₄和CS₂分子的Raman光谱。用Bertran理论和群论等相关理论对其光谱强度进行了分析,获得了发生费米共振分子的拉曼光谱强度的特殊规律： (1)发生费米共振的基频和倍频(和频)间发生能量转移,两光谱强度大小相互接近,当发生费米共振的基频和倍频(和频)间距离很小时,两发生费米共振的光谱强度相等(R=1);(2)能出现倍频光谱强度高于其基频光谱强度;(3)也会观测到费米共振光谱,而观测不到参与费米共振的和频中的基频光谱。此研究对化学、材料科学中的分子结构、材料成分等研究中的谱线认证、归属有很好的参考价值。     

Infrared Quantitative Study of Acetylation of Microspheres of Polystyrene

Abstract

Fourier transform infrared spectroscopy has been used to study quantitatively the acetylation of monodisperse polystyrene microspheres with diameters ranging from 7 to 9μm. The CH₂ stretching infrared vibration mode at 2921 cm^?1 was used as the internal intensity standard. The acetylation extent could be easily measured by comparing the relative intensities of the bands of acetyl group (1678, 1415, 1359 cm^?1) or the bands due to the para-substituted benzene ring to the band at 2921 cm^?1 from the calibration curve.     

Asymptotic properties of sequences of iterates of nonlinear transformations

By considering functions defined on the unit interval with a single zero minimum and a single unit maximum we are led to a version of the doubling or universal transformation. The fixed point functions of this doubling transformation have certain invariance properties under conjugacy. These invariance properties lead to a widening of the concept of universality to power law conjugacy classes in which the Feigenbaum divergence parameter is a function only of the product of the powers with which iterating functions approach unity at the maximum and zero at the minimum. We also construct an effective method for computing the divergence parameter from iterates, and derivatives of iterates, generated by the appropriate fixed point function.On leave from Mathematics Department, University of Melbourne, Parkville, Victoria 3052, Australia.     

Application of the method of X-ray fluorescence analysis for determination of the degree of chlorination of copper phthalocyanin

To whom correspondence should be addressd.     

BSA-SDS-Ag聚合物纳米微粒的制备及其水凝胶性质的研究（Ⅰ）

报道了BSA－SDS－Ag聚合物纳米微粒的制备及水凝胶的性质,用X射线衍射（XRD）、透射电镜（TEM）、傅里叶变换红外（FT－IR）光谱考察了这种聚合物微粒的结构,微粒粒径32nm左右,用UV／Vis光谱及SEM考察了冰凝胶的性,表明Ag^ 离子先与BSA产生化学键合,再学原了Ag粒,进行聚合成网状结构的聚合物。     

Basin of attraction of cycles of discretizations of dynamical systems with SRB invariant measures

Computer simulations of dynamical systems arediscretizations, where the finite space of machine arithmetic replaces continuum state spaces. So any trajectory of a discretized dynamical system is eventually periodic. Consequently, the dynamics of such computations are essentially determined by the cycles of the discretized map. This paper examines the statistical properties of the event that two trajectories generate the same cycle. Under the assumption that the original system has a Sinai-Ruelle-Bowen invariant measure, the statistics of the computed mapping are shown to be very close to those generated by a class of random graphs. Theoretical properties of this model successfully predict the outcome of computational experiments with the implemented dynamical systems.     

Electron microscopy study of aggregation of microclusters of sulphur

A study of aggregation of sulphur particles in colloidal suspension of sulphur in water-methanol mixture using TEM and electron diffraction is reported. From the micrographs the aggregates formed have been found to be random and tenuous indicating a fractal structure. The electron diffraction patterns of the aggregates are used to study the mechanism of diffusion and reaction limited aggregation.     

Some peculiarities of deep PT-changes of physical properties of rocks

Abstract

Results of petrophysical PT-experiments are discussed. Used is a method of program modeling of experiments. Thermobaric dependence of elastic properties of acid, intermediate and basic rocks as well as elastic wave velocity anisotropy in amphibolites is studied. Deep PT-regimes effect on electrical resistance of dry and water-saturated rocks has been studied. PT-conditions of full loss of the remanent magnetization of volcanites have been established. A number of regional petrophysical lithosphere models has been constructed.