液相色谱-同位素稀释串联质谱法测定动物源性食品中硝基呋喃类代谢物残留

加入同位素标记物的动物源性样品(龙虾、肠衣),在酸性条件下用2-硝基苯甲醛,使样品中呋喃唑酮、呋喃西林、呋喃它酮、呋喃妥因实现衍生。经乙酸乙酯提取浓缩、用甲醇水溶液溶解过滤后,滤液用液相色谱-串联质谱定量。在0.5,1.0和2.0μg/kg3个浓度水平上进行添加回收试验,回收率为80.1％～92.2％,检出限(LOQ)...     

碳纳米管辐射太赫兹波的理论分析与数值验证

基于简单紧束缚方法理论,利用一维碳纳米管的量子化周期边界条件得到了碳纳米管的电子能级结构关系.并结合已报道的碳纳米管中电子与声子相互作用的实验结果,得到了碳纳米管能够辐射太赫兹波的结论.通过数值结果验证了碳纳米管在外场作用下能够产生太赫兹波,并对数值计算结果中太赫兹波的振荡现象给予合理的解释.其结果为进行碳纳米管产生太赫兹辐射的实验研究提供深入的理论基础. 关键词： 太赫兹波 碳纳米管     

Novel wavelength-accurate InP-based arrayed waveguide grating

A 13-channel, InP-based arrayed waveguide grating （AWG） is designed and fabricated in which the on-chip loss of the central channel is about -5 dB and the crosstalk is less than -23 dB in the center of the spectrum response. However, the central wavelength and channel spacing are deviated from the design values. To improve their accuracy, an optimized design is adopted to compensate the process error. As a result, the central wavelength 1549.9 nm and channel spacing 1.59 nm are obtained in the experiment, while their design values are 1549.32 nm and 1.6 nm, respectively. The route capability and thermo-optic characteristic of the AWG are also discussed in detail.     

Quantum key distribution transmitter chip based on hybrid-integration of silica and lithium niobates

A quantum key distribution transmitter chip based on hybrid-integration of silica planar light-wave circuit (PLC) and lithium niobates (LN) modulator PLC is presented. The silica part consists of a tunable directional coupler and 400-ps delay line, and the LN part is made up of a Y-branch, with electro-optic modulators on both arms. The two parts are facet-coupled to form an asymmetric Mach-Zehnder interferometer. We successfully encode and decode four BB84 states at 156.25-MHz repetition rate. Fast phase-encoding of 0 or $\pi $ is achieved, with interference fringe visibilities 78.53% and 82.68% for states $|+\rangle$ and $|-\rangle$, respectively. With the aid of an extra off-chip LN intensity modulator, two time-bin states are prepared and the extinction ratios are 18.65 dB and 15.46 dB for states $|0\rangle$ and $|1\rangle$, respectively.     

基于COMSOL的纳米傅里叶红外光谱系统数值模型

傅里叶红外光谱（FTIR）是材料表征的一种重要手段,然而受限于光的衍射极限,传统傅里叶红外光谱仪的极限空间分辨率在微米量级,无法应用于纳米材料的表征。纳米傅里叶红外光谱（Nano-FTIR）是一种新兴的超分辨光谱表面分析技术,其以纳米级空间分辨率、宽光谱范围和高化学灵敏性的特点在纳米材料表征研究中展现了巨大的潜力。定性及定量的研究Nano-FTIR信号高空间分辨的来源和系统中光谱信号的提取过程,可以为Nano-FTIR仪器的设计研发和样品光谱表征结果的解释提供重要依据。该研究从典型的仪器结构和基本的工作原理出发,在多物理场有限元分析软件COMSOL中建立了等效研究模型,并对模型的重要细节和数值计算过程分别进行了说明。在仿真研究中,首先基于麦克斯韦电磁波理论计算了模型空间的电磁场增强情况,再模拟了探针在介电常数差异巨大的两种材料交界处的“线扫”过程,探讨了针尖近场增强信号的空间分辨率。随后,以探针与样品的散射功率为数值模型的研究对象,仿真了探针“轻拍”对信号的调制和解调提取的过程,并讨论了不同入射倾角和解调频率对光谱信号提取的影响。最后,为了验证模型的合理性,仿真了20,100和300 nm三种厚度SiO₂薄膜样品在900～1 250 cm-1波数范围的光谱响应,并将仿真得到的光谱与实测结果进行了对比。结果表明随着样品厚度的增厚,光谱信号得到相应的增强,模型预测的谱图与实测谱图波形与波峰位置较为一致,且与以往一些文献中采用针尖-样品间电场强度表示针尖处散射信号强弱的方法相比,获得的谱图在峰形上更为接近。提出的数值模型可用于Nano-FTIR光谱的预测,此外,模型也具有一定的通用性,可以为其他基于散射型近场光学显微（s-SNOM）技术的太赫兹光谱技术和针尖增强拉曼光谱研究提供一定的借鉴。     

用于放射性束流的RFQ冷却聚束器

简要概述RFQ冷却聚束器的基本原理, 并给出了利用SIMION程序模拟的部分结果. 设计中的RFQ冷却聚束器与国际上其它同类设备相比, 具有特征半径大、入射粒子的允许能量上限值高和氦气气压高的特点, 因此本文最后对需要克服的困难作了一个简要的阐述.     

2.5维圆波导开放边界截断的修正完全匹配层方法

 在时域有限差分算法中，完全匹配层是一种高效的吸收边界条件。通过在标准完全匹配层(PML)方程中添加具有物理意义的电导率和导磁率附加项，提出了修正完全匹配层(MPML)方法，给出了圆柱坐标下3维MPML方程，并应用于2.5维圆波导开放边界的截断计算。计算结果表明，在不同频率和模式的激励下，加入平滑电导率和导磁率附加项后，与标准PML方法相比，MPML方法的相对误差降低8~10 dB。     

MOVPE生长的InGaN/GaN单量子阱的光致发光和光吸收特性

研究了用金属有机物气相外延(MOVPE)法在蓝宝石衬底上生长的In组分浓度保持不变的InGaN/GaN单量子阱结构在室温下的发光特性和光吸收特性.实验结果表明,在InGaN厚度<3nm时,随着样品InGaN势阱层宽度的增加(1nm),光致发光(PL)谱的发光峰值波长出现明显的红移33nm现象,而且发光强度下降8%,谱线半峰全宽(FWHM)展宽,通过对样品的透射、反射光谱研究发现,量子阱层窄(1.5nm)的样品在波长接近红外区时出现无吸收的现象,即R+T达到了100%,而在阱层较宽的样品中没有发现这一现象,对引起这些现象的原因进行了讨论.这些结果有助于开发和优化三族氮化物半导体光电器件的进一步研究工作.     

Configuration of the valence neutrons of 17B

The reaction cross section of ~(17)B on ~(12)C target at(43.7±2.4)MeV/u has been measured at the Radioactive Ion Beam Line in Lanzhou(RIBLL).The root-mean-square matter radius(R_(rms))was deduced to be(2.92±0.10)fm,while the R_(rms)of the core and the valence neutron distribution are 2.28 fm and 5.98 fm respectively.Assuming a"core plus 2n"structure in ~(17)B,the mixed configuration of(2s_(1/2))and(1d_(1/2))of the valence neutrons is studied and the s-wave spectroscopic factor is found to be(80±21)%.     

Realization of MMI Power Splitter by UV-light Imprinting Technique Using Hybrid Sol-Gel SiO2 Materials

An efficient fabrication scheme of buried ridge waveguide devices is demonstrated by UV-light imprinting technique using organic-inorganic hybrid sol-gel Zr-doped SiO2 materials. The refractive indices of a guiding layer and a cladding layer for the buried ridge waveguide structure are 1.537 and 1.492 measured at 1550nm, respectively. The tested results show more circular mode profiles due to existence of the cladding layer. A buried ridge single-mode waveguide operating at 1550 nm has a low propagation loss （0.088 dB/cm） and the 1× 2 MMI power splitter exhibits uniform outputs, with a very iow splitting loss of 0.029 dB at 1549nm.