一维丝室气体探测器衍射像差的修正方法研究

一维位置灵敏单丝气体探测器采用单根镀金钨丝和200根阴极感应条的探测结构, X射线在阳极丝上产生的信号被多个阴极条感应, 利用重心法得到X射线的原初电离点的位置信息, 位置分辨率达到160 μm(半高全宽). 在同步辐射衍射实验中, X射线通过样品后会形成不同大小的衍射环, 本实验中测量得到11.148°和14.201°的两组衍射角位置信息; 通过平行移动一维探测器在衍射环范围内多次扫描, 可以重建得到二维衍射环. 由于一维探测器的气体厚度和入射窗宽度会给测量结果带来像差, 分析发现像差的影响大于一维探测器的位置分辨. 基于相应的物理分析对测量到的衍射位置进行修正, 修正后的衍射位置相比修正前的衍射位置的相对像差最大改善达到7%, 该方法实现了无像差二维衍射环的重建.     

Beam test of a one-dimensional position sensitive chamber on synchrotron radiation

A one-dimensional single-wire chamber was developed to provide high position resolution for powder diffraction experiments with synchrotron radiation. A diffraction test using the sample of SiO₂ has been accomplished at 1W2B laboratory of Beijing Synchrotron Radiation Source. The data of the beam test were analyzed and some diffraction angles were obtained. The experimental results were in good agreement with standard data from ICDD powder diffraction file. The precision of diffraction angles was 1% to 4.7%. Most of the relative errors between measured values of diffraction angles and existing data were less than 1%. As for the detector, the best position resolution in the test was 138 μm (σ value) with an X-ray tube. Finally, discussions of the results were given. The major factor that affected the precision of measurement was deviation from the flat structure of the detector. The effect was analyzed and the conclusion was reached that it would be the optimal measurement scheme when the distance between the powder sample and detector was from 400 mm to 600 mm.     

Time calibration for the end cap TOF system of BESⅢ

The time calibration for end cap TOF system of BESⅢ is studied in this paper. It has achieved about 110 ps time resolution for muons in dimu events. The pulse height correction using electronic scan curve and the predicted time calculated using Kalman filter method are introduced. This paper also describes the study of using electrons and muons as calibration samples.     

散裂中子源高气压二维位置灵敏3He探测器的实验研究

为满足中国散裂中子源多功能反射谱仪中子探测器的基本物理要求:有效面积达到200 mm×200 mm、探测效率大于50%（2Å）、位置分辨好于2 mm等,中国科学院高能物理研究所研制了3He高气压二维多丝正比室位置灵敏中子探测器。该探测器采用二维多丝室结构,腔体内充3He/C₃H₈（6 atm/2.5 atm）的组合气体。本文首先利用Am/Be中子源完成对探测器全面积均匀性测试,均匀性指标达到了95.1%;探测器在中国散裂中子源的20号束流线站安装后,对其进行了在束测量,通过飞行时间选取波长2.8Å的慢中子,测量了探测器二维位置分辨和二维成像性能。在X方向（垂直于阳极丝的方向）的位置分辨为0.99 mm,Y方向（平行于阳极丝的方向）的位置分辨为1.36 mm,探测器具有很好的二维位置分辨和二维成像能力。测量结果表明探测器满足反射谱仪的研制要求。     

MoSe2/Ag3PO4复合材料的制备及其可见光降解罗丹明B的光催化性能

通过原位沉积法合成了一种光催化活性强、稳定性高的MoSe2/Ag3PO4复合材料。MoSe2/Ag3PO4形成的异质结构能有效分离光生电子-空穴对,从而提高光催化活性。光生电子从Ag3PO4表面向MoSe2的转移降低了Ag+向金属Ag的可能性。当MoSe2和Ag3PO4的质量分数为1∶5(最优组合)时,MoSe2/Ag3PO4在可见光照射下30 min内降解RhB效率达98%,并且经过4次重复试验,其可见光照射下RhB降解效率仍可达到89%。通过液相色谱/质谱(LC/MS)技术测定光催化过程中产物的变化,提出了MoSe2/Ag3PO4光催化降解RhB的途径。