共查询到19条相似文献,搜索用时 531 毫秒
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采用固体烧结法制备了Sr2-xSmxFeMoO6(x=0,0.03,0.05,0.08,0.10,0.13,0.15,0.20)多晶结构样品,用X射线衍射对材料的结构进行了检测。通过光热偏转技术方法对该材料的热扩散率进行了研究,给出了掺杂比例与材料热扩散率的关系曲线,结果发现Sr2FeMoO6样品随着参杂Sm浓度的增加,结构发生变化的同时,样品的热扩散率也随着波动变化。这与文献[1]中给出的结论有明显不同,从声子、电子、自旋及其相互作用角度揭示了与文献[1]不同的根本原因;并且从x射线和热扩散率两个角度给出了样品Sr2-xSmxFeMoO6结构转变的参杂比例在10—13%的范围,说明光热偏转技术方法是研究参杂镧系元素的双钙钛矿结构和电子参杂效应的可行有效方法。 相似文献
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采用激光光热透射技术测量材料的热扩散率 总被引:2,自引:0,他引:2
介绍利用激光光热透射技术测量材料热扩散率的方法,用该方法测量黄铜,纯铁、铝、纯铜及锗的热扩散率,其结果与能常采用的检测手段一致。 相似文献
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在热导率沿试样厚度按指数规律渐变的假设下,利用两种基本数学变换,求解了非均匀材料的热传导方程,得到了试样内及与其相邻媒质内的温度场解析解。再根据光热光偏转理论,确定了检测光束切向偏转分量的位相与调制频率之间的函数关系,如果利用熟知的由检测光束法向偏转分量测定试样热扩散率的技术,测定试样两表面的热扩散率,这样就可以由Mirage效应的两个偏转分量来测定试样热扩散率沿厚度方向的分布。本文给出有关的理论推导,同时也给出了人造金刚石试样内热扩散率分布的实验结果。 相似文献
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描述了光热辐射测量术的特点、原理和测量装置,并扼要介绍了材料热扩散率、材料表面伤痕和内部缺陷的无损检测。 相似文献
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Transient thermal gratings at surfaces for thermal characterization of bulk materials and thin films
O. W. Käding H. Skurk A. A. Maznev E. Matthias 《Applied Physics A: Materials Science & Processing》1995,61(3):253-261
Transient Thermal Gratings (TTGs) at surfaces of absorbing materials have been utilized for investigating heat diffusion in bulk materials and thin films. In this report, we describe the theoretical background of the technique and present experimental data. TTGs were excited in the surface plane by interference of two pulsed laser beams and monitored by a cw probe beam, either via temperature dependence of the reflectivity or by deflection from the displacement pattern. A theoretical model describing the thermal and thermoelastic surface response was developed, both for a homogeneous material and a multilayer structure. The potential of the technique will be demonstrated by experimental results on (i) thermal diffusivities of bulk materials, (ii) anisotropic lateral heat transport, and (iii) thermal diffusivities of metal and diamond films. Furthermore, we will show that TTGs allow thermal depth profiling of inhomogeneous materials whenever there is a vertical gradient in thermal conductivity. 相似文献
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Study on thermal diffusivity of materials by laser photothermal reflection technique 总被引:1,自引:0,他引:1
A method of measuring thermal diffusivity of materials at room temperature by photothermal reflection technique is described. An intensity-modulated Ar+ laser beam is used as incident light. The beam is focused to about 1 mm diameter spot and illuminates the sample surface. HgCdTe infrared detector is used to receive photothermal signal. Using this technique, the photothermal signals are experimentally measured as the function of different frequencies. The thermal diffusivities can be obtained by fitting the experimental data. On the other hand, the thermal diffusivities of one-way composite and orthogonal symmetric arranged composites Al2O3/Al are measured in transverse, longitudinal and arbitrary directions. The results show that the diffusivity of one-way material decreases with the increase of the measurement angle; the diffusivity of orthogonally arranged material almost keeps the same when measurement angle changes. 相似文献
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本文报道了在室温下BaTiO3及BaTiO3:Ce的拉曼谱的特点,着重讨论了前向散射配置下两个1I(TO)模(位于275cm-1和516cm-1左右)出现在A1(TO)谱中的原因。通过设计特别的前向散射实验得到了此配置下由于晶体出射面对入射光的反射造成的背向散射的强度。在BaTiO3的前向散射谱中扣除了背向散射信号后,两个宽峰基本减掉,而掺Ce后经同样扣除背向散射信号两宽峰却依然很强。这样便证明了它们在前向散射中的出现与杂质有关系。在BaTiO3扣除背向散射后的谱中,还首次观察到一个位于492cm-1的峰。掺Ce后晶体的吸收曲线有很大变化,本文还讨论了吸收对散射强度的影响。 相似文献
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A distance-scan method to determine the distance between the probe beam and sample, which is not easily measured exactly, in photothermal deflection (PD) was reported, with which the distance and thermal diffusivity of the deflecting medium can be simultaneously measured. Probe beam size effect (PBSE) on PD phase signal was quantitatively analyzed to clearly show its physical meaning. The measured distance was experimentally verified as correct and reliable, and the measured thermal diffusivities of N2 and CO2 are in good agreement with the literature values. They could not be precisely measured by phase signal without considering the PBSE. 相似文献
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用共线光热偏转技术测量光学薄膜的微弱吸收 总被引:2,自引:0,他引:2
用具有高灵敏的共线光热偏转技术研究SiO_2、ZrO_2、MgF_2、ZnS等单层光学薄膜的吸收特性,测得它们的吸收率.实验结果与激光量热法及横向光热偏转技术符合良好,表明共线光热偏转技术是测量光学薄膜弱吸收的较理想方法. 相似文献
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《中国物理 B》2018,(12)
The electrocaloric effect of the model ferroelectric BaTiO_3 was investigated using phenomenological theory. The results indicate that the applied electric field strength is a key factor for the induced electrocaloric response and there are two distinguishing electrocaloric responses. When a moderate electric field is applied, the electrocaloric temperature variation is small but the electrocaloric strength is high. In contrast, the electrocaloric temperature variation is large but electrocaloric strength is low when a very high electric field is applied. These results are consistent with the experimental observations on BaTiO_3 based bulk and thin film ferroelectric materials. 相似文献
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