基于同步辐射的快速扫描X射线微束荧光成像方法

在上海光源硬X射线微聚焦光束线站(BL15U1)上, 基于EPICS软件平台, 集成运动控制, 光强探测, 荧光探测等功能, 实现了"飞行"模式 (on-the-fly) X射线扫描微束荧光成像方法. 用"飞行"扫描X射线荧光成像法获得了标准镍网, 以及微量元素Cu, Zn,K, Fe在样品老鼠脾内的分布图像, 结果显示该方法不但在速度上有了极大的提高, 而且获得的元素分布图像具有高质量. 关键词： 快速扫描X射线微束荧光成像 同步辐射 微量元素分布     

Hard X-ray one dimensional nano-focusing at the SSRF using a WSi2 /Si multilayer Laue lens

The multilayer Laue lens (MLL) is a novel diffraction optics which can realize nanometer focusing of hard X-rays with high efficiency. In this paper, a 7.9 μm-thick MLL with the outmost layer thickness of 15 nm is designed based on dynamical diffraction theory. The MLL is fabricated by first depositing the depth-graded multilayer using direct current (DC) magnetron sputtering technology. Then, the multilayer sample is sliced, and both cross-sections are thinned and polished to a depth of 35-41 μm. The focusing property of the MLL is measured at the Shanghai Synchrotron Facility (SSRF). One-dimensional (1D) focusing resolutions of 205 nm and 221 nm are obtained at E=14 keV and 18 keV, respectively. It demonstrates that the fabricated MLL can focus hard X-rays into nanometer scale.     

上海同步辐射装置波荡器光源空间相干性的研究

利用高斯-谢尔光源模型理论与交叉谱密度函数在自由空间传输的规律, 研究了上海同步辐射装置波荡器光源(BL15U)的空间相干性; 讨论了预聚焦镜、单色器对光束空间相干性的影响;实验测量了单色光狭缝S2处光束的横向相干长度(Z方向). 理论计算表明, S2处光束的横向相干长度为66.5 μm,但实验测量结果为27 μm. 理论与实验相差较大的原因是由于S2上游光学元件预聚焦镜或单色器周期性高频振动导致了光束空间相干性的退化.实验结果表明,上海同步辐射装置波荡器光源已有较强的空间相干性, 可以满足微米尺度的硬X射线相干性实验.     

级联式平面抛物面型X射线组合折射透镜的设计与制作

X射线组合折射透镜(CRL)已逐步成为同步辐射光源下X射线聚焦光学器件的标准配件之一,它具有结构紧凑、易调节校准、适用光子能量范围大等优点.本文设计了一种级联式平面抛物面型CRL,它将N1个具有较大抛物面几何孔径(R0)的折射单元I与N2个具有较小抛物面顶点曲率半径(R)的折射单元II级联,以解决常规CRL设计过程中焦斑尺寸与透过率的矛盾.采用PMMA材料,利用LIGA技术制作了一组级联式平面抛物面型CRL,其中折射单元I的主要结构参数为N1=15,R1=200μm,2R01=564μm;折射单元II的主要结构参数为N2=20,R2=50μm,2R02=140μm.在上海光源同步辐射线束上,所制作的级联式平面抛物面型CRL实现了对初始光斑尺寸为200μm×100μm的入射X射线的一维聚焦,测试得到的焦距为1.052 m,横向焦斑尺寸为24.9μm@8 keV,透过率为2.19%.     

Design optimization of a tapered mirror for microfocusing optics

A facile microfocusing optical design is presented which is optimized for less slope error against the traditional tapered mirror. The essential idea of the innovation is based on the characteristics of the slope-error curve for the prototype. The relationship between the mirror shape of the improved model and the driving moments is established. Analytical results have been compared with the results of the prototype. The design demonstrates theoretically that smaller slope error is obtained with longer active length.