不同杂环取代(E)-β-Farnesene类似物的合成及生物活性研究

为了寻求新型蚜虫控制剂,以蚜虫报警信息素(E)-β-farnesene(EBF)为先导,引入不同类型的杂环取代EBF结构中不稳定的共轭双键,设计合成了一系列不同杂环取代的EBF类似物.所有化合物结构均通过1H NMR、13C NMR、IR及HRMS确证.对化合物进行了生物活性测试及初步构效关系分析.结果表明,所有化合物均对桃蚜和大豆蚜表现出一定的生物活性,部分化合物的杀虫活性优于先导EBF,酯基的引入则对驱避活性有利.     

玻璃料对铜基金属结合剂性能及结构的影响

采用粉末冶金法向铜基金属结合剂中引入玻璃料,结合材料电子万能试验机、洛氏硬度仪、SEM等检测方法,研究了玻璃料加入对铜基金属结合剂及金刚石磨具的影响.结果表明,随着玻璃料含量的增加,铜基结合剂的抗折强度和抗冲击强度呈下降的趋势,其硬度呈逐渐上升趋势,硬脆相的引入提高了铜基金属结合剂的自锐性;玻璃相和金属相之间结合紧密,两相之间化学元素在界面处发生相互扩散;玻璃料的加入使结合剂对磨料的包裹更加紧密,大大提高了结合剂对金刚石的把持力,有利于增加金刚石磨具寿命及加工效率.     

O′-β′复相Sialon陶瓷中相组成的控制

用Si₃N₄,SiO₂和Al₂O_?作原料,以Y₂O_?为添加剂,研究了O’-β’所在的四个相容性区中组成,于1400—1800℃之间,O’和β’的形成动力学。O’于1400℃开始生成,1600℃达到最大形成量。高于1600℃,O’减少乃至消失。研究发现,O’的这种不稳定性,并非自身热分解的结果。Al含量的增加,液相出现和β’的形成,才是导致O’-Sialon溶解而消失的原因。 此外,认为Si₃N₄-O’(x=0.3)-Y₂Si₂O₇-YAG相容性区,是在制备具有合理的O’-β’平衡相组成的复相陶瓷时,可供实际选用的组成区。     

The compensability between the longitudinal andtransverse mismachining tolerance of gratingin the optical pick-up head

In this paper numeric analysis is made to the influence of the longitudinal mismachining tolerance (LMT) and the transverse mismachining tolerance (TMT) of the grating in the optical pick-up head (GOPH) of VCD, DVD, and CD-ROM on the transmissivity and the intensity ratio of the auxiliary light beam to the main read-write light beam (IRAM) by using the general expression of diffraction efficiency obtained from the scalar diffraction theory. On solving GOPH problem, the scalar diffraction theory and the vector diffraction theory are coincident, and the scalar diffraction theory is reliable. The result shows that LMT and TMT can compensate for the inverse effect of IRAM, however, at the expense of reducing transmissivity. As far as GOPH is concerned, the goodness that LMT and TMT can be effectively compensated for is very advantageous in manufacturing of the grating.     

“神龙一号”注入器研制

“神龙一号”注入器是直线感应加速器的束流源，它采用了感应叠加的高压加载方式，包括脉冲功率系统、感应腔、阴阳极杆、绝缘支撑、二极管和束流传输系统等子系统. 在研制中采用了径向绝缘支撑、对中支撑调节系统、类Pierce阴极等先进技术，以及二极管线圈内置和外径为800mm的铁氧体大环等创新. 参数测试显示，3.5MeV注入器达到了世界先进水平.     

改变教学观念提高写作能力——论成人高等教育应用文写作课的特点和教法

本文在分析应用文写作课普遍存在的问题的基础上，探讨成人高校应用文写作课的特点、目的，提出解决的办法，提高学生写作能力，使学生写出合乎规范的文章，适应实际工作的需要。     

铂对硫芴加氢脱硫钼催化剂的促进作用

铂对硫芴加氢脱硫钼催化剂的促进作用王军李文钊张盈珍ＴＨＥＰＲＯＭＯＴＩＯＮＥＦＦＥＣＴＯＦＰＬＡＴＩＮＵＭＯＮＭＯＬＹＢＤＥＮＵＭＣＡＴＡＬＹＳＴＦＯＲＨＹＤＲＯＤＥＳＵＬＦＵＲＩＺＡＴＩＯＮＯＦＤＩＢＥＮＺＯＴＨＩＯＰＨＥＮＥＷａｎｇＪｕｎ，ＬｉＷ...     

Effects of Substrate Temperature on Helium Content and Microstructure of Nanocrystalline Titanium Films

Helium-charged nanocrystalline titanium films have been deposited by HeAr magnetron co-sputtering. The effects of substrate temperature on the helium content and microstructure of the nanocrystalline titanium films have been studied. The results indicate that helium atoms with a high concentration are evenly incorporated in the deposited titanium films. When the substrate temperature increases from 60℃ to 350℃ while the other deposition＇parameters are fixed, the helium content decreases gradually from 38.6 at.% to 9.2at.%, which proves that nanocrystalline Ti films have a great helium storage capacity. The 20 angle of the Bragg peak of （002） crystal planes of the He-charged Ti film shifts to a lower angle and that of （100） crystal plane is unchanged as compared with that of the pure Ti film, which indicates that the lattice parameter c increases and a keeps at the primitive value. The grain refining and helium damage result in the diffraction peak broadening.     

活动标形及其在点啮合齿轮传动误差分析中的应用

活动标形法的论述首推苏步青译，佐佐木重夫著《微分几何学》，还有的著作从外微分形式引入活动标形,本文论证取曲面的正交曲率网为参数网时，曲面论的基本公式就是活动标形的微分形式，并用其分析了点啮合齿轮传动误差．