Nano-Crystalline Diamond Films with Pineapple-Like Morphology Grown by the DC Arcjet vapor Deposition Method

A nano-crystlline diamond film is grown by the dc arcjet chemical vapor deposition method. The film is characterized by scanning electron microscopy, high-resolution transmission electron microscopy （HRTEM）, x-ray diffraction （XRD） and Ftaman spectra, respectively. The nanocrystalline grains are averagely with 80hm in the size measured by XRD, and further proven by Raman and HRTEM. The observed novel morphology of the growth surface, pineapple-like morphology, is constructed by cubo-octahedral growth zones with a smooth faceted top surface and coarse side surfaces. The as-grown film possesses （100） dominant surface containing a little amorphous sp2 component, which is far different from the nano-crystalline film with the usual cauliflower-like morphology.     

基于核映射多光谱特征融合的高光谱遥感图像分类法

多光谱遥感图像的波段设定在理论和实践上都极具地物针对性,在更有效的数据挖掘方法帮助下可以提取足够的光谱特征以区分地物,本文将光谱匹配技术用于相似性度量,以提高分类准确度.首先选定光谱角制图、光谱相关制图、Mahalanobis距离、光谱相似度和光谱信息差异做为光谱度量;随后选择高斯核函数,在选定核函数之后,得到了核映射下的光谱特征度量来挖掘高光谱遥感数据的光谱特征.最后采用核映射多光谱特征融合法对多光谱遥感图像光谱特征的相似性进行描述,得到基于核映射多光谱特征融合的高光谱遥感图像分类算法.使用MATLAB中的LIBSVM工具箱对AVIRIS高光谱遥感数据进行分类实验,并与已有算法进行对比,结果表明本文提出的算法具有较高的分类准确度和性能.     

食品中三聚氰胺的光谱检测与分析技术研究进展

三聚氰胺是豆、乳类制品中的非法食品添加剂,曾作为蛋白质的廉价代替物被非法添加进奶粉等食品中,造成了严重的社会危害,极大地威胁人民生命财产安全。目前光谱技术已成为识别和定量检测非法食品添加剂的有效手段,为质量监管部门提供了可靠的研究方法和鉴定依据。光谱检测技术的时效性、无损性和准确性提高了食品中三聚氰胺的检测效率,促进了精准化、自动化食品质量检测的发展。近年来有大量研究围绕着三聚氰胺的光谱检测新技术,如开发新型增强底物或传感器,降低三聚氰胺的检测限,提高检测精度;开发更加便携的自动化光谱快检设备,降低检测成本,提高检测效率。这些光谱技术各具优势,但很难形成标准化、统一化的检测规范,使得各种光谱检测技术仅仅停留在试验阶段,无法应用于实战。另一方面,随着人工智能与模式识别技术的发展,光谱数据分析方法在近年来也有着长足的进步,各种光谱预处理和数据建模方法被不断提出,大大提高了光谱检测技术的灵敏性和稳定性。综述了近十年光谱技术（拉曼光谱、近红外光谱、荧光光谱、光谱成像等）在三聚氰胺检测中的应用现状,总结了不同仪器检测限、定量范围和样品前处理方法;分析了各种光谱预处理和光谱数据建模方法在不同光谱数据中的适用性,归纳出这些方法的优劣与适配的仪器,并对其应用前景和研究趋势进行了展望。     

用于固态功放反射式宽带预失真器设计方法

提出了一种特定增益和相位补偿的反射式宽带线性化器设计方法,并通过此方法设计了一种补偿固态功率放大器失真特性的预失真电路。利用肖特基二极管产生非线性补偿,根据电路拓扑结构,利用matlab优化工具找到单频点处特定增益补偿和相位补偿特性的并联负载值,改变频点,并重复上述步骤,可进一步得到特定增益和相位补偿所需的并联负载随频率的变化关系（即Z_L～f曲线）。利用ADS仿真软件优化设计使二极管后端阻抗随频率的变化逼近Z_L-f曲线。仿真的电路增益补偿和相位补偿分别为6 dB和?40°。最终实测频率范围为9.4～11.4 GHz,增益扩张在3.9～4.4 dB,相位补偿在?32.3°～?41.5°,频带特性良好,并且相对带宽达到了19.2%。通过改变二极管直流偏置电压,还实现了补偿曲线的斜率可调。     

1.5次微分吸附阴极溶出伏安法测定毛地黄毒苷及其电极过程的探讨

毛地黄毒苷是治疗心脏病的有效药物,它在汞电极上能吸附还原.以1.5次微分吸附阴极溶出伏安法测定检出限达3.2×10~(-10)mol/L.吸附溶出响应依赖于试液浓度、富集电位、富集时间、介质、溶液pH、温度及扫速等因素.不同富集时间,不同浓度范围内.浓度与峰高有良好的线性关系.毒苷的常规循环伏安图上出现两对氧化还原峰,电极反应相似于α,β不饱和羰基的1,2和1,4加成,电极反应可逆.毒苷在汞电极上的饱和吸附量为3.54×10~(-11)mol/cm~2.     

Behaviour of Self-Standing CVD Diamond Film with Different Dominant Crystalline Surfaces in Thermal-Iron Plate Polishing

Self-standing CVD diamond films with different dominant crystalline surfaces are polished by the thermal-iron plate polishing method. The influence of the dominant crystalline surfaces on polishing etfficiency is investigated by measuring the removal rate and final roughness. The smallest rms roughness of 0.14 μm is measured with smallest removal rate in the films with the initial （220） dominant crystalline surface. Activation energy for the polishing is analysed by the Arrhenius relation. It is found that the values are 170kJ/mol, 222kJ/mol and 214kJ/mol for the film with three different dominant crystalline surfaces. Based on these values, the polishing cause is regarded as the graphitization-controlling process. In the experiment, we find that transformation of the dominant crystalline surfaces from （111） to （220） always appears in the polishing process when we polish the （111） dominant surface.     

A RELAXATION RESULT OF FUNCTIONALS IN THE SPACE SBD（Ω）

In this article,the authors obtain an integral representation for the relaxation of the functional
F（x,u,Ω）：={∫^f（x,u（x）,εu（x））dx Ω if u∈W^1,1（Ω,R^N）, ＋∞ otherwise, in the space of functions of bounded deformation,with respect to L^1-convergence.Here Eu represents the absolutely continuous part of the symmetrized distributional derivative Eu.f（x,p,ξ）satisfying weak convexity assumption.     

Design of new seismometer based on laser Doppler effect

In order to improve the resolution of seismic acquisition,a new seismic acquisition system based on tangential laser Doppler effect with an optimized differential optical configuration is proposed.The relative movement of the inertia object and the immobile frame is measured by laser Doppler effect,which can avoid the electromagnetic and thermometric interference,and the adoption of frequency-modulated (FM) transmission can improve the ability of anti-jamming.The frequency bandwidth is properly determined by analyzing the frequency of the Doppler signal.The velocity, displacement,acceleration, and frequency to be measured can be real-time acquired by frequency/velocity (F/V) converting the FM Doppler signal. A 100-dB dynamic range and the linear frequency range of 1.0 to 1000 Hz are realized.     

12kW二极管泵浦激光模块

二极管泵浦固体激光器（DPL）具有寿命长、热负载小、结构紧凑等优点，在工业加工、军事、通讯等领域都得到了广泛的应用。在高光束质量、高平均功率DPL激光器的研究中，目前普遍采用MOPA结构的光路布局——由谐振腔产生出低功率的单横模激光输出，经多路放大后达到满足需求的功率水平。而激光放大模块作为放大光路中的核心部件，其增益分布特性将直接影响到光束放大过程中的波前变化，因此如何在提高激光放大模块储能的同时提高模块增益分布的均匀性，从而减少光路放大过程的波前畸变，对于进一步研制高平均功率、高光束质量的半导体泵浦固体激光器具有非常重要的意义。