用Re/Al2O3/Al隧道结的电子隧道测定重掺杂Re膜的超导能隙

用Re/Al₂O₃/Al隧道结的电子隧道测定了重掺杂Re膜的超导能隙,△₀=(1.04±0.02)meV,2△₀/kT_c=3.31±0.04。△₀值是用电导极大值法确定的。结果表明,杂质使Re膜的T_c与能隙△₀增加了许多倍,但是Re仍然属于弱耦合超导体。 关键词：     

FLUX CREEP, FLUX PINNING AND CRITICAL CURRENT DENSITY OF Y-, Gd-, AND Tl-BASED SUPERCONDUCTIVE THIN FILMS

Magnetic hysteresis loops have been measured for YBa₂Cu₃O_6+x, GdBa₂Cu₃O_6+x and Tl₂Ba₂Ca₂Cu₃O_10-y films at different temperatures with a vibrating sample magnetometer. Based on Bean model, magnetic critical current density J_cm has been derived approximately. The field and temperature dependence of J_cm for all samples can be written as: J_cm= J_c0(T)×f(B,T), Where f(B,T) = 1 - Aln(B/B₀(T)), which is similar to the transport critical density strongly affected by flux creep: J_ct = J_c0(B,t)(1 - (k_BT/U₀)ln(BΩd/E_c)). The extraordinary similarity suggests that J_cm is determined not only by flux pinning but also by flux creep. In the first formula, f(B,T) may be correlated with the effect of flux creep on J_cm, and J_c0(T) is determined by flux pinning. J_c0(T) is independent of magnetic field and is proportional to (T_c - T). Similar results have also been found for other samples. It may be the common characteristic of high-T_c superconductors. Magnetic relaxation of YBa₂Cu₃O_6+x and GdBa₂Cu₃O_6+x films has been measured at LN₂ temperature. Using the equation of Hagen et al., effective activation energy U₀ has been deduced, which is about 0.3eV, one order bigger than the value obtained by A = k_BT/U₀. U₀ is almost independent of the field in the field range selected.     

庐山石韦中总黄酮的提取工艺研究

优选庐山石韦中总黄酮类化合物的提取工艺.以芦丁为对照品,就微波提取法、碱提酸析法、丙酮提取法、乙醇提取法对庐山石韦中总黄酮类化合物的提取效果进行了比较,并采用正交试验,以提取物中总黄酮得率为指标进行试验.优选出庐山石韦中总黄酮类化合物的最佳提取工艺为20倍量的55%乙醇溶液在80℃条件下浸提5 h.总黄酮的得率为5.91%.该提取工艺可行.提取率高.     

介质谐振器法测量高温超导薄膜微波表面电阻的误差分析

用微扰法研究了两端接地型蓝宝石介质谐振器测量高温超导薄膜微波表面电阻R_S的误差与几何结构和工作频率的关系.结果表明,介质柱直径与高度之比2a/L,金属屏蔽腔内半径与介质柱半径之比b/a以及工作频率f对测量误差和最小可测表面电阻R_smin有很大影响.所得到的曲线可用于蓝宝石介质谐振器的设计中.结果还表明,适当选取2a/L,b/a与f可使测量误差接近于1%,最小可测表面电阻R_smin可达到微欧姆的数量级.这对于高温超导薄膜的检测和微波器件应用说 关键词： 介质谐振器 高温超导薄膜 微波表面电阻 误差分析     

PrBa2Cu3O6+x(x=1,0.3)中Pr价态随氧含量的变化

报道了陶瓷和c轴取向薄膜 PrBa₂Cu₃O_6+x(x=1,0.3)材料的红外反射光谱，通过比较区分出该材料的沿着c轴振动和沿着a-b平面振动的声子模，PrBa₂Cu₃O_6+x和RBa₂Cu₃O_6+x(x=1-0,R=Y和稀土元素)有类似的晶体结构，分析和比较它们的声子谱，其中尤其是Pr和Y,Pr和其它稀土元素 关键词：     

高温超导膜微波表面电阻Rs对微波滤波器插入损耗的贡献

利用微波电路仿真软件，分析高温超导膜微波表面电阻Rs对各种频率、各种级数的滤波器插入损耗的影响.结果给出:对于级数较少、频率较低的滤波器，使用Rs较高的薄膜或厚膜就可以得到很低的插入损耗;对于频率较高(高于6GHz),或极数较多（超过8极）的滤波器，就必须采用高质量的高温超导薄膜（Rs<1mΩ）. 关键词： 高温超导膜 微波滤波器 微波表面电阻 插入损耗     

庐山石韦叶中多糖提取初探

用蒸馏水、10 g/L氢氧化钠、1%三氯乙酸分别从庐山石韦叶中提取多糖.通过苯酚-硫酸法进行多糖含量测定并比较它们的多糖得率.结果表明10g/L氢氧化钠的提取效果比蒸馏水和1%三氯乙酸的提取好.     

Ba_xY_(1-x)CuO_(3-y)系列的高Tc超导电性

本文研究了钡-钇-铜氧化物的高Tc超导电性,其名义组份为Ba_xY_(1-x)CuO_(3-y)(0.05≤x≤0.95)。结果表明,x<0.50时,超导转变温度TC_(1/2)随组份x单调上升;在较宽的组份范围0.60相似文献