共查询到18条相似文献,搜索用时 734 毫秒
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在核四极矩共振(NQR)领域,射频激励脉冲信号的优劣对NQR响应信号有重要影响.针对常规方法中射频激励脉冲参数不可控的问题,本文基于32位闪存微型控制器STM32和直接数字频率合成(DDS)芯片AD9910设计了一种相位可控激励脉冲发生器.采用STM32控制AD9910产生波形参数(脉冲宽度、脉冲间隔、脉冲个数和共振频率等)可控的射频激励脉冲,利用LabVIEW软件平台设计脉冲参数设置界面,并建立计算机与微控制器通信,实现波形参数的精确优化控制.实验结果表明,该方法实现了相位可控的NQR激励脉冲序列,可为后续NQR信号检测提供有效激励源. 相似文献
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一、前言自1950年德国哥廷根大学的Dehmelt和Kr(?)ger发现~(35)Cl、~(37)Cl的核四极共振信号,到现在已37年.由于核四极共振信号比核磁共振信号弱得多,实验上灵敏度很低,对于生物学上很有意义的~(14)N、~2D、~(17)O等无法检测,使得核四极共振的理论和技术的发展停滞不前.但近年来“核磁——核四极”双 相似文献
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氮-14远程核四极共振谱仪 总被引:1,自引:0,他引:1
为了满足检测与探头有一定距离的含氮化合物的核四极共振信号,本文研制了一台结构简单,造价低廉的核四极共振操测仪.它利用了脉冲付里叶变换技术,可将获得的核自由感应衰减信号或者回波信号进行相干累加.整个系统分硬件和软件两大部分.前者由射频脉冲放大器(约500W脉冲输出功率),探头,接收机,MCS-96型单片机和PC机构成.后者由单片机上的脉冲序列程序与PC机上的数值信号处理程序组成.利用这台谱仪,可以在几十秒时间内得到距离探头线圈10cm内的典型 ̄(14)N样品的核四极共振谱. 相似文献
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氮-14远程核四极共振谱仪 总被引:1,自引:1,他引:0
为了满足检测与探头有一定距离的含氮化合物的核四极共振信号,本文研制了一台结构简单,造价低廉的核四极共振操测仪.它利用了脉冲付里叶变换技术,可将获得的核自由感应衰减信号或者回波信号进行相干累加.整个系统分硬件和软件两大部分.前者由射频脉冲放大器(约500W脉冲输出功率),探头,接收机,MCS-96型单片机和PC机构成.后者由单片机上的脉冲序列程序与PC机上的数值信号处理程序组成.利用这台谱仪,可以在几十秒时间内得到距离探头线圈10cm内的典型14 N样品的核四极共振谱. 相似文献
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D. Ya. Osokin R. R. Khusnutdinov G. V. Mozzhukhin B. Z. Rameev 《Technical Physics》2014,59(5):749-753
The application of the multipulse sequences in nuclear quadrupole resonance (NQR) detection of explosive and narcotic substances has been studied. Various approaches to increase the signal to noise ratio (SNR) of signal detection are considered. We discussed two modifications of the phase-alternated multiple-pulse sequence (PAMS): the 180° pulse sequence with a preparatory pulse and the 90° pulse sequence. The advantages of optimal filtering to detect NQR in the case of the coherent steady-state precession have been analyzed. It has been shown that this technique is effective in filtering high-frequency and low-frequency noise and increasing the reliability of NQR detection. Our analysis also shows the PAMS with 180° pulses is more effective than PSL sequence from point of view of the application of optimal filtering procedure to the steady-state NQR signal. 相似文献
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J L Schiano T Routhier A J Blauch M D Ginsberg 《Journal of magnetic resonance (San Diego, Calif. : 1997)》1999,140(1):84-90
A method for increasing the signal-to-noise ratio (SNR) of nuclear quadrupole resonance (NQR) measurements by automatically adjusting a pulse parameter in real-time is presented. This approach is useful in situations where the optimal pulse parameters cannot be chosen beforehand due to lack of knowledge regarding the system. For example, NQR provides a means for detecting explosives by revealing the presence of (14)N. In this particular application, the distance between the search coil and the explosive, as well as the temperature of the explosive, is unknown. As a result, a fixed set of pulse parameters will not yield the largest SNR for all possible search applications. This paper describes a feedback algorithm that uses measurements of the NQR signal to automatically adjust the pulse width in the strong off-resonant comb sequence to maximize the SNR of the NQR measurement. Experimental results obtained using a sample of sodium nitrite are presented. 相似文献
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Three-Frequency Composite Multipulse Nuclear Quadrupole Resonance Technique for Explosive Detection 总被引:1,自引:0,他引:1
G. V. Mozzhukhin B. Z. Rameev R. R. Khusnutdinov N. Do?an B. Aktas 《Applied magnetic resonance》2012,43(4):547-556
New method of multifrequency nuclear quadrupole resonance (NQR) for the explosive detection has been proposed. This technique consists of application of the series of composite excitation circles, each consisting of two or three successive pulses of different frequencies. In this work, we study in detail the multipulse sequence consisting of n excitation sets, each set consists of three pulses. The first pulse is applied with frequency ?? ?, the second pulse with frequency ?? 0, and the third pulse with frequency ?? ?C, but with a shifted phase. The NQR signal is detected at the frequency ?? +. The maximal amplitude of the detected signal is obtained by tuning the pulse parameters at frequencies ?? ? and ?? 0. We have shown that the phase of the NQR signal at the frequency ?? + second part of the composite pulse with the frequency ?? 0 the signals with different phases to suppress the spurious signals. The method could be used for increasing the NQR signal, avoiding the spurious signals and improving the reliability of NQR detection. Possible applications of the method for the explosive detection are also discussed. 相似文献
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介绍了基于核四极矩技术的爆炸物检测原理及信号处理方法.系统分析了NQR信号检测中主要误差来源,提出多种方法消除NQR信号处理中检测误差,主要包括相关累加消除随机噪声;单通道自适应消除振铃影响;相关性检测抑制同频干扰.实验表明相关检测可有效提高NQR信号信噪比,提高微弱NQR信号检测的准确性. 相似文献
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This paper presents first experiments on using Zeeman polarization-enhanced nuclear quadrupole resonance (NQR) method in detecting explosive substance pentaerythritoltetranitrate (PETN). The NQR signals were detected on nitrogen nuclei at room temperature using a multi-pulse spin-locking sequence after the sample was kept in a very inhomogeneous magnetic field. The dependence of enhancement factor on the time of protons polarization in the magnetic field was studied. 相似文献
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The angular dependence of the nuclear quadrupole resonance (NQR) signal intensity emitted from polycrystalline hexamethylenetetramine has been analytically investigated for all directions for non-contact detection of chemicals by nuclear quadrupole resonance. The field pattern of the NQR signal from a column sample was measured. The emitted patterns were the same as that from a united single magnetic dipole, which fitted well to the estimation based on quadrupole principle axis system. This result is helpful to design an antenna for NQR remote detection. 相似文献