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排序方式: 共有756条查询结果,搜索用时 15 毫秒
1.
YuchengWu YongZhang LideZhang 《中国颗粒学报》2004,2(1):19-24
Nanosized palladium particles were incorporated into mesoporous silica matrix to obtain nanocomposites using the sol-gel technique. Effects of the finely dispersed metallic palladium on the microstructure and properties of the nanocomposites were investigated. By means of X-ray diffraction and optical absorption, it was found that palladium particles were 5-9 nm in diameter and their uniform dispersion in the mesoporous silica depended on both the content of the palladium and the structural features of the silica matrix. The results showed that the mixing method of preparation led to wider size distribution of the nanosized particles as compared to the immersion method, but dispersed degree was reduced. Although the incorporation of nanosized palladium particles could not substantially induce significant structural changes of the matrix, the apparent red-shifted optical absorptions for the nanocomposites were observed as compared to the parent monolithic silica, particularly with increase in palladium loading and calcination temperature. 相似文献
2.
JIA HongSheng JIA XiaoPeng XU Yue WAN LianRu JIE KaiKai & MA HongAn State Key Laboratory of Superhard Materials Jilin University Changchun China Test Science Experiment Center Changchun 《中国科学:物理学 力学 天文学(英文版)》2011,(1)
Polycrystalline diamond compacts (PDC) were synthesized using diamond powder of average crystal size 3-20 μm by the Ni 70 Mn 25 Co 5 alloy infiltration technique at high temperature and high pressure (HPHT).The surface residual stress of polycrystalline diamond (PCD) layer was measured using micro-Raman spectroscopy with hydrostatic stress model and X-ray diffraction (XRD).Measurements of the stress levels of PCDs show that the residual compressive stresses range from 0.12 to 0.22 GPa,which increase with th... 相似文献
3.
YANG YuJuan & YAN Biao School of Materials Science Engineering Tongji University Shanghai China Shanghai Key Lab of Development Application for Metal Functional Materials 《中国科学:物理学 力学 天文学(英文版)》2011,(5)
With the multi-phase field model, the unidirectional solidification with constant velocity growth and variable velocity growth of the CBr4-C2Cl6 eutectic alloy is simulated in three dimensions. The simulated results with constant velocity growth show that with the increase of pulling velocity, the morphology of the CBr4-C2Cl6 alloy evolves in the sequence of lamellar merging →lamellar-rod transition→stable lamellar growth→oscillating growth→lamellar branching. A morphology selection map is established with ... 相似文献
4.
ZHAO ChunRan & YE Liu School of Physics & Materials Science Anhui University Hefei China School of Physics & Electronic Information Huaibei Normal University Huaibei 《中国科学:物理学 力学 天文学(英文版)》2011,(3)
A scheme is proposed for generating a multiphoton entangled cluster state among four modes. The scheme only uses Kerr medium, beam splitter and homodyne measurements on coherent light fields, which can be efficiently made in quantum optical laboratories. The photon in the signal mode is prepared in a superposition state of the vacuum state and one-photon state while the probe beam is initially set in a coherent state superposition. The strong probe mode interacts successively with multiple signal-mode photo... 相似文献
5.
Aperiodic molybdenum/silicon (Mo/Si) multilayer designed as a broadband reflective mirror with mean reflectivity of 10% over a wide wavelength range of 12.5-28.5 nm at incidence angle of 5° is developed using a numerical optimized method. The multilayer is prepared using direct current magnetron sputtering technology. The reflectivity is measured using synchrotron radiation. The measured mean reflectivity is 7.0% in the design wavelength range of 12.5-28.5 nm. This multilayer broadband reflective mirror can be used in extreme ultraviolet measurements and will greatly simplify the experimental arrangements. 相似文献
6.
The accumulation effects in high-reflectivity(HR) HfO2/SiO2 coatings under laser irradiation are investigated.The HR HfO2/SiO2 coatings are prepared by electron beam evaporation at 1 064 nm.The laser-induced damage threshold(LIDT) are measured at 1 064 nm and at a pulse duration of 12 ns,in 1-on-1 and S-on-1 modes.Multi-shot LIDT is lower than single-shot LIDT.The laser-induced and native defects play an important role in the multi-shot mode.A correlative theory model based on critical conduction band electron density is constructed to elucidate the experimental phenomena. 相似文献
7.
Yucheng Du a Shuli Shi a Hong He b Hongxing Dai b a Key Laboratory of Advanced Functional Materials Ministry of Education Beijing University of Technology Beijing China b 《中国颗粒学报》2011,9(1)
Nanorod-like Ce 0.7 Zr 0.3 O 2 solid solutions were synthesized by a sodium dodecyl sulfate-assisted precipi- tation method. The samples were characterized by means of scanning electron microscopy, transmission electron microscopy, X-ray diffraction, Fourier transform infrared spectroscopy, and specific surface area measurement. Typical Ce 0.7 Zr 0.3 O 2 nanorods were 40 nm in average diameter and 450 nm in length, with specific surface area and oxygen storage capacity of 194 m 2 /g and 374 mol/g, respectiv... 相似文献
8.
9.
YBa2Fe3O8(YBFO)是具有三方钙钛矿结构的反铁磁(AFM)体,研究它的结构和磁性质对于我们认识三方钙钛矿结构具有重要作用.目前,关于固相法制备YBFO中退火温度方面的研究并不多,而控制退火温度是这种工艺中的重要环节.为制备高含量的YBa2Fe3O8,本文分别在760℃、950℃和1100℃退火温度下,采用固相... 相似文献
10.
用溶胶-凝胶(so-lgel)法制备了多铁Bi1-xLaxMnO3(BLMO,0.1≤x≤0.4)系列样品.样品的结构表征(X-射线衍射,扫描电子显微镜)及差热-热重(TG-DTA)分析测量显示,形成稳定的BLMO钙钛矿相的烧结温度位于900~950℃.La掺杂对BLMO样品(950℃烧结)的结构和磁性能的影响也被仔细研究.结果显示,随着La掺杂减少,样品中BLMO钙钛矿相减弱,铁磁转变温度(TC)由53K降至41K,而饱和磁化强度经历了先降低再升高的变化.这可归因于La含量较少的样品中Bi空位浓度的增加诱导了Mn-O-Mn键角的减小和局域Mn4+离子的增多,使得Mn3+和Mn4+离子的铁磁超交换增强和Mn3+离子的dz2轨道有序受到局域破坏. 相似文献