关于开设内光电效应实验的探索与思考

介绍了开设以内光电效应为理论基础的半导体光电器件的重要性和迫切性,并详细介绍了内光电效应的理论与半导体光电器件的分类和应用前景。     

非晶硅太阳电池的光伏检测磁共振研究

本文利用光伏检测磁共振(PDMR)方法初步研究了p⁺in⁺ a-Si:H太阳电池中与自旋状态有关的复合机制。研究表明太阳电池的制作工艺不同,相应的PDMR共振信号的线型和g因子亦不同,因而起支配作用的复合过程不同。根据PDMR结果讨论了a-Si:H膜的生长速度、衬底温度、本征层厚度等对太阳电池性能的影响。 关键词：     

怀菊花中微量铁的测定

为探讨邻二氮菲分光光度法测定怀菊花中微量元素铁含量的可行性,怀菊花的药理功效、食用营养价值与微量元素含量可能存在的关系,根据铁离子与特定显色剂显色产生可见吸收,采用混合酸y（HNO3）：V（HClO4）=4＋1对怀菊花样品湿法消化处理,在pH2～9的溶液中试剂与铁生成稳定的橙色络合物,并用分光光度法测定了怀菊花中微量元素铁含量。结果表明,所选的怀菊花中铁含量303．9～337．9μg／g,加标回收率为90．2％～100．6％。分光光度法操作简便、干扰离子少,测量快速、结果准确度和灵敏度高,易推广和 普及使用。     

关于强Armendariz环和强拟Armendariz环

提出了强拟Armendariz环的概念,给出了强Armendariz环和强拟Armendariz环上的一些结果.     

旋流燃烧器复合小火焰模型的大涡模拟

对低旋燃烧器内的流动和燃烧进行了大涡模拟,其中化学反应分别采用传统的扩散小火焰模型和所提出的复合小火焰模型描述。复合小火焰模型借助于燃烧区索引的概念区分当地的燃烧模式,若当地的燃烧为扩散燃烧,则调用扩散小火焰库,否则调用预混小火焰库。数值结果与实验数据的对比表明,采用大涡模拟方法结合小火焰模型能够很好地模拟实验室尺度的低旋燃烧器,且采用复合小火焰模型能够得到更加符合实际的结果。     

丝瓜中维生素C含量的测定

为建立丝瓜中维生素C含量直接测定的新方法,以10%盐酸溶液为溶剂,采用紫外分光光度法测定其含量。结果表明,维生素C在0～10 mg/L质量浓度范围内与吸光度呈良好的线性关系,回归方程为:y=0.047 46ρ+0.001 09,r=0.999 7。检出限为0.023μg/mL,加标回收率在90.6%～99.0%之间。该法操作简单,结果准确,应用于维生素C含量的测定,结果准确,令人满意,可作为控制维生素C质量的方法。     

FC-空间中新的连续选择定理及其对广义模糊约束多目标对策的应用

建立了非紧FC-空间中新的连续选择定理,作为应用,获得了非紧FC-空间中广义模糊约束多目标对策的弱Pareto平衡存在定理.我们的结论统一、改进和推广了一些近期文献的已知结果.     

Phytochemical characterisation of Phlomis linearis Boiss. & Bal and screening for anticholinesterase,antiamylase, antimicrobial,and cytotoxic properties

In the present work, essential oil and fatty acids and extracts obtained from aerial parts of Phlomis linearis Boiss. & Bal. were investigated for chemical composition and biological activities. The phytochemical analyses were conducted with gas chromatography-mass spectrometry/flame ionisation detector (GC-MS/FID) and liquid chromatography-mass spectromtetry (LC-MS/MS) techniques. The extracts and essential oil were studied for α-amylase and acetylcholinesterase activities with two different spectrophotometric methods. Antimicrobial activities of the extracts were investigated by microdilution. The extracts were evaluated in vitro for cytotoxic effects against cancer and normal cell lines by MTT assay. The essential oil (EO) contained α-pinene (12.5%) and β-caryophyllene (10.7%) as main compounds. Palmitic (26.5%) and nonadecanoic acids (26.6%) were determined as fatty acids. Phytochemical analysis of the extracts found phenolic acids, phlinosides, verbascoside, and flavonoids. The extracts and essential oil demonstrated poor α-amylase inhibitory activity. The best acetylcholinesterase inhibitory activity was obtained for diethly ether extract of P. linearis (67.2 ± 3.4%) at 10 mg /mL concentration. Ethyl acetate extract found to be effective against Staphlococcus aureus at a minimum inhibitory concentration (MIC) of 156.26 µg/mL. Diethyl ether extract of P. linearis was active on A549 cell lines with an IC₅₀ = 316 ± 4.16 µg/mL when compared with cisplatin IC₅₀ = 24.43 ± 0.14 µg/mL. To the best of our knowledge, the present work is the first comprehensive report on anti-acetylcholinesterase, anti-α-amylase, and antimicrobial activities, as well as cytotoxic effects of P. linearis.     

怀菊花总黄酮的提取工艺及其抗氧化活性

以新鲜怀菊花为原料,用芦丁为对照品,硝酸铝作为显色剂,正交设计优化怀菊花中总黄酮提取条件,采用超声波和水浴提取法等2种工艺提取怀菊花中总黄酮,研究单因素对总黄酮提取率的影响,确定提取总黄酮的最佳条件,同时用碘量法研究对猪油的抗氧化性作用.水浴提取怀菊花总黄酮以A1B1C3组合为最佳提取条件,提取率为109.74mg/g.超声波提取怀菊花总黄酮以A2B2C2组合为最佳提取条件,提取率为114.47mg/g.实验结果表明,超声波法提取效果优于水浴提取法,怀菊花黄酮对猪油有一定的抗氧化能力.