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To improve the performance of Beamline 3W1B at the Beijing Synchrotron Radiation Facility for the soft X-ray magnetic linear dichroism research at transition metals L2, 3 edges, a new monochromator was designed and built to replace the original one. After the assemblage, alignment and adjustment of the monochromator system, the first commissioning results were obtained. The photon energy range is from 50 to 1000 eV with spectral resolutions of 1600 at 250 eV and 1000 at 870 eV. The photon flux is of the order of 108-109 photons/s/200 mA/0.1%BW. In the electron's orbital plane the linear polarization degree of the light is higher than 99% at 704 eV. The beamline has satisfied the basic experimental requirements.  相似文献   
2.
Ca-based additives have been widely used as a sulfur adsorbent during coal pyrolysis and gasification. The Ca speciation and evolution during the pyrolysis of coal with Ca additives have attracted great attention. In this paper, Ca species in the coal chars prepared from the pyrolysis of Ca(OH)2 or CaCO3-added coals are studied by using Ca K-edge X-ray absorption near-edge structural spectroscopy. The results demonstrate that Ca(OH)2 , CaSO4 , CaS and CaO coexist in the Ca(OH)2-added chars, while Ca(OH)2 and CaSO4 are the main species in the Ca(OH)2-added chars. Besides, a carboxyl-bound Ca is also formed during both the pyrolysis for the Ca(OH)2-added and the CaCO3-added coals. A detailed discussion about the Ca speciation is given.  相似文献   
3.
Conventionally, the polarization of a synchrotron soft X-ray beam is measured through a polarimeter based on multilayer optical elements. The major drawback of the traditional approach is the difficulty in comparing different configurations due to the misalignment of each incident angle. In this paper, a new analytical model, based on the variation of reflectivity for different incident angles, is established to facilitate the extraction of important polarization-related information, i.e. angular distribution of polarization components, a tiny change of the direction of azimuth rotation axis of polarizer, etc.  相似文献   
4.
Three ultra-short-period W/B4C multilayers (1.244 nm, 1.235 nm and 1.034 nm) have been fabricated and used for polarization measurement at the 4B7B Beamline at the Beijing Synchrotron Radiation Facility (BSRF). By using the rotating analyzer ellipsometry method, the linear polarization degree of light emerging from this beamline has been measured and the circular polarization evaluated for 700-860 eV. The first soft X-ray magnetic circular dichroism measurements are carried out at BSRF by positioning the beamline aperture out of the plane of the electron storage ring.  相似文献   
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王得来  崔明启  杨栋亮  董俊才  徐伟 《中国物理 B》2016,25(10):107501-107501
In this work, the magnetocrystalline anisotropy energy(MAE) on the surface of Fe_(33)Co_(67) alloy film is extracted from x-ray magnetic linear dichroism(XMLD) experiments. The result indicates that the surface MAE value is negatively correlated with thickness. Through spectrum calculations and analysis, we find that besides the thickness effect, another principal possible cause may be the shape anisotropy resulting from the presence of interface roughness. These two factors lead to different electron structures on the fermi surface with different exchange fields, which produces different spin–orbit interaction anisotropies.  相似文献   
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