利用玻纤厂烟气脱氟副产物合成莫来石晶须

以氢氧化铝和二氧化硅为莫来石前驱体,玻纤厂烟气脱氟副产物作为助剂合成莫来石晶须。采用了X射线衍射仪(XRD)和扫描电镜(SEM)研究了热处理温度和助剂含量等对莫来石晶须合成的影响。结果表明助剂的加入对莫来石的合成有显著的促进作用,当助剂添加量为5wt%时,莫来石化的开始和完成温度和文献报道相比分别降低了约100℃和300℃,并且莫来石晶粒为晶须形貌。助剂含量为5wt%的样品在1400℃热处理两小时制备的莫来石晶须的长径比可达20。     

A new approach for dynamic modeling of widely tunable GCSR lasers

A new dynamic model is developed for simulating the widely tunable grating assisted codirectional coupler with rear sampled grating reflector （GCSR） lasers. The gain section of the device is calculated in timedomain using traveling-wave method, while the transmission spectrum of the coupler and the reflection spectrum of the reflector are firstly simulated in frequency-domain, and then transformed into time-domain via digital filter approach. Both static and dynamic performances based on this model agree well with the published results. Compared with previous works, this new model is more efficient and applicable, especially in the dynamic simulation.     

弹性地基上含孔隙功能梯度材料板的自由振动和动力响应

为研究弹性地基上含孔隙的材料特性沿厚度呈Sigmoid函数变化的功能梯度材料(S-FGM)板的振动特性,本文基于改进的Voigt模型,分别建立了孔隙为均匀分布和非均匀分布两种类型的功能梯度材料的物性参数模型。根据复合材料薄板理论导出了弹性地基上含孔隙的功能梯度材料板的运动方程,用伽辽金法寻求四边简支边界条件下板自由振动和动力响应的解析解;讨论了孔隙、弹性地基参数、材料组分指数等因素对S-FGM板自由振动和动力响应的影响。结果表明:孔隙对板自振频率的影响比较复杂,不仅与孔隙率的大小和分布形式有关,还与弹性地基参数有关;当有弹性地基作用时,板的量纲归一化基频随着孔隙率的增大而提高,并且孔隙均匀分布的S-FGM板与孔隙非均匀分布的情况相比,其量纲归一化基频更高;孔隙增大了板的动力响应,其中孔隙为均匀分布的板的动力响应对孔隙率的变化更为敏感。     

利用无机胶凝材料制备莫来石多孔陶瓷

本文利用无机胶凝材料成功制备了莫来石多孔陶瓷.以硅藻土和ρ-Al2O3为原料,AlF3和MoO3为添加剂,利用ρ-Al2O3遇水硬化的特点,来实现陶瓷浆料的固化成型,再将成型后的陶瓷生坯经高温烧结得到莫来石多孔陶瓷.该方法绿色环保,整个制备过程中无有机物的排放.通过使用XRD、SEM等表征测试手段,研究了烧结温度对莫来石多孔陶瓷的相组成、微观形貌、线收缩率、开孔孔隙率以及抗压强度的影响.实验结果表明,制备的莫来石多孔陶瓷由生长良好的莫来石晶须构成,在1500℃下烧结的莫来石多孔陶瓷孔隙率可达到82.3;.     

快速老化模型小鼠海马蛋白质组学初步研究

应用双向凝胶电泳结合质谱鉴定, 分析比较6月龄和12月龄快速老化模型小鼠(Senescence-accele-rated mouse, SAM)的快速老化亚系SAM-prone/8(SAMP8)及抗快速老化亚系SAM-resistance/1(SAMR1)海马蛋白表达的差异, 从蛋白质水平初步探讨与老化相关的学习记忆功能障碍的发生机制. 结果表明, 与同龄SAMR1比较, 6月龄SAMP8海马中有15个蛋白点表达显著上调, 5个蛋白点表达显著下调; 12月龄SAMP8海马中有12个蛋白点表达显著上调, 2个蛋白点表达显著下调, 2个蛋白点只在SAMP8中有表达. 应用质谱分析结合数据库检索, 共鉴定了22种蛋白质. 6月龄和12月龄SAMP8与SAMR1海马中表达有明显变化的蛋白按功能可分为如下4类: (1) 能量代谢相关蛋白; (2) 线粒体功能相关蛋白; (3) 信号转导相关蛋白; (4) 其它蛋白. 研究结果表明, SAMP8和SAMR1海马蛋白表达存在明显差异, 其中一些蛋白与SAMP8随龄出现的学习记忆功能减退相关, 并可能为研究或发现促智药物作用的新蛋白靶标提供线索.     

流量与环量对低扬程泵装置流道水头损失的交叉影响

流道水头损失与流量及环量之间的关系,是低扬程泵装置水力设计理论中对提高其水力性能的研究具有较大影响的重要问题.低扬程泵装置水泵导叶出口水流所具有的速度环量使上述关系变得复杂起来,需全面认识.研究结果表明:在无环量的条件下,进、出水流道水头损失与流量平方成正比;在Reynolds数达到阻力平方区要求的条件下,在一定转速范围内,对于不同转速下运行时的相似工况,流道水头损失与流量平方成正比,表现为泵装置效率保持不变;低扬程泵装置中设计流量时的出水流道水头损失决定于导叶出口水流的速度环量,两者之间的关系为一开口向上的曲线,存在最优环量;在低扬程泵装置变工况运行的条件下,出水流道水头损失受流量和环量的交叉影响,在水泵正常运行工况范围内,流道水头损失与流量之间呈现出接近于线性的关系,其机理有待进一步深入研究.     

毛樱桃叶片挥发油成分GC-MS分析

采用GC—MS技术,分析了毛樱桃叶片中的挥发性成分．气相色谱共检测出163个峰,经与质谱标准图谱比较,鉴定了其中15种化学成分,其中含量较高的为棕榈酸酐、12E-11-甲基乙酸十四烯酯和十四酸甲基乙酯（相对百分含量分别为25．104％,4．873％和2．811％）．     

Flow patterns and boundary conditions for inlet and outlet conduits of large pump system with low head

The flow patterns in the inlet and outlet conduits have a decisive effect on the safe, stable, and highly efficient operation of the pump in a large pumping station with low head. The numerical simulation of three-dimensional （3D） turbulence flow in conduits is an important method to study the hydraulic performance and conduct an optimum hydraulic design for the conduits. With the analyses of the flow patterns in the inlet and outlet conduits, the boundary conditions of the numerical simulation for them can be determined. The main obtained conclusions are as follows： （i） Under normal operation conditions, there is essentially no pre-swirl flow at the impeller chamber inlet of an axial-flow pump system, based on which the boundary condition at the inlet conduit may be defined. （ii） The circulation at the guide vane outlet of an axial-flow pump system has a great effect on the hydraulic performance of the outlet conduit, and there is optimum circulation for the performance. Therefore, it is strongly suggested to design the guide vane according to the optimum circulation. （iii） The residual circulation at the guide vane outlet needs to be considered for the inlet boundary condition of the outlet conduit, and the value of the circulation may be measured in a specially designed test model.     

Cross influence of discharge and circulation on head loss of conduit of pump system with low head

The relationship between the head loss and the discharge and circulation of the conduit of a pump system with low head is an important problem with an obvious influence on the improvement of its hydraulic performance. The velocity circulation from the pump guide vane makes the relationship more complicated, which has to be understood comprehensively. The results indicate that, under the condition of zero circulation, the head loss of the inlet and outlet conduits is in proportion to the square of discharge. Under the condition that the Reynolds number is satisfied with the resistant square area, the conduit loss is in proportion to the square of discharge for the similar working points with different speeds in a certain rotational speed range, indicating that the pump system efficiency is constant. The outlet conduit loss of design discharge for a pump system with low head depends on the velocity circulation from the guide vane exit, and the relationship between the loss and the circulation is an open curve with an upward direction, meaning that there is an optimal circulation for the loss. Under the condition of various working points for a pump system with low head, the head loss of the outlet conduit is under the cross influence of both the discharge and the circulation. As a result, the relationship between the head loss and the discharge is almost linear, and the mechanism needs to be further studied.