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Chinese Journal of Polymer Science - The emerging chemical recyclable polymers, such as poly(γ-butyrolactone) (PGBL) and poly((R)-3,4-trans six-membered ring-fused GBL) (P((R)-M)), provide a... 相似文献
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为弥补标准检测方法的不足,建立了石墨消解-ICP-MS法同时检测铜精矿中Pb、Cd、As 和Hg等4种有害元素。确定了样品前处理和仪器分析条件。用铜精矿标准样品和参考样品分别进行7次重复实验,Pb、Cd和As的检测结果均在标准值范围内,Hg的检测结果与参考值基本一致。7次重复检测结果的变异系数符合GB/T 27417-2017《合格评定 化学分析方法确认和验证指南》要求。选择5种不同物相铜精矿作为待测样品,通过与标准方法比对,两种方法检测结果的绝对差符合标准方法的再现性要求,说明本方法适用于不同种类的铜精矿。本方法操作简单,可同时测定多种有害元素,实用性强。 相似文献
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采用浸渍-提拉法制备了一系列石墨烯氧化物(GO)薄膜,并通过X射线衍射(XRD),扫描电镜(SEM),傅里叶变换红外光谱,紫外-可见吸收光谱和光电化学测量等技术对样品进行了表征.在GO电极上观察到阴极光电流,且光电流密度受薄膜的厚度影响.GO薄膜电极厚度为27nm时,光电流密度为0.25μA·cm-2.此外,GO电极的光电响应还受紫外光照影响,随着紫外光照时间的延长,阴极光电流逐渐减小.该工作提供了简便的通过控制薄膜厚度或紫外光照时间来控制GO薄膜半导体光电化学性能的方法. 相似文献
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Determination of Thickness of an Inaccessible Thin Film under a Multilayered System from Natural Frequencies 下载免费PDF全文
We investigate the relationship between natural frequencies of a multilayered system of different elastic materials and the thickness of the undermost thin film. The natural frequencies are numerically calculated from the reflection coefficient of a sample system of "steel-epoxy resin-aluminium-thin polymer" with normal incidence. Strain energy ratio is defined and calculated to give the physics explanation why some frequencies are sensitive to thickness of the thin film in certain range. Experiments of three specimens indicate that the measured natural frequencies agree well with the theoretical ones. It is found in our experiments that the ratio of the lowest film thickness to wavelength is about 1/5. The average relative errors for the inverted polymer film thicknesses are found to be 11.8%, -4.8% and -1.3%, respectively. 相似文献
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检测声学是以声波作为载体,采集信息,在不损坏被检对象的情况下,探测其内部的缺陷或目标,测量其物理和力学性质,分析其组织结构作媒质的质量评价等.它是工业上的医生,资源勘探的侦察兵,探索物质结构的利器.声学检测涉及到几乎所有各个工业部门,已成为这些部门中为保证质量、保证安全、保证效益的一种不可缺少的技术.作为一门专业技术,它所涉及部门之广,领域之深,对工业发展和国防建设影响之大,不可代替作用之独特,是一般的其它专业技术无法与之比拟的.这样一个重要的学科和技术,在我国经济高速发展中,检测声学学科和声学检测技术应该是大发展的有利时机. 相似文献
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Morphology Control of SrCO3 Crystals using Complexons as Modifiers in the Ethanol-water mixtures 总被引:1,自引:0,他引:1
ZHAGN Ming-Xuana HUO Ji-Chuana② YU Yong-Shengb CUI Cai-Pinga LEI Yong-Lina a 《结构化学》2008,27(10):1223-1229
Using SrC12-6H2O and Na2CO3 as the main raw materials and adding different complexons as modifiers with simple co-precipitation method, SrCO3 crystals with distinct morphologies like spherical, bundle-like, overlapping plate-like, hexagonal star-like, dumbbell-like, etc. can be synthesized in the ethanol-water mixtures. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infrared spectrograph (FT-IR). The interrelated effect mechanism is presented in the end. Results show that the modifier carboxyl groups play a significant role in controlling the SrCO3 crystal morphologies, which can alter the crystal growth unit (Sr^2+) supply mode and induce the crystal formation with the morphologies matching their spatial configurations. 相似文献
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Synthesis of the glycolurils catalyzed by potassium hydroxide was carried out in 17–75% yield at 40 °C in EtOH under ultrasound irradiation. Compared to the method using stirring, the main advantage of the present procedure is milder conditions and shorter reaction time. 相似文献
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The propagation of a longitudinal ultrasonic wave normally incident upon an adhesively bonded structure is studied. The structure consists of adherend and adhesive layers with finite thickness. Interfaces between adherend and adhesive are regarded as distributed springs. Theoretical and experimental results show that resonant frequencies of the bonded structure vary sensitively with the interface stiffness constants and adhesive thickness, and these interface characteristics are inversed by the simulation annealing (SA) method. Furthermore, the distribution image of interface stiffnesses is compared with the state of fracture interface, and quantitative prediction of shear strength is achieved based on the distribution of interface stiffnesses and adhesive thicknesses by using a back-propagation neutral network. The average relative error of the shear strength from prediction to real value is 10.7%. 相似文献