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P-350萃取色层分离测定岩石中痕量镓和铟 总被引:1,自引:0,他引:1
萃取色层分离法目前已成为岩矿测试工作者研究痕量元素之间分离的重要手段,本文研究了在氢溴酸体系中P—350萃取色层连续分离镓、铟的行为。试验结果证明,以聚二乙烯苯为载体,P—350为固定相,5.5mol/L H_2SO_4为解脱剂相继解脱镓和铟,不仅分离效率高,操作简便,而且具有良好的选择性。经分离后的Ga和In用丁基罗丹明B光度法测定,准确可靠,并 相似文献
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1.本单元知识点串讲1)夹角与距离.空间角和距离是立体几何中的两个重要概念,它们是空间图形位置关系的具体体现,是对空间图形位置关系进行定量分析的两大量化指标.它们的主要求解方法有“构造法”和“向量法”.2)空间向量.向量方法是一种重要的数学方法,它在处理立体几何问题时,更能显示出它的优越性,而且高考为支持中学课程改革,有意向空间向量倾斜.利用空间向量求解立体几何问题要比传统几何方法“程序化”一些.当然,这是以掌握空间向量的基本概念和基本运算为前提的.3)关于“构造法”与“向量法”.这是本单元的两大基本方法.“构造法”即… 相似文献
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现行高中数学教材第二册(下)立体几何一章在阅读材料《欧拉公式与正多面体的种类》一文中证明了正多面体只有五种.笔者在教学中发现,学生在阅读此材料时,对于过每个顶点的棱数m和每个面的边数n的求解过程难以理解,本文将给出该命题的 相似文献
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ECR离子源的等离子体阻抗对其微波传输与阻抗匹配设计至关重要。在中国科学院近代物理研究所现有的2.45 GHz ECR 质子源上,对等离子体阻抗进行了测量。首先用水吸收负载代替等离子体负载测量得到了所用微波窗阻抗,然后根据质子源测量数据,推算得到了等离子体阻抗。实验结果表明,脊波导输出端阻抗与后续负载不完全匹配,等离子体阻抗随微波功率变化呈非线性。这些结果为ECR离子源过渡匹配和微波窗的设计提供了参考依据。Plasma impedance of an ECR ion source is important for microwave transmission and impedance matching design. Plasma impedance was measured indirectly with the 2.45 GHz ECR proton source at the Institute of Modern Physics, Chinese Academy of Sciences. In the test, we got microwave window mpedance by using water absorption load instead of plasma load, and the source plasma impedance was derived from the test data with the 2.45 GHz ECR proton source and microwave window impedance. The experimental results show that ridge waveguide output impedance and the subsequent load does not exactly match, plasma impedance variation is nonlinear with microwave power. The achievedresult is useful in the design of ridged waveguide and microwave window. 相似文献
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为了提高强流ECR 离子源的引出束流品质,分别设计了1# 和2# 引出系统,利用束流引出模拟软件PBGUNS 对1# 和2# 引出系统进行了质子束流引出与传输的模拟计算,结合实际测得的发射度数据分析引出系统,发现2# 引出系统比1# 引出系统引出束流品质高。对ECR 离子源引出系统的电势等位线分布等参数引起的球差进行了简单数学推导及MATLAB 绘图,并结合1# 和2# 引出系统束流相图模拟结果证明了球差会使引出束流品质有效发射度增长,通过适当加大电极孔径可改善束流聚焦情况,得到了束流光学聚焦较好的束流引出系统设计。To improve the quality of extracted ion beam from a high current ECR ion source, 1# and 2# extraction systems were designed and tested. The PBGUNS code was used to simulate the 1# and 2# extraction systems of proton ion beam. The emittance measurement results with the two different extraction systems were compared and analyzed with the simulation, the conclusion that more high quality beam extracted from 2# system than 1# system was got. The formula derivation of ECR ion source extraction system spherical aberration and MATLAB drawing was done by the analyzing on the distribution of extraction field equipotentials, effective emittance increasing caused by spherical berration was proved by 1# and 2# extraction systems beam phase space simulation result, beam focusing would be improved if electrode hole size increasing appropriately and a general concept on good optics focusing of ion beam extraction system was proposed finally. 相似文献
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为全面研究ECR(Electron Cyclotron Resonance)离子源引出的高电荷态离子束流品质,获取ECR离子源引出离子束流的横向四维相空间分布,提高向加速器的注入效率,中国科学院近代物理研究所研制了一台高精度Pepper Pot型发射度测量仪PEMiL(Pepper pot Emittance Meter in Lanzhou)。根据使用需求,利用KBr晶体喷涂技术取代传统的CsI闪烁体成像技术,解决了束流光斑重叠效应,获得了边界清晰的束流图像;并开发了相应的数据处理分析程序,以分析处理得到的束流横向四维相空间分布。利用PEMiL获得了75 keV,170 eμA的O5+束流横向四维发射度。分析结果表明:PEMiL测量分析后的束流发射度结果可靠性高,荧光屏电荷累积效应造成的发射度差异不超过25%,PEMiL可作为ECR离子源引出离子束流品质诊断的有效装置。 相似文献
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CdS, CdS:Mn, ZnS, ZnS:Mn and ZnS:Tb nanoparticles were prepared by using carboxylic-containing copolymer, polystyrene-maleic anhydride (PSM), as template. Average particle size, 2.5 nm for CdS nanoparticles, is deduced from UV-vis absorption spectra and consistent with the observation of TEM. Characteristic emissions of the doping ions can be observed and the energy transfer from the host to the doping ions is verified. Fourier transform infrared (FTIR) spectra were studied to confirm the bonding effect of the copolymer and the metal ions. PSM hydrolyzed and chelated metal ions by its carboxylic group, and then performed as a protection layer after the formation of nanoparticles. 相似文献