车轮所受静摩擦力的演示

汽车、自行车车轮所受静摩擦力方向往往被初学者弄错,教者又不易说明。我们用如下方法进行实验演示,效果明显。用直径为0.2mm左右的细钢丝做轮幅,做四个直径为25mm的车轮,安装在木制车斗上。前轮是从动轮,后轮是主动轮(轴上装上手摇曲柄)如图所示。为了增大前     

有色金属分析情报网第三次发射光谱分析学术交流会在青岛召开

全国有色金属分析情报网发射光谱分析学术交流会于1984年10月20日至26日在青岛召开。来自全国各省市的厂矿企业、研究院所、高等院校、仪器生产厂家共154个单位,188名代表参加了会议。西藏代表首次参加了情报网的发射光谱分析交流会。此次会议由北京有色金属研究总院和中国科学院海洋研究所共同主办。在大会上共交流了学术论文115篇,其中,矿石、矿物、金属与合金的分析45篇、高频等离子体光源光谱分析31篇、数据处理及计算机应用14篇、其它21篇。这次会议的显著特点是生产第一线的分析工作者提出了很多很好的     

An amperometric biosensor based on covalent immobilization of ascorbate oxidase on biocompatiable and low-toxic poly(thiophene-3-acetic acid) matrix

The biocompatiable and low-toxic poly（thiophene-3-acetic acid）（PTAA） matrix was successfully electrosynthesized in ionic liquid 1-butyl-3-methylimidazolium hexafluorophosphate（BmimPF₆） in comparison with the electrosynthesis of PTAA matrix in acetonitrile（ACN）.Ascorbate oxidase（AO） was used as a model for the development and application of biosensor.Vitamin C（VC） biosensors were facilely fabricated by the covalent immobilization of AO molecules on PTAA matrices electrosynthesized in ACN containing tetrabutylammonium tetrafluoroborate and BmimPF₆, respectively.Electrochemical impedance spectroscopy,scanning electron microscopy and FTIR spectroscopy indicated that AO molecules were covalently immobilized on PTAA matrices.Parameters of the as-obtained biosensors such as working potential,pH and temperature have been optimized.The amperometric biosensor based on PTAA matrix electrosynthesized in BmimPF₆ exhibited wider linear range,lower detection limit,higher sensitivity and bioaffinity,and better operational and storage stability than that electrosynthesized in ACN under optimal conditions.The as-obtained biosensor based on PTAA matrix electrosynthesized in BmimPF₆ was employed for the detection of VC content in commercial juices,and the result was close to the data given by manufacturers.Excellent results indicate that the PTAA matrix electrosynthesized in ionic liquid is a promising platform for the covalent immobilization of biologically-active species and the development of biosensors.     

环己烷氧化微孔催化剂的研究进展

环己烷氧化是化工生产中的重要反应之一,其氧化产物为重要的化工生产中间体,因此开发高效的环己烷氧化多相催化剂体系具有重要的理论意义和应用前景。本文综述了国内外环己烷选择氧化微孔催化剂的研究进展,分别对Y沸石、ZSM-5沸石及MOFs三大类微孔催化剂体系的组成及催化性能进行了介绍,最后展望了环己烷多相催化体系的发展趋势。     

基于NIR高光谱成像技术的长枣虫眼无损检测

为了研究快速识别虫眼枣与正常枣的有效方法,利用特征波长主成分分析法结合波段比算法进行虫眼枣识别。首先,利用NIR高光谱成像系统采集130个长枣(50个正常、80个虫眼枣)图像,提取并分析不同类型长枣特征区域的平均光谱曲线,对970~1 670 nm范围内的光谱数据进行主成分分析,确定7个特征波长(990,1 028,1 109,1 160,1 231,1 285,1 464 nm)。然后,对长枣图像做主成分分析,选择PC2图像进行虫眼识别,虫眼与正常枣的识别率分别为67.5%、100%。为了进一步提高虫眼枣的识别率,采用波段比(R1231/R1109)对未识别的虫眼枣进行再次识别,识别率提高到90%。结果表明,基于NIR高光谱成像技术的检测方法对虫眼枣识别是可行的,同时也为多光谱成像技术应用于在线检测长枣品质提供了理论依据。     

微型平像场近红外光谱仪的消杂散光设计

设计和研制了结构紧凑、杂散光低的微型平像场近红外光谱仪。在分光系统设计中不采用附加杂散光遮挡装置的常规方法,而是在准直物镜前设置一块直径为8．5mm的平面反射镜,通过调节平面反射镜改变入射光束的空间角,使光束全部被准直镜接收,不再产生旁光,从而有效地消除系统内的杂散光,使仪器整体杂散光水平降低了1．13％。另外,该光谱仪选择线阵CCD作为探测器件,不再设置冷却系统也避免了平面光栅带有扫描旋转机构。由于使用CCD作探测器和新的消杂散光设计方法,该光谱仪实现了微型化。     

具分布时滞Cohen-Grossberg神经网络周期解的存在性与吸引性

利用数学分析方法,讨论了具分布时滞Cohew-Grossberg神经网络周期解的存在性与吸引性,推广了已有的结论．     

Lifetimes of High Spin States in an Odd-Proton Nucleus 129Cs

Lifetimes of high spin states in 129Cs axe measured using the Doppler shift attenuation method. The high spin states of 129 Cs axe populated following the fusion evaporation reaction 124 Sn（UB, 6n）129 Cs at a beam energy of 65 MeV. The reduced transition probabilities B（E2） and the transition quadrupole moments Qt in the negativeand positive-paxity bands are deduced. The experimental results indicate that the Qt values of the negative parity band are smaller than those of the positive parity bands, probably due to different γ-deformation driving effects of different proton orbitals. The Qt values exhibit a considerable increase near the band crossing region in these bands. This behavior demonstrates that nuclear shape changing results from the neutron or proton alignments. The signature splitting of the πh11/2 and πg7/2 bands shows the opposite changing trend after backbending due to the h11~2 neutron and h11/2 proton alignments, respectively.