示波极谱测定甲基橙

<正> I. M. Kolthoff等曾指出甲基橙在滴汞电极下可被还原,我们在试验中发现:在Na2CO3底液中,于示波极谱仪上,甲基橙有一良好的极谱波,其峰电位在-0.75伏,在6×10-6～6×10-5M间,峰高与浓度成线性关系。常见离子和若干指示剂干扰不大。在实验的基     

大黄中大黄酚的二阶导数差示脉冲极谱法定量研究

建立了中草药大黄中大黄酚的二阶导数差示脉冲极谱定量分析方法。大黄酚在1moL／L氢氧化钾-1moL／L盐酸-甲醇(体积比为1：2：22)的溶液中，于-0．130V(vs．Ag／AgCl)处产生二阶导数差示脉冲极谱峰，大黄酚的浓度在10～80ug／mL范围内与其峰幅值呈良好的线性关系，线性相关系数r=0．9998，检出限为8．6ng／mL。测定结果的相对标准偏差为1．17％(n=8)，加标回收率为100．0％。     

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对所研制的质谱测量与分析系统进行了性能测试。烘烤后系统的极限真空达到了7.3×10-7Pa,总漏气率为3.84×10-9Pa.m3.s-1。上下球室之间的气体压力,以及漏孔的漏气率与高分辨四极质谱计的氦分压力均呈现了良好的线性关系。结果满足动态流导法真空校准的技术要求,为氘、氦混合气体的测量与分析提供了条件。     

Memristance controlling approach based on modification of linear M–q curve

The memristor has broad application prospects in many fields, while in many cases, those fields require accurate impedance control. The nonlinear model is of great importance for realizing memristance control accurately, but the im- plementing complexity caused by iteration has limited the actual application of this model. Considering the approximate linear characteristics at the middle region of the memristance-charge （M-q） curve of the nonlinear model, this paper pro- poses a memristance controlling approach, which is achieved by linearizing the middle region of the M-q curve of the nonlinear memristor, and establishes the linear relationship between memristances M and input excitations so that it can realize impedance control precisely by only adjusting input signals briefly. First, it analyzes the feasibility for linearizing the middle part of the M-q curve of the memristor with a nonlinear model from the qualitative perspective. Then, the lin- earization equations of the middle region of the M-q curve is constructed by using the shift method, and under a sinusoidal excitation case, the analytical relation between the memristance M and the charge time t is derived through the Taylor series expansions. At last, the performance of the proposed approach is demonstrated, including the linearizing capability for the middle part of the M-q curve of the nonlinear model memristor, the controlling ability for memristance M, and the influence of input excitation on linearization errors.     

高中物理实验中线性关系的建立与应用

高中物理实验是高考的重要考点,而在实验中合理应用图像解决问题更是热点.在高中物理实验中,各个物理量的关系错综复杂,多为非线性关系,因此,绘制出有关两个物理量的图像也多以曲线为主,很难利用图像解决实际问题.此文意从如何适当地转化物理量的形式,从而建立起它们之间的线性关系等相关问题进行研讨.     

Determination of iminodiacetic acid in the glyphosate by ion chromatography

In this paper,a simple method based on ion chromatography（IC） with conductivity detection was developed for the determination of iminodiacetic acid（IDA） in the herbicide of glyphosate.Under optimized chromatographic conditions,good linear relationship,sensitivity and reproducibility were obtained.The detection limit（LOD） for IDA obtained by injecting 25 μL of sample was 31.8 μg/L（S/N = 3）.Relative standard deviation（RSD） of repeated analysis for the peak areas was less than 1.53%（n = 6）.A spiking study was performed with satisfactory recoveries between 92.8%and 103.6%.It was confirmed that this method could be applied in glyphosate products.     

磁场对铁质类金属热导率影响的初步分析

通过使用TC-3型固体热导率测定仪测量外加磁场的铁质类金属圆柱的热导率,并采用控制变量法,从而探究磁场对固体热导率的关系,发现外加磁场与铁质类的金属热导率变化存在线性关系。     

Non-Markovian decoherent quantum walks

Quantum walks act in obviously different ways from their classical counterparts, but decoherence will lessen and close this gap between them. To understand this process, it is necessary to investigate the evolution of quantum walks under different decoherence situations. In this article, we study a non-Markovian decoherent quantum walk on a line. In a short time regime, the behavior of the walk deviates from both ideal quantum walks and classical random walks. The position variance as a measure of the quantum walk collapses and revives for a short time, and tends to have a linear relation with time. That is, the walker's behavior shows a diffusive spread over a long time limit, which is caused by non-Markovian dephasing affecting the quantum correlations between the quantum walker and his coin. We also study both quantum discord and measurement-induced disturbance as measures of the quantum correlations, and observe both collapse and revival in the short time regime, and the tendency to be zero in the long time limit. Therefore, quantum walks with non-Markovian decoherence tend to have diffusive spreading behavior over long time limits, while in the short time regime they oscillate between ballistic and diffusive spreading behavior, and the quantum correlation collapses and revives due to the memory effect.     

协方差不等式的证明和推论

利用构造二次函数的方法,证明了改进的协方差不等式,并在证明过程中得到3个推论,进一步探讨了随机变量具有线性关系时的若干结论.     

从多种角度看线性相关系数

1引言 在科学研究中,我们不但要了解一个变量的变化情况,更要进一步了解一个变量与另一个变量之间的关系．变量之间的常见关系有两种：一是确定性函数关系,变量之间的关系可以用函数表示;二是非确定性相关关系,变量之间有一定的关系,但不能完全用函数表达,变量间只存在统计规律．相关和回归是研究变量间线性关系的重要方法．但两者研究的角度不同．回归是研究变量间的因果关系的,力图把非确定性相关关系化归为确定的函数关系,达到通过自变量的已知值来预测因变量的未知值的目的．