用双波长可见光谱法快速测定半纤维素提取液中糖的含量

传统的Douglas比色法(间苯三酚-冰醋酸显色法)只能测定水溶性聚戊糖或戊糖,该研究对上述方法进行了改进,通过采用双波长技术实现对总糖和戊糖、己糖含量的同时测定。研究发现,425 nm是戊糖和己糖的等摩尔吸收波长,553 nm是戊糖的特征吸收波长,以上述二波长为基础大大简化了双波长法的计算公式。半纤维素提取液中干扰物质的光谱结果显示,提取液中的木素和葡萄糖醛酸对戊糖和己糖的测定结果都没有显著干扰。结果表明,该方法测定总糖和戊糖、己糖的含量都具有较高的精度和准确性,回收率为97.4%~101.9%。该方法简单、快速,非常适用于阔叶木和禾本科植物半纤维素提取液中混合糖含量的同时测定。     

关于二重极限的某种定义的一个注记

本文考虑二重极限的某种定义的缺陷.     

基于仓单质押融资的物流企业与银行的演化博弈分析

物流企业与银行之间的良好合作关系是物流金融业务继续发展的前提和基础。以仓单质押融资业务为例,运用演化博弈理论对物流企业与银行之间的监督包庇问题进行了分析,构建复制动态方程和运用动态相位图分析群体策略的演化过程及结果,为建立良好的合作关系提供理论依据。分析结果表明:该动态系统的演化方向受到博弈支付矩阵以及系统的初始状态的影响。银行监督成本、银行的收益损失、物流企业的包庇成本和物流企业的罚金是影响演化结果的关键性因素。通过外部力量的加入,可促使系统演化至(不包庇,不监督)这一期望演化稳定策略。     

K/n(G)系统可靠性评定的多源验前信息融合方法

在多源验前信息的情况下,以k/n(G)系统为例,讨论了如何对系统的可靠性指标进行估计的问题.在多个验前信息源给出了系统可靠性指标点估计的情况下,利用多层Bayes方法及经验Bayes方法对这些数据进行融合,并给出系统可靠性指标的Bayes点估计,同时对系统可靠度的置信区间也作了讨论.仿真算例表明这种处理方法是合理有效的.     

岩土工程位移时间序列的组合预测研究

将组合预测方法用于岩土工程位移时间序列预测.结合实际观测数据,分别建立位移时间序列预测的GM(1,1)模型、Verhulst模型和趋势曲线模型.采用极小误差法确定各单一模型的权重,建立组合预测模型.应用表明,组合预测的精度高,为岩土工程位移预测提供了一种实用、可靠的方法.     

Banach空间中Mann迭代和Ishikawa迭代的等价性问题

用不同于已有的方法证明了任意实Banach空间中一致Lipschitz强连接伪压缩算子在具误差的修正的Mann迭代和具误差的修正的Ishikawa迭代下收敛和稳定的等价性,其中迭代参数{βn}仅需lim sup n→∞βn〈k/L（L＋1）,这推广和改进了目前需假设lim n→∞ βn=0和两迭代程序初始点的取值需相同条件下的已有结果.     

甲磺酸培氟沙星与氯冉酸的荷移反应

利用甲磺酸培氟沙星与氯冉酸在甲醇介质发生荷移反应,建立了荷移分光光度法测定甲磺酸培氟沙星含量的方法。结果表明,荷移反应生成1∶1型配合物,最大吸收波长为530nm,甲磺酸培氟沙星线性范围为2.25×10-8—3.38×10-6mol/L浓度内,回收率为98.7%—101.4%。     

驻波情形的液体声光效应的理论与实验研究

模拟计算了液体声光衍射的贝塞尔函数,测量了不同质量分数NaCl溶液对激光的衍射效率和不同温度纯水对激光衍射的相对光强比,计算了不同质量分数NaCl溶液的声光相位延迟、声致折射率变化量幅值.结果表明:随着NaCl溶液质量分数的增加,声光衍射效率、相对光强比、声致折射率变化量幅值均不同程度下降,而温度对纯水的相对光强比影响很小.     

Attenuation correction for dedicated breast PET using only emission data based on consistency conditions

Accurate attenuation correction is required in dedicated breast PET imaging systems for image artifact removal and quantitative studies. In this study, a method using only emission data based on consistency conditions is proposed for attenuation correction in breast PET imaging systems. The consistency conditions are exploited to evaluate the accuracy of the estimated attenuation distribution and find the appropriate parameters that yield the most consistent attenuation distribution with the measured emission data. We have proved the validity of the method with experimental investigations and single-patient studies using a dedicated breast PET. The results show that the method is capable of accurately estimating the attenuation distribution of a uniform attenuator from the experimental data with various relatively low activities. The results also show that in single-patient studies, the method is robust for the irregular boundary of breast tissue and provides a distinct improvement in image quality.     

Multi-Slit Diffraction of Evanescent Electromagnetic Waves

The well-known Fraunhofer multi-slit diffraction is described as the multi-slit interference modulated by the singleslit diffraction, namely the multiplication between the single-slit diffraction factor and the multi-slit interference factor. By considering the simplified argument we show that the multi-slit diffraction of evanescent waves which are in the near-field region also has the interference and diffraction effects, and that this two-fold effect can be expressed as the convolution of the diffraction factor and the interference factor. Our conclusion could be helpful to understand the contribution of evanescent waves to the optical responses of sub-wavelength structures such as slits and grooves.