微波消解ICP-MS测定鲜竹笋中7种微量元素

建立同时检测鲜竹笋中铬、铜、锌、砷、镉、汞、铅等7种元素的分析方法。竹笋样品在硝酸介质中经微波消解,用电感耦合等离子体质谱(ICP-MS)检测,全定量法采集数据。校准曲线线性良好,相关系数在0.9937—1.0000之间;检出限为0.005—0.202μg/L;加标回收率在88.96%—110.5%;精密度RSD小于6.09%;国家标准样品西红柿叶(GSBZ51001-94)中几种元素的测定值都在标准范围内。该方法具有灵敏、可靠、快速、准确等优点,适用于竹笋中微量元素的分析测定。     

Ni-Zn合金物相分析的实验研究

利用X射线物相分析技术,辅以金相分析方法、差热分析技术研究了Ni-Zn体系的4个合金.实验结果表明,Ni-Zn合金系中存在中间化合物NiZn3,该化合物稳定地存在于650℃到室温之间.400℃下NiZn3(75%Zn)化合物的点阵常量为a=3.31919(4)nm,b=0.8866(2)nm,c=1.2518(2)nm.     

含Dzyaloshinski-Moriya相互作用的三量子位HeisenbergXX链的热纠缠

研究了外加磁场下具有Dzyaloshinski-Moriya(DM)各向异性反对称相互作用的三量子位Heisenberg XX链的对热纠缠以及在热平衡下用该链作为信道来传输未知的量子态。详细地给出了磁场、DM相互作用及温度对热纠缠和平均传输保真度的影响。结果表明:磁场和DM相互作用可以有效地调控对热纠缠;在温度较低情况下,关闭磁场和DM相互作用,顺铁磁链可以很好地用来做隐形传态的信道;纠缠不能完全反映平均传输保真度,相同的纠缠可以导致不同的平均传输保真度。     

Evolution of the ring-like vortices and spike structure in transitional boundary layers

At the late stage of transitional boundary layers, the nonlinear evolution of the ring-like vortices and spike structures and their effects on the surrounding flow were studied by means of direct numerical simulation with high order accuracy. A spatial transition of the flat-plate boundary layers in the compressible flow was conducted. Detailed numerical results with high resolution clearly represented the typical vortex structures, such as ring-like vortices and so on, and induced ejection and sweep events...     

Physical design of scanning gantry for proton therapy facility

A proton therapy facility based on a linac injector and a slow cycling synchrotron is proposed.To achieve effective treatment of cancer,a scanning gantry is required.The flexible transmission of beam and high beam position accuracy are the most basic requirements for a gantry.The designed gantry optics and scanning system are presented.Great efforts are put into studying the sensitivity of the beam position in the isocenter to the element misalignments.It shows that quadrupole shift makes the largest contribution and special attention should be paid to it.     

Investigation of the energy resolution with a RETGEM detector

A novel Micro-pattern gaseous detector (MPGD), thick GEM with electrodes made of a resistive material (RETGEM) is presented. In this paper we mainly investigate the energy resolution of a RETGEM in Ar+CO_2 with different gas mixtures. The results indicate that an energy resolution 30% in single and double mode can be obtained. The existence of an optimum energy resolution is discussed.     

微型平像场近红外光谱仪的消杂散光设计

设计和研制了结构紧凑、杂散光低的微型平像场近红外光谱仪。在分光系统设计中不采用附加杂散光遮挡装置的常规方法,而是在准直物镜前设置一块直径为8．5mm的平面反射镜,通过调节平面反射镜改变入射光束的空间角,使光束全部被准直镜接收,不再产生旁光,从而有效地消除系统内的杂散光,使仪器整体杂散光水平降低了1．13％。另外,该光谱仪选择线阵CCD作为探测器件,不再设置冷却系统也避免了平面光栅带有扫描旋转机构。由于使用CCD作探测器和新的消杂散光设计方法,该光谱仪实现了微型化。     

在化学教学中培养学生变量控制能力的实施和分析

设计受控实验是科学实验实证的重要手段,这种科学探究的核心能力,也是教育部在《普通高中化学课程标准(2017年版2020年修订)》中对学生能力的评价之一.在分析学生能力现状、教材内容后,经过教学实施,充分利用教材,帮助学生认识变量控制要素,达成能系统地综合应用变量控制解决实际问题的教学目标.     

矩形毛细微槽横截面上气液分界面形状理论分析

对背面有热流输入的矩形毛细微槽群横截面上的气液分界面形状进行了理论分析,在一定条件下对Wayner蒸发模型进行简化,根据等壁温条件推出蒸发薄液膜区域热流密度近似为定值,通过流体动力学理论推导出了微槽横截面薄液膜区域液膜厚度变化的关系式,并与Wayner蒸发模型的计算结果进行了比较。进一步提出了全新的交界线区域长度的判定方法,根据蒸发薄液膜区域总换热量计算得到蒸发薄液膜区域的长度,交界处接触角,以及固有弯月面区域的曲率半径,从而最终得出了微槽横截面整个气液分界面的形状曲线,理论分析表明:槽宽、热流密度、过热度等因素对蒸发薄液膜区域长度、接触角以及固有弯月面曲率半径等参数有较大的影响。     

Excitation and propagation of axisymmetric longitudinal guided waves in pipes immersed in infinite liquid media

The transient elastodynamic responses of the vacuum-filled and liquid-filled pipes surrounded by infinite liquid to external axisymmetric forces are simulated by employing the acoustic-structural coupled finite element method. The time-frequency distributions of the transients waveforms are obtained by the short-time Fourier transform （STFT）. Then the influence of the distribution of the external forces on the excitation of the guided waves is analyzed. The study shows that the L（O, 2） mode in the vacuum-filled pipe surrounded by the liquid is suitable for the pipe inspection because it is the fastest mode in a weakly dispersive and at- tenuative region of frequency. And it can be excited with high efficiency in the above region of frequency if the axisymmetric external force is applied on the inner or outer surface of the pipe axially. Analogously, the L（0,3） and L（0,4） modes in the liquid-filled pipe surrounded by the liquid are suitable for the pipe inspection.