高效液相色谱法测定原油脱钙工艺排水体系中NS-3缓蚀剂浓度

将反相高效液相色谱法用于原油脱钙工艺排水体系中缓蚀剂浓度测定研究,建立了缓蚀剂的快速分离检测方法.使用C18柱,以乙腈∶二氯甲烷=9∶1(V/V)混合溶剂为流动相,采用紫外检测器在300 nm处对排水体系中的缓蚀剂进行测定,外标法进行定性定量分析.测定结果表明缓蚀剂浓度在100~900 mg/kg时其峰面积与相应的质量浓度有良好的线性关系,其线性相关系数为0.999 9,相对标准偏差(RSD)和相对误差(RD%)都小于2.0%.用二氯甲烷为萃取剂对排水体系中的缓蚀剂进行萃取,其平均回收率为100%±2%.最低检测线为0.75mg/kg.该方法具有测定结果准确可靠,操作简便快速,重现性好等特点.     

微流控芯片计算机辅助设计、辅助制造方法研究

介绍了一种采用计算机辅助制造中快速成型技术实现微流控芯片快速制作的方法。采用VB二次开发工具(VBA),在计算机辅助设计(CAD)二次开发平台上建立微流控芯片三维CAD立体模型,并通过计算机软件算法对CAD模型进行分层切片,为实现微流控芯片计算机辅助制造提供加工数据。文中针对微流控芯片加工精度要求高的特点,提出了采用位图数据图像格式(BMP)数据格式取代快速成型分层切片中常用的三角面片数据格式(STL),并对具体实现方法进行了详细介绍。     

(Sm0.5Gd0.2Nd0.3)2(Hf0.3Ce0.7)2O7复合氧化物的热物理性能

为寻求新型热障涂层用陶瓷材料,本文采用高温固相烧结法制备了(Sm_0.5Gd_0.2Nd_0.3)₂(Hf_0.3Ce_0.7)₂O₇复合氧化物。利用XRD分析了其晶体结构,SEM分析其显微组织,膨胀仪测试其热膨胀性能,激光热导仪测试其热扩散系数。结果表明,成功制备了具有单一萤石晶体结构的(Sm_0.5Gd_0.2Nd_0.3)₂(Hf_0.3Ce_0.7)₂O₇复合氧化物。其显微组织结构致密,晶界清晰无其他相存在。由于复杂的元素组成和较大的原子量,其热导率明显低于7YSZ和Sm₂Ce₂O₇。其较低的热膨胀系数则归因于B位离子较小的离子半径,但其热膨胀系数依然满足热障涂层的要求。     

基于收入管理的CRM策略优化研究

在以客户关系为竞争导向的服务经济时代,有效的收入管理必须深入的结合客户关系管理策略.利用赋值马尔科夫过程方案决策的基本理论构建起了基于收入管理的CRM策略优化方案决策的随机模型,并对该模型方法进行了实证应用.结果表明通过应用该模型方法进行CRM策略的优化选择后,企业在加强客户关系承诺的同时能有效的提升其收入管理水平.讨论了研究结论对企业管理实践的意义.     

中子单色化新方法

提出了中子单色化的新想法，并从理论上给出了具体的处理方法．以石墨、硅及锗为例演示了新方法的应用，并得到满意结果．将新方法与三组双晶法作了比较，二者效果相差无几，但是新方法简单易行且节省费用 关键词：     

The Effects of CO2 Addition on the Partial Oxidation of Heptane for Hydrogen Generation

The effects of CO2 on the partial oxidation of heptane for hydrogen generation have been studied. Based on the experimental results and thermodynamic equilibrium calculations, the validity of CO2 addition to weaken the hot spots, and the feasibility of the autothermal operation are discussed.     

The Design of the ECRH/ECCD Launcher System for the HL-2A Tokomak

Electron cyclotron resonance heating and electron cyclotron current drive （ECRH/ECCD） have developed significantly in recent years such as Tore Supra, JT-60U , Heliotron j. It has many advantages over other means of heating and current drive. Firstly, the launcher can be located far away from the plasma. Secondly, the fact that the ECRH/ECCD power can be injected as narrow Gaussian beams, giving rise to highly localized power deposition, makes ECRH/ECCD an ideal candidate for local MHD control.     

HL—1装置交流放电碳化实验

一种交流放电原位碳化技术首次在HL-1装置环形真空室内壁进行了试验。碳沉积膜样品作了扫描电镜,俄歇电子能谱和二次离子能谱深度轮廓和成分分析。壁碳化前后托卡马克放电杂质可见光谱和真空紫外光谱强度对照分折表明,碳化壁状态下,孔烂和金属壁材料Mo和Cr等在等离子体中含量下降80％左右,而C,O等轻杂质量有所上升;氢粒子约束时间τ_p和再循环率系数R较裸金属壁状态大致增加20％。碳化壁经惰性气体He或Kr放电锻炼后,在托卡马克放电中壁表面显示出明显的抽吸作用。     

AN APPROACH OF ESTIMATING EXCITATION CROSS SECTIONS IN MULTIPHOTON PROCESSES

We suggest a simple approach to roughly estimate the excitation cross sections of various steps in a multiphoton ionization (or dissociation) process by applying the measured dependence of product signal on laser intensity. The validity of this method is demonstrated theoretically by means of the rate equations based upon a two-step kinetic model and can, in principle, be extended to the multiphoton process with steps more than two. Some results of numerical test and experiment are quoted.     

HL-2M �����֧�Ŷ���ͼ�������

The manufacturing process of integral special-shaped forgings of the HL-2M vacuum vessel support trunnion was introduced, and the material testing was conducted by cutting the samples from the forging body. The test results show that the yield strength of the surface and core position of the trunnion forgings are 1100MPa and 1057MPa respectively, the grain size grade of those two positions can be up to grade 4, and all mechanical performance parameters can meet the design requirements.