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81.
Ultralong mesoporous TiO2-B nanowires were synthesized via a hybrid hydrothermal-ion exchanging-thermal treatment using tetrabutyl titanate (TBOT) as a raw material. The phase transformations and porous structures of TiO2-B nanowires were characterized and studied by X-ray diffraction (XRD), transmission electron microscopy (TEM) and N2 adsorption-desorption measurement. Mesoporous TiO2-B nanowires showed a length of several micrometers and diameter of about 25 nm. The porous structures of obtained TiO2-B nanowires were demonstrated by BJH pore distribution measurement. The wirelike morphologies and porous structures of monodisperse nanowires calcined at 600 °C showed little change, which indicated that such nanowires possessed high thermal stability. The formation mechanism of TiO2-B nanowires with mesoporous structures were also discussed based on our experimental results. 相似文献
82.
The surface reconstruction of SrTiO3(110) is studied with scanning tunneling microscopy and density functional theory (DFT) calculations. The reversible phase transition between (4×1) and (5×1) is controlled by adjusting the surface metal concentration [Sr] or [Ti]. Resolving the atomic structures of the surface, DFT calculations verify that the phase stability changes upon the chemical potential of Sr or Ti. In particular, the density of oxygen vacancies is low on the thermodynamically stabilized SrTiO3(110) surface. 相似文献
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报道了Na2+离子的三个低激发态1Σu、2Σg、2Σu在二个光脉冲作用下的解离动量谱,激光波长为680nm,各脉冲功率为1×1012W/cm2,脉宽50fs,从研究结果可见,其单光子、双光子、三光子激发的对应的解离峰及峰值随相对相位而变,并且这种影响随延时增大而减小. 相似文献
87.
患有呼吸问题的病人由于呼吸道腺体不受意识控制、异物或者其本身肺部病变等原因会出现呼吸异常。医护人员通过病人的呼吸状况可以找寻和分析病人出现这种呼吸状况的原因。而以往呼吸声的诊断方式是专业的医护人员通过使用听诊器对病人进行肺部听诊。但是听诊的结果取决于医护人员的经验与相关参数。在初级诊断治疗阶段,初级医生识别听诊声的效率以及准确率很低,一般从20%到80%不等。因此会存在10%到20%的高误诊率(漏诊、错诊和延误)。本文提出了一种利用PVDF薄膜传感器提取语声特征的检测系统,该检测系统根据病人发出声音的不同,提取呼吸声特征值判断病人的呼吸状况。通过PVDF传感器采集的微弱呼吸声再经过KNN算法分类之后其识别率可达90.6%,对于细分种较类多的湿罗声,其识别率在80.2%左右。综上表明相比于传统听诊方式通过PVDF传感器采集识别的结果具有更高的准确性和可靠性,其判断呼吸状况的结果可以为医护人员提供参考,更好的为患有呼吸疾病的病人提供监测。 相似文献
88.
The Isodyne technique based on the scattered light scanning from a thin laser beam can be used to obtain the information inside
the loaded object in the room temperature nondestructively, so it is a very powerful technique in 3D stress analysis. The
problems are how to interpret the information and how to get sufficient information from the few interference fringe. Birefringence
phase shift technique can distinguish the fringe orders automatically and enrich the information in 256 gray levels between
maxim and minim light intensity. In the paper the Isodyne birefringence phase shift method with an oblique incidence and equilibrium
equation is presented, by which the 3D stresses in the middle plane of a plate with U shape notch are separated successfully.
The project supported by the National Natural Science Foundation of China under the Grant No. 1380345 相似文献
89.
Assoc. Prof. Dr. Tuo Wang Prof. Dr. Jinlong Gong 《Angewandte Chemie (International ed. in English)》2015,54(37):10718-10732
Solar water splitting provides a clean and renewable approach to produce hydrogen energy. In recent years, single‐crystal semiconductors such as Si and InP with narrow band gaps have demonstrated excellent performance to drive the half reactions of water splitting through visible light due to their suitable band gaps and low bulk recombination. This Minireview describes recent research advances that successfully overcome the primary obstacles in using these semiconductors as photoelectrodes, including photocorrosion, sluggish reaction kinetics, low photovoltage, and unfavorable planar substrate surface. Surface modification strategies, such as surface protection, cocatalyst loading, surface energetics tuning, and surface texturization are highlighted as the solutions. 相似文献
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