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采用原子吸收光谱法测定了96例精神分裂症患者和101名正常对照组的头发Zn、Cu、Fe、Ca、Mg元素含量。结果发现,精神分裂症患者头发n和Mg元素含量明显低于对照组,而Cu、Fe和Ca元素含量明显高于对照组。提示精神分裂症的发病,可能与Zn和Mg元素含量降低,Cu、Fe和Ca元素含量升高有关。 相似文献
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应用装有EPM-810Q电子探针扫描分析电镜,对50例乙肝患者头发中Mg、Al、Cd、Ca、Cr、Mn、Fe、Cu、Zn、Pb、Se11种元素含量进行分析,并与健康人头发进行比较。结果表明:乙肝组中Zn含量低于健康组,Cu、Cd、Fe含量高于健康组(P〈0.01)。 相似文献
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用原子吸收光谱法测定了70例健康老年人、30例健康成年人和30例老年高血压病人血清中Cu、Zn、Fe、Mn、Ca、Mg6种元素的含量.结果表明,健康老年人组与健康成年人组(对照组)相比,除Fe以外,Cu、Zn、Mn、Ca、Mg均有显著性差异;与老年高血压病人组相比,除Mg以外,Cu、Zn、Fe、Mn、Ca均有显著性差异.我们认为稳定的Cu/Zn比值及较高的血Mg水平是健康老年人未发生心血管疾病及糖尿病的重要原因之一,而高Cu、高Ca及显著偏高的Cu/Zn比值,则是发生高血压的一个重要原因。 相似文献
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菊花微量及宏量元素分析 总被引:8,自引:0,他引:8
用ICP-AES法测定了药用野菊花和抗白菊及6种人工栽培菊花中As,B、Ba、Ca、Cd、Co、Cu、Fe、Mg、Mn、Mo、Ni、Pb、Se、Si、V、Zn、P、S、K等元素的含量。结果表明:(1)菊花中Ca、Mg、P、S、K含量很高,B、Fe、Mn、Zn也有较高的含量;(2)野菊花中B、Ca、Fe、Mg含量较其他品种高、,抗白菊中Mn、Se、S含量高地其他品种;(3)代栽培的菊花K、P含量高于 相似文献
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通过EPM-810Q电子探针扫描分析电镜,对在治疗中53例结核患者头发Mg、Al、Cd、Ca、Cr、Mn、Fe、Cu、Zn、Pb、Se11种元素含量进行分析,并与健康人头发比较。结果表明:结核组中Ca、Zn元素含量低于健康组,Cu、Fe元素含量高于健康组(P〈0.01)。 相似文献
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利用火焰原子吸收法测定了中国银行韶关节市分行458名职工头发中Cu,Fe,Zn,Ca含量,运用统计学方法求出该人群中正常者与白发,脱发者Cu,Fe,ZnCa的特征含量,通过数据比较可看出,白发者Cu,Fe,Zn,Ca的含量均低于正常组,而脱发者与正常组较接近,经相关性检验,证明了Cu,Fe,Zn,Ca偏低的血发存在的相关性,与脱发没有相关性,经过性别比对,女性发中Cu,Fe,Zn,Ca含量均高于男 相似文献
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采用原子吸收分光光度法测定87例中风患者血清中Ca、Mg、Zn、Cu、Fe含量,并与正常组作对比。结果表明:中风患者Zn、Fe降低,而Mg、Cu增高,Zn/Cu比值降低(P<0.05~0.01);而两组血清Ca无统计学上的差别(P>0.50)。 相似文献
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用等离子体发射光谱法测定了广州和化州两地区半边旗的25种元素,在检出的20种元素中,含有人体必需的微量元素Fe、Zn、Cu、Mn、Co、Mo、Ni、Cr、V,以Zn、Mn、Fe、Cu等元素含量较高,这为研究微量元素对半边旗的生长和抗癌作用的影响提供了启示。 相似文献
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The spectral-polarization characteristics of absorption and phosphorescence of molecules of the initial form of nitro-substituted
indolinospirobenzothiopyran were studied in oriented polyethylene films and in solutions with different polarity. An oscillator
model of the electron transitions responsible for the formation of absorption and luminescence spectra was suggested. It was
established that the principal differences in the spectral and photophysical properties of the compound studied and its oxygen-containing
analog are associated with the fact that the electronegativity of the S atom is lower than that of the O atom.
Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 6, pp. 1143–1146, June, 1997. 相似文献
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Two vanilloids, (5E)-8-(4-hydroxy-3-methoxyphenyl)oct-5-en-4-one (1) and 4-[3-hydroxydecyl]-2-methoxyphenol (2), isolated from the dried seeds of Grains of Paradise (Aframomum melegueta), were synthesized; the latter compound was made as the S-enantiomer and the material derived from the seeds was found to be a 1:1.7 mixture of the R and S isomers. The synthetic route used should allow the preparation of analogs having extended alkyl chains and consequently different lipophilicity, and 3, a homolog of 2, was also prepared. 相似文献
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Stepkowska E. T. Perez-Rodriguez J. L. Jimenez de Haro M. C. Sayagues M. J. 《Journal of Thermal Analysis and Calorimetry》2002,69(1):187-204
Main hydration products of two cement pastes, i.e. CSH-gel, portlandite (P) (and specific surface S) were studied by static heating, and by SEM, TEM and XRD, as a function of cement strength (C-33 and C-43) hydration time (th) and subsequent hydration in water vapour.Total change in mass on hydration and air drying, Mo, increased with strength of cement paste and with hydration time. Content of water escaping at 110 to 220°C, defined as water bound with low energy, mainly interlayer and hydrate water, was independent on cement strength but its content increased with (th). Content of chemically bound (zeolitic) water in CSH-gel, escaping at 220-400°C, was slightly dependent on strength and increased with (th). It was possibly derived from the dehydroxylation of CSH-gel and AFm phase. Portlandite water, escaping at 400-500°C, was independent on cement strength and was higher on longer hydration. Large P crystals were formed in the weaker cement paste C-33. Smaller crystals were formed in C-43 but they increased with (th). Carbonate formated on contact with air (calcite, vaterite and aragonite), decomposed in cement at 600-700oC. It was high in pastes C-33(1 month) and C-43(1 month), i.e. 5.7 and 3.3%, respectively; it was less than 1% after 6 hydration months (low sensitivity to carbonation) in agreement with the XRD study showing carbonates in the air dry paste (1month), and its absence on prolonged hydration (6 months) and on acetone treatment. Water vapour treatment of (6 months) pastes or wetting-drying increased this sensitivity.Nanosized P-crystals, detected by TEM, could contribute to the cement strength; carbonate was observed on the rims of gel clusters.This revised version was published online in November 2005 with corrections to the Cover Date. 相似文献
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Cotton cellulose was swollen in a sodium hydroxide solution and carboxymethylated by a two-bath method for different periods of time for each process. The kinetics of acid hydrolysis and the crystallinity of the swollen and carboxymethylated samples were measured. The proportion of broken bonds, rate constants for hydrolysis, and permeability of cellulose to hydrolyzing agents were calculated. The susceptibility of glycosidic linkages to acid hydrolysis was improved by carboxymethylation more than by swelling in alkali. The increased accessibility of carboxymethylcellulose to acid was regarded as a consequence of increased intra-and intercrystalline swelling and of the glycosidic bonds' weakness caused by the electron-attracting carboxymethyl group on the C-6 position. 相似文献
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The aim of the presented work was the investigation of thermal oxidation of ilmenite in static air atmosphere. The investigations
were carried out by use of a derivatograph (MOM, Hungary). The changes of crystallographic structure of investigated samples
were identified by X-ray diffractometry on Philips PW-1710 diffractometer. In temperature above 500°C appears structure of
hematite Fe2O3. On the basis of the thermogravimetric measurements, the contracting area and contracting volume models were found as the
best fitting experimental data.
This revised version was published online in August 2006 with corrections to the Cover Date. 相似文献
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Cyclopropyl derivative of 2,6-di-tert-butylphenol is synthesized as a probe to investigate the mechanism of base-catalyzed autooxidation of phenol derivatives. Our study indicates that one electron reduction of molecular oxygen from phenolate gives phenoxyl radical 3, a key intermediate of autooxidation. The coupling of phenoxyl radical and superoxide radical gives peroxylate anion 4 and produces the final epoxy alcohol adduct 6. 相似文献