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1.
铝-铜-镓三元系富铜合金的室温固相截面已经用X射线分析法测定出来了,并对每一个相区的相边界都作了精密的测定.合金含量最高达50%(重量)1)铝及50%镓. 室温相截面由7个单相(即)相区、10个双相 区和7个三相(即       所构成.所有单相和三个二元系内所有单相相同,没有新相出现.  相似文献   

2.
本文采用了铝-8-羟基喹啉-5-磺酸(H2QS)-十六烷基三甲基溴化铵(CTMAB)胶束增敏体系,用荧光光度法对7种儿童膨化食品中痕量铝进行了测定,同时对样品的测定条件和消化处理进行了较详细的研究。方法简单、快速、灵敏度高,测定结果令人满意。  相似文献   

3.
叙述了镧-镍-铝(La-Ni-Al)合金分镍、铝及微量杂质元素锌、铁、锰、镁、硅、铜和钙的ICP-AES测定方法。样品以HNO3(1+1)溶解,稀释后直接测定主量元素镍和铝;用基体匹配法补偿基体效应测定其他杂质元素。各元素回收率在95%-106%,相对标准偏差优于5%。  相似文献   

4.
偏最小二乘法用于荧光法同时测定锌,铝研究   总被引:2,自引:0,他引:2  
本文将偏最小二乘法用于荧光光度法同时测定锌,铝。确定了锌、铝-桑色素在表面活性剂存在下最佳实验条件。所建立的方法用于人发中微量锌、铝测定。  相似文献   

5.
铝-氟-DSPCF分光光度法测定地下水中铝   总被引:1,自引:1,他引:0  
本文研究了铝-氟-1,5-二(2-羟基-5-磺基苯基)-3-氰基甲(DSPCF)的显色反应。在硼酸-硼砂介质中,显色反应灵敏,最大吸收波长为610nm,配合物的表现摩尔吸光系数5.0×104,铝含量在0-15μg/25mL符合比尔定律。该法用于地下水中微量铝的测定获得了满意结果。  相似文献   

6.
铝的空气-乙炔火焰原子吸收法测定的研究   总被引:6,自引:1,他引:5  
本文建立了一种用空气-乙炔火焰原子吸收法直接测定土壤中铝的分析方法。研究了添加四甲基氯化铵(TMAC)对测定铝时的增感效果,方法简便,快速实用,应用于土壤标准样品的测定,获得满意的结果。  相似文献   

7.
铝酸锶铕镝磷光体及其发光特性研究   总被引:6,自引:0,他引:6  
万体智  汤玲 《光谱实验室》1999,16(5):511-513
用燃烧法在600℃合成了铝酸锶铕及铝锶铕镝磷光体并测定了其激光光谱、发射光谱及长余辉性质。结果表明,铝酸锶铕镝更适宜于制备长余辉材料,而铝思铕适宜于制作瞬时激发--发光材料。  相似文献   

8.
阿莫西林-铜络合物光度法测定阿莫西林   总被引:10,自引:0,他引:10  
赵丽瑞 《光谱实验室》1999,16(2):189-190
本文提出了一种简便,快速,准确测定阿莫西林含量的方法,在Na2CO3介质中,阿莫西林与铜离子形成络合物,于334nm处产生最大吸收,测定阿莫西林的线性范围为2-50g.mL^-1本方法用于阿莫西林原料样品的测定结果满意。  相似文献   

9.
运用RH-402测氢仪测定具有高挥发性锂的铝-锂合金的固态氢含量具有相当难度。本文就如何鉴别体内氢和表面氢、如何选择加热功率和加热时间及试样大小做了大量探索实验,初步形成了可行的铝-锂固态氢含量的分析方法。同时就测量的误差来源及测氢过程中应注意之点进行了讨论。结果重复性好,且结果比较准确(利用俄罗斯铝-锂合金氢标样比较)。  相似文献   

10.
波长色散X射线荧光光谱法测定黄金饰品含金量   总被引:1,自引:0,他引:1  
本文提出应用波长色散X射线荧光光谱仪测定黄金饰品含金量的方法,本法对原有样品盒进行了改造,增设特制窗口和采取样品固定等措施,以系列参考标样建立校准曲线,用经验系数法校正基体效应。比例模拟法校正含量。9个参考标样和16个金标牌的测定结果表明,在含金量为37.50%-99.99%的范围内,方法的准确度好:含金量在99.99%-98.98%范围时,误差为0.03%-0.12%,在98.98%-37.50%范围时,误差为0.01%-0.52%,选用含金量不同的5个参考标样为代表,以0.7和1.4的模拟比例,经不同时间多次测定进行统计,相对标准偏差为0.05%-0.50%,说明方法的精密度好,本法操作方便,时样品无破坏  相似文献   

11.
Cyclic competition game models, particularly the “rock–paper–scissors” model, play important roles in exploring the problem of multi-species coexistence in spatially ecological systems. We propose an extended “rock–paper–scissors” game to model cyclic interactions among five species, and find that two of the five can coexistent when biodiversity disappears, which is different from the “rock–paper–scissors” game. As the number of fingers is five, we named the new model the “fingers” game, where the thumb, forefinger, middle finger, ring finger, and little finger cyclically dominate their subsequent species and are dominated by their former species. We investigate the “fingers” model in two ways: direct simulations and nonlinear partial differential equations. An important finding is that the number of species in a cyclic competition game has an influence on the emergence of biodiversity. To be specific, the “rock–paper–scissors” model is in favor of maintaining biodiversity in comparison with the “fingers” model when the variables (population size, reproduction rate, selection rate, and migration rate) are the same. It is also shown that the mobility and reproduction rate can promote or jeopardize biodiversity.  相似文献   

12.
Downstep in pitch contour of Chinese Putonghua is examined using subtly designed sentences by controlling tone combinations. The results show both automatic and nonautomatic downstep phenomena exist in Chinese. In non-automatic downstep, low tones compress downwards the pitch range of the following syllables. and the main influence of downstep is on topline. Low tone not only lower the topline behind it, but also raise the high tones before it, the effects are compatible with each other. In automatic downstep, the topline of pitch contour in intonational phrase is presented as a linear downtrend, but it differs among speakers due to the effect of personal stress practice. In comparison with downstep phenomenon in other tone or non-tone languages, the downstep ratio in Chinese is not constant, and the domain of downstep is not limited within the adjacent tones.  相似文献   

13.
The differences of the pitch and duration of Chinese syllables between Putonghua (PTH) and Taiwan Mandarin (TM) were studied. The speech materials to be used are not only isolated syllables, but also sentences. The results reveal that: For the isolated syllables, T1 and T2 in TM are influenced by Minnan dialect, therefore their pitch are lower than those in PTH. T3 is fall-rise in PTH, while it is fall in TM. Moreover, the syllable duration sequence for different tone is T3〉T2〉T1〉T4 in PTH, while it is T1〉T2〉T3〉T4 in TM. For the syllables in sentences, T2 is mid-rise in PTH, while it is mid-level in TM. And the T3 is longer than T4 but shorter than T1 or T2 in PTH, while it is the shortest in TM. Furthermore the effects of prosodic phrase boundary on duration for different tones are almost the same in PTH, but the lengthening part of T1 or T2 is longer than that of T3 or T4 in TM.  相似文献   

14.
It is shown that SU(2) QCD admits an dual Abelian-Higgs phase, with a Higgs vacuum of a type-Ⅱ superconductor. This is done by using a connection decomposition for the gluon field and the random-direction approximation. Using a bag picture with soft wall, we presented a calculational procedure for the glueball energy based on the recent proof for wall-vortices [Nucl. Phys. B 741(2006)1].  相似文献   

15.
16.
Two-dimensional scanning of a 0.6328 mum guided-light beam has been realized using noncolinear acousto-optic (AO) coplanar Bragg diffraction together with colinear AO guided-mode to substrate radiation-mode conversion in a Z-cut Xpropagation LiNbO3 proton-exchanged (PE) waveguide. The two surface acoustic (SAW) waves utilized are at the center frequencies of 500 and 200 MHz, propagating in the Y and X axes, respectively. Two-dimensional scanning of approximately 720 resolvable light beam spots, namely, 18 40 (horizontal vertical) scanning, has been demonstrated using a light beam of 1.0 mm aperture. The total number of resolvable beam spots can be greatly increased from 720 by simply utilizing SAW transducers of larger bandwidth and a light beam of greater aperture. It should also be possible to significantly increase the diffraction efficiency from 3 % by optimizing the parameters of the PE waveguide and the SAWs.  相似文献   

17.
Based on the research in Ref. [5][Materials Science and Engineering, 1989; A122: 57 63], an improved model of heat source is set up, the different modes of Lamb wave in an isotropic sample generated by a chopped electron beam at frequency f are obtained with integral transform and normal function expansion method, and the output signal of PZT coupled at the back surface of the sample is found out. The generation mechanism of SEAM (Scanning Electron Acoustic Microscopy) signal is discussed. It shows that the SEAM is a near field imaging technique with high spatial resolution and its best lateral spatial resolution is about 2√2α (α is the radius of the focused electron beam). Some of experimental results of SEAM images are presented in the paper and it shows that the spatial resolution of SEAM is better than 0.5 μm and smaller than the thermal diffusion length of the sample. Therefore the character of near field imaging in SEAM is also proved experimentally.  相似文献   

18.
Transmission spectra of coupled cavity structures (CCSs) in two-dimensional (2D) photonic crystals (PCs) are investigated using a coupled mode theory, and an optical filter based on CCS is proposed. The performance of the filter is investigated using finite-difference time-domain (FDTD) method, and the results show that within a very short coupling distance of about 3λ, where λ is the wavelength of signal in vacuum, the incident signals with different frequencies are separated into different channels with a contrast ratio of 20 dB. The advantages of this kind of filter are small size and easily tunable operation frequencies.  相似文献   

19.
The key to the restoration of rotational motion blurred image is how to restore the image under a low cost and to correct the irreversibility of the degradation function matrix.Based on the special qualities of degradation function matrix and precise deduction in space-domain, we present a new approach using gradient-loading for restoration of rotational blurred image.By easily adding a gradient operator, the irreversibility of the original matrix is corrected and can be applied for inverse filtering then.Gradientloading is the optimized approach which combines the advantages of both the approaches using constrained least square filtering and traditional diagonal-loading.Compared with the approach using least square filtering, its peak signal-to-noise ratio (PSNR) is improved from 3.18 to 6.46dB, while the computing time is reduced to 1/2-1/3.Experimental results demonstrate the effectiveness, noise-resistibility, robustness, and low complexity of this approach, which make it more suitable for real-time environment.  相似文献   

20.
We propose an all-optical logic device made of a bent tapered Y-junction waveguide with a Kerr-type nonlinear interface. It could provide an AND gate, OR gate, and exclusive-OR (XOR) gate. We could obtain different transmission results by adjusting the bending angle. The numerical simulation results show that the device functions as AND, OR, and XOR gates.  相似文献   

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