声学劳厄衍射和描述劳厄衍射斑的晶格模型

波在晶格中的衍射是波动学和固体物理学领域中的重要课题。本文第一部分描述了一个与在晶格中X射线的劳厄衍射相似的声学实验;第二部分主要讨论描述立方晶体中劳厄衍射斑的晶格模型。     

晶体X射线衍射的发现及其深远影响

1912年4月,弗里德里希、克里平和劳厄成功地观察到X射线透过硫酸铜晶体后的衍射斑点!随后劳厄推导出描述晶体衍射的著名劳厄方程.由于晶体X射线衍射的发现,劳厄于1914年荣获诺贝尔物理学奖.1912年10月,W.L.布拉格通过X射线透射ZnS晶体实验,推导出了著名的布拉格方程.1915年布拉格父子荣获诺贝尔物理学奖.晶体X射线衍射的发现对自然科学的影响是深远的.2012年是劳厄发现晶体X射线衍射100年,文章回忆了这段光辉的历史及其对科学技术所产生的深远影响,以怀念科学先驱们对科学技术的贡献,弘扬他们对科学研究的认真严谨的科学态度、勇于创新的科学精神和谦逊无私的品德.     

劳厄对晶体衍射的发现

介绍了劳厄提出晶体衍射思想的科学背景及当时的实验过程,并探讨在劳厄发现晶体衍射的过程中其科学思想的形成及X射线晶体衍射的发现带给我们的启示及影响．     

晶体X射线劳厄衍射分束特性研究

本文基于X射线衍射动力学分析了劳厄晶体的分束特性,模拟了晶体吸收和入射光角发散对于透射光和衍射光摇摆曲线的影响,定量给出晶体衍射面内角调节范围和晶体加工厚度对于劳厄衍射分束比的调制.在实验中,采用分析晶体和分束晶体的消色散配置限制入射光角发散的影响,实现300μm厚Si(220)晶体面内角调节劳厄衍射分束的精确测量,并得到300μm, 400μm和500μm厚度Si晶体分束比的调节范围,实现了透射光和衍射光强度的定量调制.     

多层膜劳厄透镜对8keV X射线的聚焦性能模拟研究

基于多层膜技术的劳厄(Laue)透镜能实现硬X射线纳米级聚焦,在X射线微纳分析领域具有重要的应用前景.基于衍射动力学理论,分析了X射线在多层膜劳厄透镜中的传播,计算了不同结构的多层膜劳厄透镜对8 keVX射线的聚焦性能.结果表明,最外层厚度为5 nm的倾斜多层膜劳厄透镜可获得5.7 nm的聚焦光斑和26%的平均衍射效率...     

纪念劳厄发现X射线衍射90周年学术报告会简讯

20 0 2年是劳厄 (MaxVonLaue)发现晶体X射线衍射 90周年 .劳厄的这一发现是 2 0世纪物理学的一件意义深远的大事 ,使物理学中关于物质结构和研究领域从宏观进入微观 ,从经典过渡到现代 ,发生了质的飞跃 .同时 ,X射线衍射的发现和研究对生物、材料科学和化学的发展起到了巨大的推动作用 .中国物理学会和中国晶体学会为纪念劳厄发现X射线衍射 90周年 ,由中国科学院物理研究所于 2 0 0 2年 12月 10日召开了学术报告会 ,会议邀请了部分院士、专家和广大同行 ,就X射线衍射的发现、发展历程 ,最新进展和研究展望以及在相关领域的应用进行了广泛…     

用劳厄相机研究金属玻璃的晶化过程

研究金属玻璃的晶化过程是了解金属玻璃的结构状态,探索金属玻璃微观结构信息的主要方法.我们采用劳厄相机对样的晶化过程进行了系统观测,所得的劳厄相清晰地记录了相变引起的衍射环形态和强度的变化.采用长的曝光时间有利于获得微弱信息。 本方法实际上是X射线针孔衍射法.过去一些书刊如文献[1]一样,认为这种方法只能获得几个有限的同心环,故不适用于物相分析.因此,用劳厄相机研究金属玻璃还没引人注意.我们的实验表明,在同一条件下劳厄法比德拜法所获得的衍射花样清晰,对花样变化反应灵敏,有时衍射环还比德拜法的多.这两者差异的原因是在…     

晶体的X射线衍射理论--劳厄与埃瓦尔德的遗产

文章概述了晶体X射线衍射理论的发展过程，介绍了不同形式的衍射几何理论、劳厄方程、布拉格方程与埃瓦尔德作图法，讨论了它们之间的异同之处．文章还介绍了运动学衍射理论和不同形式的动力学衍射理论，后者包括达尔文的简化处理、埃瓦尔德的表述和劳厄的表述，并对其物理后果进行了讨论，强调了动力学理论所预言的电磁波在周期结构中传播所引起的能隙．     

物理2003年第32卷第1—12期总目次

题　　　　　　目作者期号页码纪念劳厄发现晶体X射线衍射 90周年从劳厄发现晶体X射线衍射谈起唐有祺…………………………………………………………………………… 7(4 2 4 )X射线衍射发现郭可信………………………………………………………………………………………………… 7(4 2 7)晶体的X射线衍射理论———劳厄与埃瓦尔德的遗产冯　端　冯少彤…………………………………………… 7(4 34)X射线粉晶衍射仪的今天和明天林　帆　陆金生…………………………………………………………………… 7(4 4 1 )北京大学物理学科 90年专题历史的…     

纪念劳厄发现晶体X射线衍射100周年

文章从劳厄发现晶体X射线衍射的前因后果谈起.劳厄的这个发现产生了两个新学科,即X射线晶体学和X射线光谱学.文章中还回顾了布拉格父子对开展这两个新学科研究所作出的卓越贡献,并略述了X射线晶体学所产生的深远影响.     

Thermal characterization of longitudinal merging of turbulent spots

This study presents the thermal behavior of two young turbulent spots merging into a longitudinal direction on an isothermal flat plate for the local Reynolds number between 6.1 × 10⁴ and 1.3 × 10⁵ in a low freestream turbulence water tunnel having a turbulent intensity of 1.16%. The two turbulent spots are generated by water injection through a 1-mm-diameter hole in the perpendicular direction of the mainstream flow with a dimensionless separating time (Δτ) of 42.08, 84.16, and 126.24. Thermochromic liquid crystals are utilized mutually with an image processing technique to extract the spot characteristics qualitatively and quantitatively. The results demonstrate that the following turbulent spot directly causes an increase in the local Nusselt number and heat rate within the footprint of the merging spots. The relatively highest increase in this study occurs when Δτ = 84.16. The average Nusselt number and effectiveness characterize differently in the intersection zone, non-intersection zone of the leading spot, and non-intersection zone of the following spot. The results confirm that turbulent spots under the boundary layer transition augment the heat transfer rate to the level of full turbulence by not only their spot maturity but also the merging mechanism. Finally, the heat transfer mechanism is discussed and the predictive formulas for the Nusselt number and heat flux of the longitudinal merging of turbulent spots for Δτ from 0 to 126.24 are provided.     

On the Nature and the Motion of Arc Cathode Spots in UHV

Cathode spot types and spot motion of arcs in ultra high vacuum have been investigated with large area cathodes that consisted of two adjacent pieces of Mo and Cu. Arc currents were 20–60 A dc and 8–20 kA pulse (duration about 1 ms). Two spot types occured with different velocities and surface erosion: Type 1 spots are typical for surfaces covered by oxides or thick adsorption layers, whereas clean surfaces show only type 2 spots. During arc-conditioning both types exist simultaneously in a complex mutual dependence. Type 1 spots react weakly on the cathode material, while type 2 spots burn preferentially on Cu and at the boundary line between Mo and Cu. The motion of type 1 spots is determined by the expanding spot plasma, whereas type 2 spots show a step-by step motion, determined by explosions in the arc craters. Generally a spontaneous formation of type 2 spots beneath the arc plasma takes place only with contaminated surfaces (probably by a transition from type 1 to type 2 spots). Thus a breakdown between plasma and cathode surface requires the presence of contaminations. The observed effects occur in low current dc-arcs as well as in high current pulse arcs. They are discussed for different spot models.     

Growth criterion for small dry spots in the falling liquid films

In thin films of liquid falling over an inclined surface random (or non-random) small dry spots shut and disappear or expand into the large-scale dry spots depending on the initial spot sizes and parameters of the liquid film. On consideration of the gravity forces, inertial forces of the film and surface tension, affecting the elements of a roller surrounding the dry spot, we have formulated a criterion, which helped us to answer the following question: if this spot shuts or not? This criterion includes the numbers of Bond and Reynolds and the contact wetting angle as the determining parameters. It is generalization of the known Hartley — Murgatroid criterion, which allows determination of the zone of falling film metastability, i. e., determination of the critical film thickness, below whose value the formation of stable dry spots is possible. It is shown that the critical values of parameters of the initial dry spot depend on the shape and sizes of a roller surrounding this spot.     

强激光远场焦斑重构算法研究

 通过CCD图像采集单元结合传统的列阵相机测量高功率固体激光器的远场焦斑分布，采用图像处理技术的边缘算子提取焦斑的几何中心，提出通过几何中心对心的焦斑嵌套重构算法，解决了光斑饱和时的对心难题，实现了快捷准确测量激光焦斑，为激光器的实时控制提供参考数据。     

Concerning the Types of Cathode Spots

The kinds of electrical-arc cathode spots described in literature are analyzed. Division of spots into two types qualitatively different in nature?explosive spots and thermal spots?is proposed. The observed microsecond oscillations of the brightness of a rapidly moving spot are interpreted in terms of heat accumulation in the cathode and random motion of the spot. The transition of the spot to a thermal region is analyzed and the lifetime of nonstationary thermal spots is shown to be proportional to their size squared.     

Cathode Spot Phenomena in Low Current Vacuum Arcs on Arc-Cleaned Electrode Surfaces. II. Spot Dynamics

Part II of the paper presents results of high temporal and spatial resolution experiments with vacuum arcs on pre-arced surfaces. Immobile spots, continuous spot motion and spot position oscillations have been observed. Tentative explanations of these phenomena are offered.     

Voronoi analysis of the breakdown of order in spontaneous optical spot patterns

In a nonlinear optical single feedback system, patterns of bright spots evolve spontaneously. Making use of the Voronoi construction, the breakdown of spatial order in experimental spot patterns under increase of the pump laser intensity is analyzed. The spot density is found to increase with the pump intensity. Our analysis shows that maximum order is maintained for a finite range of spot densities and starts to break down at a clearly detectable threshold value. The enhanced disorder with increasing density contrasts the behavior of simple hard-core systems. A separate analysis of the metrical properties of the Voronoi cells in ordered and disordered regions yields remarkably smaller nearest-neighbor distances in disordered regions. This suggests that the creation of new spots is a governing mechanism for the observed breakdown of order.     

基于顺序形态变换的生物芯片图像网格化

生物芯片图像网格化是对由生物芯片扫描得到的荧光成像中的信号(Foreground)和背景(Background)进行划分,以便提取各点的吸光度值、面积和吸光度比等荧光点的数据。网格化的准确与否决定了数据提取的正确性。提出了一种运用顺序形态变换理论实现生物芯片荧光图像网格化的方法,通过对百分位值在0~1之间的顺序形态进行变换,可实现像素灰度的极小值、中间值等多刻度值的灰度取值运算。理论分析表明,该算法能够识别信号与背景的边界,可去除噪声等非边界信息,能判断信号区域,可确定荧光点的边界和范围,可实现荧光点阵图像的网格化。试验结果表明,该算法对不同信噪比的荧光图像来说有很强的适应性,可用于高密度生物芯片图像的处理。     

Microscopic high speed investigations of vacuum arc cathode spots

The main parameters and dimensions of cathode spots have been under discussion for years. To solve these current questions, a new system was specially designed. The image converting high speed framing camera (HSFC) combines a micrometer lateral resolution with a nanosecond time resolution and a very high optical sensitivity. This camera was used to study the microscopic behavior of vacuum arc cathode spots in a pulsed high current arc discharge on copper. The direct observation of these spots with high resolution revealed that one single cathode spot, as normally observed by optical means, consists of a number of simultaneously existing microscopic subspots, each with a diameter of about 10 μm and a mean distance of 30-50 μm between them. The mean existence time of these subspots on copper was found to be about 3 μs, where the position of a subspot remains unchanged (with an upper limit of about 5 μm) during its existence time. The lower limit of the current density in the cathode spots was estimated to be on the order of 10¹⁰-10¹¹ A/m². An upper limit of the crater surface temperature was estimated by a comparison between the brightnesses of a cathode spot and of a black body radiation lamp to about 3000 K