Low noise submillimeter SIS receiver with niobium nitride quasiparticle tunnel junctions

We have developed and tested a submillimeter waveguide SIS mixer with NbN-MgO-NbN quasiparticle tunnel junctions. The two junction array is integrated in a full NbN printed circuit. The NbN film critical temperature is 15 K and the junction gap voltage is 5 mV. The size of the junctions is 1.4 × 1.4 µm and Josephson critical current density is about 1.5 KA/cm² resulting in junction R_NC product about 40. The inductive tuning circuit in NbN is integrated with each junction in two junction array. A single non contacting backshort was tuned at each frequency in the mixer block.At 306 GHz the minimum DSB receiver noise temperature is as low as 230 K. The sources of the receiver noise and of the limits of the NbN SIS submillimeter mixer improvement are discussed.     

A low-noise SIS receiver measured from 480 GHz to 650 GHz using Nb junctions with integrated RF tuning circuits

A heterodyne receiver using an SIS waveguide mixer with two mechanical tuners has been characterized from 480 GHz to 650 GHz. The mixer uses either a single 0.5 × 0.5 µm² Nb/AlO_x/Nb SIS tunnel junction or a series array of two 1 µm² Nb tunnel junctions. These junctions have a high current density, in the range 8 – 13 kA/cm². Superconductive RF circuits are employed to tune the junction capacitance. DSB receiver noise temperatures as low as 200 ± 17 K at 540 GHz, 271 K ± 22 K at 572 GHz and 362 ± 33 K at 626 GHz have been obtained with the single SIS junctions. The series arrays gave DSB receiver noise temperatures as low as 328 ± 26 K at 490 GHz and 336 ± 25 K at 545 GHz. A comparison of the performances of series arrays and single junctions is presented. In addition, negative differential resistance has been observed in the DC I–V curve near 490, 545 and 570 GHz. Correlations between the frequencies for minimum noise temperature, negative differential resistance, and tuning circuit resonances are found. A detailed model to calculate the properties of the tuning circuits is discussed, and the junction capacitance as well as the London penetration depth of niobium are determined by fitting the model to the measured circuit resonances.     

高临界电流密度NbN约瑟夫森结的制备和特性表征

我们开展了高临界电流密度的NbN约瑟夫森结的制备和特性研究.利用直流磁控溅射方法在单晶MgO(100)衬底上外延生长NbN/AlN/NbN三层膜,并使用微加工工艺制备了NbN约瑟夫森隧道结,在液氦温度下对NbN约瑟夫森结的电流-电压特性进行了测量,实验结果表明,NbN约瑟夫森结具有良好的隧穿特性,其临界电流密度J_c为10 kA/cm^2,质量因子大于10,能隙是5.7 mV,这些实验结果为基于NbN结的超导数字电路研究奠定了坚实的基础.     

氮化铌表面氧化物的XPS研究

本文用X射线光电子能谱(XPS)对室温下自然氧化和射频氧化的氮化铌薄膜表面进行了成分分析。指出:与在类似条件下纯铌膜的氧化不同,NbN膜的表面氧化物中不存在NbO和NbO₂,而是以Nb₂O₃作为从NbN到Nb₂O_5-y的过渡相。氮化铌在氧化过程中表现出一种抑制Nb₂O,NbO等低价传导性氧化物生成的能力,这对于用氧化物作势垒的超导隧道结的研制具有实际参考价值。 关键词：     

A Low Noise NbTiN-Based 850 GHz SIS Receiver for the Caltech Submillimeter Observatory

We have developed a niobium titanium nitride (NbTiN) based superconductor-insulator-superconductor (SIS) receiver to cover the 350 micron atmospheric window. This frequency band lies entirely above the energy gap of niobium (700 GHz), a commonly used SIS superconductor. The instrument uses an open structure twin-slot SIS mixer that consists of two Nb/AlN/NbTiN tunnel junctions, NbTiN thin-film microstrip tuning elements, and a NbTiN ground plane. The optical configuration is very similar to the 850 GHz waveguide receiver that was installed at the Caltech Submillimeter Observatory (CSO) in 1997. To minimize front-end loss, we employed reflecting optics and a cooled beamsplitter at 4 K. The instrument has an uncorrected receiver noise temperature of 205K DSB at 800 GHz and 410K DSB at 900 GHz. The degradation in receiver sensitivity with frequency is primarily due to an increase in the mixer conversion loss, which is attributed to the mismatch between the SIS junction and the twin-slot antenna impedance. The overall system performance has been confirmed through its use at the telescope to detect a wealth of new spectroscopic lines.     

Investigation of the regimes of mixing of superconducting tunneling structures

The regimes of operation of a superconductor–insulator–superconductor tunnel junction based on three-layer structures Nb/AlOx/Nb and Nb/AlN/NbN as a harmonic mixer (for frequencies of the order of 600 and 20 GHz, respectively) and a frequency up-converter (in the frequency range from 0.1 to 5.0 GHz) have been investigated experimentally. The quasiparticle and Josephson mixing regimes have been compared. It has been shown that, in some practical applications, such as the use of the superconductor–insulator–superconductor junction as a cryogenic harmonic phase detector, the Josephson mixing regime is more preferable, because it can provide a higher signal and a greater signal-to-noise ratio as compared to the quasiparticle mixing regime. It has also been demonstrated that the Josephson mixing regime is promising for the use in signal multiplexing systems for superconducting detectors.     

Low noise 80–115 GHz quasiparticle mixer with small Nb/Al-Oxide/Nb tunnel junctions

Millimeter-wave characterization of a heterodyne receiver using (2 m²) Nb/Al-Ox/Nb Superconducting-Insulator-Superconducting (SIS) junctions arrays is reported. The fabrication of the Nb/Al-Ox/Nb SIS junction arrays as a heterodyne mixer is described. The leakage current of these junctions is below 2A at 4.2K and unmeasurable at 2.5K. The receiver gave a noise temperature Double Side Band (DSB) between 63K and 187K over the frequency range 80 to 115 GHz at the first conversion peak. The results are comparable to those obtained with SIS receivers using well researched lead junctions. Contrary to the lead junctions, our mixer using all Nb junctions have proven remarkably stable with respect to thermal cycling, characteristics which are required for space applications. To our knowledge, this is the most reliable low noise receiver operating in this frequency range.     

Superconducting integrated on-board spectrometer of the submillimeter-wave range for atmospheric research

We present the latest results of developing and implementing a fully superconducting integrated receiver of the submillimeter-wave range on the basis of the superconductor-insulator-superconductor tunnel junction. Characteristics of a new-generation unique device operated in the frequency range 500–600 GHz and intended for atmospheric research onboard a high-altitude balloon within the framework of the international TELIS project are given. This frequency range comprises spectral lines of many chlorine-containing compounds, the registration of which is a major problem of the environmental monitoring of the atmosphere. In the process of creating the spectrometer, we developed the technology for manufacturing Nb/AlN/NbN junctions, which made it possible to reduce the emission linewidth of the superconducting local oscillator based on the long Josephson junction and decrease the noise temperature of the receiver. At the same time, the possibility to continuously tune the local-oscillator frequency in the entire operating range was realized.     

Improvements of performance on sputter-coated niobium films for superconducting cavities by adding a NbN interlayer

A new type of superconducting film is studied at Peking University in order to improve the properties of sputter-coated films for superconducting cavities. NbN film and NbN–Nb film have been prepared by DC diode sputtering technology at certain nitrogen content and temperature. NbN film is prepared between copper and Nb film as a barrier against copper diffusion into Nb. Micro-structure analyses show that the NbN–Nb films grow well on the copper substrate. The T_c of the Cu–NbN–Nb increases to 9.5 K compared to the 9.2 K transition temperature of bulk Nb.     

A STJ X-ray detector with a β-tantalum sublayer

The first step in the research and development of detectors for ¹⁸¹Ta Mössbauer spectroscopy based on superconductive tunnel junctions (STJ) is taken. The idea of using β-tantalum as a trapping layer for the inactivation of the base electrode in a detector with the structure β-Ta/Nb/Al, AlO _x /Al/Nb/NbN is successfully executed.     

Production of high quality Nb/Al-oxide/Nb SIS trilayers for submillimeter wave mixers

Owing to a very sharp nonlinearity in the quasiparticle currentvoltage characteristic, which fortuitously occurs on the scale of a few millivolts rather than a few volts as with semiconductor devices, superconductor/insulator/superconductor (SIS) tunnel junctions are the most sensitive detectors for heterodyne mixing at millimeter and submillimeter wavelengths. They can also provide sources of coherent local oscillator power at very high frequencies; more broadly, they have a number of interesting applications as fast, low-power logic elements and as detectors at optical wavelengths. For submillimeterwave mixers, in many ways the most demanding of these applications, the Nb/Al-oxide/Nb material system has emerged as the system of choice to frequencies of ∼ 700 GHz and beyond. Production of SIS devices requires careful attention to a number of critical microfabrication issues, and I describe here some of the insights gained from developing a process for high-quality niobium trilayers that successfully yielded small-area junctions with unusually low sub-gap leakage current.     

On the passive electrode signal in X-ray detectors based on superconducting tunnel junctions

X-ray detectors based on superconducting tunnel junctions with the multilayer electrode structure described by the formula Ti/Nb/Al, AlO _x /Al/Nb/NbN were studied. The main signal arose during X-ray absorption in the top electrode and had an energy resolution of ∼90 eV at the 5.9-keV line. The bottom passive Ti/Nb electrode provided rapid absorption of excess quasiparticles. The residual signal of the passive electrode was from 7 to 17% of the main signal amplitude. The dependences of the amplitude of this signal on the voltage and the absorbed X-ray energy were measured for detectors with different thicknesses of the top and bottom electrodes. The rate of quasiparticle trapping by the energy trap in the Ti/Nb bilayer was estimated. The main mechanisms of the formation of the passive electrode signal formation were considered and methods for its suppression were proposed.     

Extraordinary terahertz transmission through subwavelength spindle-like apertures in NbN film

We studied numerically the temperature dependent extraordinary terahertz transmission through niobium nitride(NbN) film perforated with subwavelength spindle-like apertures. Both the resonant frequency and intensity of extraordinary terahertz transmission peaks can be greatly modified by the transition of NbN film from the normal state to the superconducting state. An enhancement of the(±1, 0) NbN/magnesium oxide(MgO) peak intensity as high as 200% is demonstrated due to the combined contribution of both the superconducting transition and the excitation of localized surface plasmons(LSPs) around the apertures. The extraordinary terahertz transmission through spindle-like hole arrays patterned on the NbN film can pave the way for us to explore novel active tuning devices.     

Fabrication of high-quality submicron Nb/Al--AlOx/Nb tunnel junctions

Nb/Al-AlOx/Nb tunnel junctions are often used in the studies of macroscopic quantum phenomena and superconducting qubit applications of the Josephson devices. In this work, we describe a convenient and reliable process using electron beam lithography for the fabrication of high-quality, submicron-sized Nb/Al-AlOx/Nb Josephson junctions. The technique follows the well-known selective Nb etching process and produces high-quality junctions with Vm=100 mV at 2.3 K for the typical critical current density of 2.2 kA/cm^2, which can be adjusted by controlling the oxygen pressure and oxidation time during the formation of the tunnelling barrier. We present the results of the temperature dependence of the sub-gap current and in-plane magnetic-field dependence of the critical current, and compare them with the theoretical predictions.     

A 650-GHz Band SIS Receiver for Balloon-Borne Limb-Emission Sounder

A superconducting low-noise receiver has been developed for atmospheric observations in the 650-GHz band. A waveguide-type tunerless mixer mount was designed based on one for the 200-GHz band. Two niobium SIS (superconductor-insulator-superconductor) junctions were connected by a tuning inductance to cancel the junction capacitance. We designed the R_nC_j product to be 8 and the current density to be 5.5 kA/cm². The measured receiver noise temperature in DSB was 126-259 K in the frequency range of 618-660 GHz at an IF of 5.2 GHz, and that in the IF band (5-7 GHz) was 126-167 K at 621 GHz. Direct detection measurements using a Fourier transform spectrometer (FTS) showed the frequency response of the SIS mixer to be in the range of about 500-700 GHz. The fractional bandwidth was about 14%. The SIS receiver will be installed in a balloon-borne limb-emission sounder that will be launched from Sanriku Balloon Center in Japan.     

230 and 492 GHz low noise sis waveguide receivers employing tuned Nb/AlOx/Nb tunnel junctions

We report results on two full height waveguide receivers that cover the 200–290 GHz and 380–510 GHz atmospheric windows. The receivers are part of the facility instrumentation at the Caltech Submillimeter Observatory on Mauna Kea in Hawaii. We have measured receiver noise temperatures in the range of 20K–35K DSB in the 200–290 GHz band, and 65–90K DSB in the 390–510 GHz atmospheric band. In both instances low mixer noise temperatures and very high quantum efficiency have been achieved. Conversion gain (3 dB) is possible with the 230 GHz receiver, however lowest noise and most stable operation is achieved with unity conversion gain.A 40% operating bandwidth is achieved by using a RF compensated junction mounted in a two-tuner full height waveguide mixer block. The tuned Nb/AlO _x /Nb tunnel junctions incorporate an end-loaded tuning stub with two quarter-wave transformer sections to tune out the large junction capacitance. Both 230 and 492 GHz SIS junctions are 0.49µm² in size and have current densities of 8 and 10 kA/cm² respectively.Fourier Transform Spectrometer (FTS) measurements of the 230 and 492 GHz tuned junctions show good agreement with the measured heterodyne waveguide response.     

Experimental observation of nonlinear ion - acoustic resonances in bounded plasma

The response of well matched Nb point-contract junctions, with a relatively small ratio of barrier and noise energy, has been measured at 35 GHz and is compared with theories on Josephson tunneling in the presence of strong fluctuations.     

1-THz low-noise SIS mixer with a double-dipole antenna

A quasi-optical mixer containing two Nb/Al/AlO_x/Nb superconducting tunnel junctions integrated into a NbTiN/SiO₂/Al microstrip line is studied experimentally in the 800–1000 GHz frequency range. The mixer is developed as an optional front end of the heterodyne receiver operating in frequency band 3 or 4 and incorporated into the HIFI module of the Herschel space-borne telescope. The double-dipole antenna of the mixer is made of NbTiN and Al films; the quarter-wavelength reflector, of a Nb film. The mixer is optimized for the IF band of 4–8 GHz. The double-sideband noise temperature T _RX measured at 935 GHz is 250 K at a mixer temperature of 2 K and an IF of 1.5 GHz. Within 850–1000 GHz, T _RX remains below 350 K. The antenna pattern is symmetrical with a sidelobe level below −16 dB.     

A Tuning Circuit with Two Half-Wave Distributed Junctions for All-NbN SIS Mixers

A novel broadband tuning circuit composed of two low-current-density half-wave NbN/MgO/NbN tunnel junctions connected by a half-wave NbN/MgO/NbN microstrip line has been successfully tested in a quasi-optical mixer at frequencies above 700 GHz. The circuit had a designed center frequency of 870 GHz, was integrated in a center-fed twin-slot antenna, and was fed via a quarter-wave impedance transformer. Heterodyne measurments showed double-side-band receiver noise temperatures equivalent to 6-9 quanta from 675 to 810 GHz for a mixer with a current density of 6.7 kA/cm². The RF bandwidth was broader than that of a conventional mixer using a full-wave junction with the same current density.