Shockwave Visualization Using Holographic Interferometer

High-speed holographic interferometry was employed to visualize and record Shockwave phenomena. We performed three kinds of holographic interferometry for visualization and recording of the propagation of a Shockwave: a real-time holographic interferometer with a high-speed framing camera, a real-time holographic interferometer with a high-speed streak camera and a double-pulse laser holographic interferometer with a dual-reference-beam module. The experimental results were compared and their advantages and disadvantages are discussed. The experimental results clearly show the high-speed Shockwave propagation and give the feasibility of quantitative interpretation of high-speed gas-dynamics.     

Analysis of the correlation between plasma plume and keyhole behavior in laser metal welding for the modeling of the keyhole geometry

The process of laser metal welding is widely used in industry. Nevertheless, there is still a lack of complete process understanding and control. For analyzing the process we used two high-speed cameras. Therefore, we could image the plasma plume (which is directly accessible by a camera) and the keyhole (where most of the process instabilities occur) during laser welding isochronously. Applying different image processing steps we were able to find a correlation between those two process characteristics. Additionally we imaged the plasma plume from two directions and were able to calculate a volume with respect to the vaporized material the plasma plume carries. Due to these correlations we are able to conclude the keyhole stability from imaging the plasma plume and vice versa. We used the found correlation between the keyhole behavior and the plasma plume to explain the effect of changing laser power and feed rate on the keyhole geometry. Furthermore, we tried to outline the phenomena which have the biggest effect on the keyhole geometry during changes of feed rate and laser power.     

Measurement of shock waves using phase shifting pulsed holographic interferometer

A phase shifting pulsed holographic interferometer was applied to the experimental study of the propagation of laser-induced shock waves over metal plates. A double-pulsed ruby laser was used to generate the shock waves and to make a holographic interferogram of the wave fields. The phase shifting method with a dual-reference beam solved the sign ambiguity problem in holographic fringe patterns and allowed a quantitative evaluation of the phase of the interference patterns. The transient surface profile and propagation behavior of the shock wave over plates were investigated from the holographic fringe patterns.     

Quantitative visualization of the laser induced plume behavior using quasi-heterodyne holographic interferometry

It is very important that we understand the dynamic behaviors of the laser induced plume in welding, because the laser induced plume has considerable effects on welding efficiency and the quality of materials. Many experimental studies have been performed in order to observe the plume behaviors using a visualization method. In this paper, we describe the visualization and quantification of the laser induced plumes by pulse holographic interferometry. A pulsed Nd:YAG laser was used for the generation of laser induced plume and a Q-switched Ruby laser was employed to record the weld plume. For qualitative visualization of the laser induced plume, we used the double-exposure holographic interferometry. Then, we chose the quasi-heterodyne holographic interferometry with the dual-reference-beam and phase shifting in order to visualize the plume quantitatively. The experimental results show the visible behavior of the laser induced plume according to a change in the output power of the pulsed Nd:YAG laser and the time delay of Q-switched Ruby laser. Finally, we obtained the quantitative results by using the dual-reference-beam.     

激光感生等离子体特性的三维数值模拟

在激光焊接过程中,作用于金属工件表面的高强度激光会引起材料的强烈蒸发,金属蒸汽与入射激光相互怍用,又会引起金属蒸汽部分电离,形成激光感生等离子体。本文采用三维模拟方法,考虑保护气和侧吹气的影响,对激光感生等离子体中的温度与速度分布进行了研究。     

Pulsed laser ablation of metals in vacuum: DSMC study versus experiment

We propose a hybrid model describing the processes of heating and ablation of a metal target with expansion of vaporized material into a vacuum under the action of nanosecond laser pulses of moderate intensity. The model is based on the integration of the thermal problem of laser-induced material heating and the direct Monte Carlo simulation method to describe the hydrodynamics of the ablation products. Modeling has been performed for niobium as an example and the results obtained are in good agreement with experimental data on mass removal and time-of-flight (TOF) measurements. Application of the commonly used fitting procedures for characterization of the laser plume parameters by the TOF signal is discussed. PACS 52.38.Mf; 79.20.Ds     

盘型激光焊金属蒸汽特征色调-色饱和度-亮度分析法研究

对于大功率盘型激光焊,金属焊件表面在激光束辐射下强烈汽化并形成等离子体状的金属蒸汽羽状物. 该金属蒸汽羽状物可逆向激光束传输,对激光有明显的屏蔽作用, 降低激光辐射至焊件的能量密度,影响焊接效率和质量. 因此研究金属蒸汽特征变化规律及其与焊接质量之间的关联 ,可实现由金属蒸汽特征实时监测激光焊接状态. 以10 kW大功率盘型连续激光焊接304不锈钢钢板为试验对象, 应用高速摄像机摄取金属蒸汽动态图像,将其转换至色调-色饱和度-亮度空间, 提取金属蒸汽面积、激光束受影响路径长度等相关特征量, 以焊缝熔宽的变化作为衡量焊接状态稳定性的参数. 通过金属蒸汽特征值的均值统计和方差分析,试验证明根据金属蒸汽面积和激光束受影响路径长度等金属蒸汽特征可有效地反映熔宽质量, 从而对焊接状况做出动态评估.     

Single-walled carbon nanotube formation with double laser vaporization technique

Single-walled carbon nanotubes (SWNTs) were prepared with double laser vaporization of a graphite target and a metal/alloy target inside an electric furnace at 1200 ^°C ambient temperature with 500 torr Ar gas atmosphere. Each target was vaporized simultaneously with a different Nd:YAG laser. Several kinds of metal/alloy target (Ni, Co, Fe, and permalloy) were tested in order to see the difference in the resulting SWNT yield and the diameter distribution of them. The Raman spectra of SWNT-containing soot prepared by use of this technique with permalloy/carbon system indicated that permalloy gives almost the same yield as compared with Ni/Co carbon composite rod with single laser vaporization technique, though the diameter distribution of them is slightly different. Also, time-resolved images of the plume by carbon and permalloy nanoparticles after laser vaporization were collected using a high-speed video camera. These images suggest that the hot plumes due to carbon and permalloy nanoparticles do not mix together so extensively, at least in a few hundred microseconds after laser vaporization. The effect of time delay between two laser pulses on the yield and the diameter distribution of SWNTs was also presented and discussed.     

Numerical analysis of hybrid plasma generated by Nd:YAG laser and gas tungsten arc

When the output from a high power Nd:YAG laser irradiates a metallic surface, metal vapor is generated and changes into the plasma state, which is called a laser-induced plasma plume. If the high power laser is combined with an arc plasma, they mutually attract and influence each other. In this study, several analytic steps are introduced to analyze the laser-arc hybrid welding plasma. A conduction equation is first solved to obtain the temperature distribution on the metallic surface. Next, an analysis of the metal vapor is conducted to investigate the Ar–Fe mixture using a numerical method. As a result of the analysis, it is revealed that the plasma is concentrated in the vicinity of the laser-irradiation position and that the local temperature of the plasma is increased. Plasma flow and current density profiles are also affected by the laser irradiation.     

Effects of laser intensity and ambient conditions on the laser-induced plume

Laser ablation presents a promising technique for material processing. The quality of products is strongly influenced by the properties of the laser-induced plume. In compressible flow, the ambient conditions can be transmitted upstream. Therefore, the laser ablation process is strongly affected by the ambient conditions. In this paper, the effects of laser intensity, back pressure and temperature on the laser-induced plume were studied using a numerical model, which calculates the density, pressure and temperature of the laser-induced plume at different laser intensity and ambient conditions. The results are in agreement with experimental results available in the literature and can be used for the optimization of the pulsed laser deposition process.     

万瓦级光纤激光焊接过程中小孔内外等离子体研究

为了进一步深入了解超高功率光纤激光深熔焊接过程中等离子体特征,试验拍摄了深熔小孔内外等离子体形态,并采用光谱仪检测分析了光纤激光致等离子体光谱信号.利用检测得到的等离子体光谱信号,计算研究了等离子体的电子温度、电子密度、电离度以及等离子体压力特征,并分析了在小孔内不同深度处及孔外等离子体的变化规律.结果表明,孔内等离子体呈现不均匀分布特征,孔外金属蒸气远多于等离子体.等离子体光谱分析显示,光纤激光致等离子体辐射出的谱线较少,即电离程度较低.进一步的计算结果同样证实了光纤激光致等离子体处于弱电离状态,但等离子体电子密度仍然处于较高水平,且等离子体瞬态压力可达到数百个大气压.     

亚微米结构的可见光聚合全息制作

报道用激光全息技术结合可见光光聚合制作周期结构的方法和物理机理;对多束激光相干产生的空间干涉光场进行了讨论;提供了一组激光束的偏振态的最佳组合,使激光全息技术制作理想的亚微米单晶结构更有效和快捷.分析了曝光量与制作效果的关系,此法可实现小球自排无法实现的大幅度占空比调节.与紫外光光聚合相比,可见光光聚合可在监视下调节,操作方便安全. 关键词： 激光全息技术 光学晶格 光子晶体     

Spectral diagnostics of a vapor-plasma plume produced during welding with a high-power ytterbium fiber laser

We have conducted spectroscopic studies of the welding plasma formed in the process of welding with an ytterbium fiber laser delivering output power of up to 20 kW. The influence of shielding gases (Ar, He) on different parts of the welding plume is investigated. The absorption coefficient of the laser radiation by the welding-plume plasma is estimated. Scattering of 532-nm probe radiation from particles of the condensed metal vapor within the caustic of a high-power fiber laser beam is measured. Based on the obtained results, conclusions are made on the influence of the plasma formation and metal vapor condensation on the radiation of the high-power fiber laser and the stability of the welding process.     

Influences of laser in low power YAG laser-MAG hybrid welding process

The influences of laser defocusing amount △z, laser power P, space distance DLA between laser and arc on weld penetration, arc modality and stability are investigated in low power YAG laser and metal active gas （laser-MAG） hybrid welding process. The experimental results indicate that the effects of laser-induced attraction and contraction of MAG arc are emerged in hybrid welding process, which result in the augmentation of hybrid welding energy. When DLA ： -0.5 - 2 mm, △z = -2 - 2 mm and P ≥ 73 W, the synergic efficiency between laser and MAG arc is obvious, the cross section at the root of hybrid arc is contracted and the hybrid weld penetration is increased. The maximal ratio of hybrid/MAG weld penetration is 1.5 and the lowest YAG laser power that augments MAG arc is 73 W. The input of YAG laser makes the stabilities of arc ignition and combustion prominent in hybrid welding process.     

Dynamics of single-wall carbon nanotube synthesis by laser vaporization

The key spatial and temporal scales for single-wall carbon nanotube (SWNT) synthesis by laser vaporization at high temperatures are investigated with laser-induced luminescence imaging and spectroscopy. Graphite/(Ni, Co) targets are ablated under typical synthesis conditions with a Nd:YAG laser at 1000 °C in a 2-in. quartz tube reactor in flowing 500-Torr Ar. The plume of ejected material is followed for several seconds after ablation using combined imaging and spectroscopy of Co atoms, C₂ and C₃ molecules, and clusters. The ablation plume expands in stages during the first 200 7s after ablation and displays a self-focusing behavior. Interaction of the plume with the background gas forms a vortex ring which segregates and confines the vaporized material within a ~1-cm³ volume for several seconds. Using time-resolved spectroscopy and spectroscopic imaging, the time for conversion of atomic and molecular species to clusters was measured for both carbon (200 7s) and cobalt (2 ms) at 1000 °C. This rapid conversion of carbon to nanoparticles, combined with transmission electron microscopy analysis of the collected deposits, indicate that nanotube growth occurs over several seconds in a plume of mixed nanoparticles. By adjusting the time spent by the plume within the high-temperature zone using these in situ diagnostics, single-walled nanotubes of controlled (~100 nm) length were grown and the first estimate of a growth rate on single laser shots (0.2 7m/s) was obtained.     

Laser ablation of YBa2Cu3O7-x: the wavelength dependence

Formation mechanisms of atomic and oxide ions in a plume (laser-induced plasma) produced by the laser ablation of a YBa₂Cu₃O_7-x (YBCO) target was studied by time-of-flight (TOF) analysis. The dependence of the TOF spectra on the laser wavelengths (266 nm and 1064 nm) was examined to elucidate photochemical phenomena in the plume. Significant changes in the relative enrichment of metal oxide and oxygen ions as well as their TOF distributions were observed by the injection of an oxygen jet to the plume, which induces reactive scattering of the YBCO plume and the oxygen jet.     

Influence of ambient gas on formation process of Si nanoparticles by laser ablation

We described the influence of a type of gas and its pressure upon the size distribution of Si nanoparticles fabricated by laser ablation in an ambient gas and the plume dynamics during the synthesis. The plume dynamics was investigated by laser-induced fluorescence and ultraviolet Rayleigh scattering. Based on the results, the importance of the gas flow within the ablation plume in the formation of the nanoparticles is understood.     

Correlation spectroscopy as a tool for detecting losses of ligand elements in laser welding of aluminium alloys

The plasma plume induced during laser welding of metals is a mixture of metal vapour, coming from the vaporised weld pool surface and shielding gas. The influence of the shielding gas on the welded joints quality is not yet well understood and very few investigations, to the best of our knowledge, were addressed to study its role in case of welding of aluminium–magnesium alloys. In this paper we present a study of the dynamics of plasma plume produced in laser welding of 5xxx aluminium alloys by means of correlation spectroscopy. By our results we can correlate the influence of the welding speed, in case of ineffective gas shielding, to the loss of alloying elements. Finally, the results obtained are consistent with the EDX analysis performed in post-processing on the welded joints.     

Study of Mn laser ablation in methane atmosphere

Laser ablation of Mn target in vacuum and in the presence of CH₄ was studied under 308 nm laser irradiation. Time-resolved emission using gated detection and scanning monochromator and absorption using the cavity ring-down spectroscopy were used to study vaporized plume. In the CH₄ atmosphere we observed transitions identified as C₂ and MnH bands, while these spectral features were not detected in emission spectra. This is a clear evidence of importance in combining both spectroscopic techniques in laser vaporized plume study.     

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利用时空分辨的测量技术,测定了XeCl紫外激光烧蚀金属Cu消融粒子的发射光谱随时间与空间的强度分布。通过在不同的氢气压强下拍摄到的XeCl308nm紫外激光烧蚀金属Cu消融粒子的发光羽照片,发现激光消融粒子发光羽的颜色在不同区域有不同的颜色,不同区域的发光羽颜色随环境气压的改变而变化。随环境气压的增大,发光羽不仅逐渐变小,而且逐渐变淡。对激光消融粒子发光羽的机理进行了探讨,激光消融粒子发光羽的发光动力学模式在不同区域有不同的发光模式,且随环境气压的变化而改变。定性地解释了所观察的实验现象。