提高射频超导加速腔性能的表面干式处理研究

射频超导谐振腔以其优越性在加速器领域起到了常温加速腔无法替代的作用. 超导腔的表面 特性直接影响到加速腔的性能. 为进一步提高超导腔的加速性能，北京大学利用超高真空氩 离子清洗技术发展了一种超导腔表面的干式处理方法. 与传统的湿处理方法(化学抛光BCP和 电抛光EP)相比，干式处理方法具有其特有的优点，有可能成为一种新的超导腔表面处理方 法，对提高加速腔的性能起到推动作用. 进一步的研究正在进行之中. 关键词： 射频超导 表面处理 溅射 抛光     

铜铌溅射型低β超导腔的研制及初步实验

超导谐振腔是超导加速器的关键部件.用于重离子超导加速器的低β加速腔的最佳选择是四分之一波长谐振腔(QWR).目前,利用无氧铜为基底,溅射一层几微米厚的铌膜,可以获得极好的超导性能和加速离子性能.但是,四分之一波长谐振腔的内表面复杂,溅射均匀的铌膜比较困难.针对此难题,发展了一种多参数可调节的溅射方法,在640×φ220的大型腔体内,成功地生成了一层均匀的、超导性能优异的铌膜.超导腔的低温实验表明铌膜的性能良好.     

改进铜铌溅射型QWR超导腔性能的探讨

通过直流偏压二级溅射方法，在无氧铜腔体表面溅射一层铌膜，研制了铜铌溅射型射频超导1/4波长谐振腔(quarter wave resonator,QWR)，该腔主要用于重离子的加速，是北京放射性核束装置中后加速部分的预研项目.目前国际上很多实验室都在研究进一步提高铜铌溅射型QWR超导腔的性能，通过多种方法的实验研究，发现在无氧铜衬底与铌膜之间加入一层氮 化铌（NbN）薄膜，可以使得表面铌膜的超导温度转变点由原来的8.8K提高到了接近9.6K ，该方法有可能成为提高QWR腔加速性能的重要途径，目前进一步研究正 关键词： 溅射 QWR超导腔 氮化铌NbN 超导温度     

射频超导腔加速性能的改进

 为提高超导加速腔的加速梯度和Q值，改进了薄膜型超导腔的加速性能。研究证明，对于铜铌溅射腔，在无氧铜衬底和铌膜之间加入NbN 层可以提高铌膜的超导转变温度，改善晶格结构；对纯铌超导腔提出了改进方法，在传统的纯铌超导腔表面制备多层的超导-绝缘-超导复合膜可以屏蔽Nb腔表面的界面场，提高超导腔的临界磁场，从而提高了铌腔的加速梯度。     

射频超导腔加速性能的改进

为提高超导加速腔的加速梯度和Q值，改进了薄膜型超导腔的加速性能。研究证明，对于铜铌溅射腔，在无氧铜衬底和铌膜之间加入NbN 层可以提高铌膜的超导转变温度，改善晶格结构；对纯铌超导腔提出了改进方法，在传统的纯铌超导腔表面制备多层的超导-绝缘-超导复合膜可以屏蔽Nb腔表面的界面场，提高超导腔的临界磁场，从而提高了铌腔的加速梯度。     

北京大学国产大晶粒铌材超导腔的性能研究

大晶粒铌材是射频超导领域的研究热点之一.采用大晶粒铌材的射频超导谐振腔,其后处理工艺可以大大简化.北京大学对此进行了深入细致的研究,自主研制了采用国产大晶粒铌材的射频超导腔,对这些超导腔进行了简单的表面处理,包括标准的化学抛光(BCP)和120.C低温烘烤处理,未进行非常复杂的电抛光处理,低温性能测试结果表明其低温超导性能优越,大晶粒1.3GHz超导腔的加速梯度达到了43.5MV/m,为我国超导加速器的国产化打下了基础.     

北京大学国产大晶粒铌材超导腔的性能研究

大晶粒铌材是射频超导领域的研究热点之一. 采用大晶粒铌材的射频超导谐振腔, 其后处理工艺可以大大简化. 北京大学对此进行了深入细致的研究, 自主研制了采用国产大晶粒铌材的射频超导腔, 对这些超导腔进行了简单的表面处理, 包括标准的化学抛光(BCP)和120℃低温烘烤处理, 未进行非常复杂的电抛光处理, 低温性能测试结果表明其低温超导性能优越, 大晶粒1.3GHz超导腔的加速梯度达到了43.5MV/m, 为我国超导加速器的国产化打下了基础.     

1．5GHz锯材超导腔的研制

介绍铌材超导腔的研制进展，重点讨论了国产铌腔的材料改性，以及相应的超导腔性能的改进．叙述了１．５ＧＨｚ铌腔的腔形设计，分析了铌材的射频性能和机械性能，制定了铌腔制作与后处理的特定工艺．最后给出了１．５ＧＨｚ铌材超导腔的低温实验结果．     

1．5GHz锯材超导腔的研制

介绍铌材超导腔的研制进展，重点讨论了国产铌腔的材料改性，以及相应的超导腔性能的改进．叙述了１．５ＧＨｚ铌腔的腔形设计，分析了铌材的射频性能和机械性能，制定了铌腔制作与后处理的特定工艺．最后给出了１．５ＧＨｚ铌材超导腔的低温实验结果．     

磁控溅射多层沉积Nb_3Sn超导薄膜北大核心CSCD

Nb3Sn金属合金是一种性能优良的超导材料。磁控溅射多层沉积是用两个溅射源分层沉积铌和锡,再经过高温退火后获得超导薄膜的方法。用这种方法所获得的超导薄膜的原子组分的调整比较方便,对于Nb3Sn的研究较为有利。实验测量了样品的超导参数和晶格参数,其超导临界温度(Tc)可达17 K,剩余电阻率(RRR)为5左右。需要进一步研究相关工艺,以便提高RRR,从而使这种方法在超导加速腔的制造中得到应用。     

Researches and Preliminary Experiments on Copper-Niobium Sputtered Low-β Superconducting Resonator

Superconducting resonator is the important component of a superconducting accelerator. The best choice of the acceleration cavity for heavy ion superconducting accelerator is quarter wave resonator (QWR). By sputtering a layer of niobium films of several microns on the OFHC copper substrate, good superconducting properties and acceleration properties of the cavity can be obtained. However, it is very difficult to get uniform niobium films by sputtering because the inner surface of the QWR is complicated. To deal with this problem, we developed a multiparameter adjusting method to control the sputtering process of different parts of the QWR. A layer of uniform niobium film with nice superconducting performance is obtained. The low temperature experiments with liquid helium show that the Cu Nb QWR has good superconducting characters. The Q value of the cavity is about 5×10⁸.     

射频超导谐振腔中的电磁场研究

由高纯铌制成的射频超导谐振腔在高场时会出现Q值下降现象，这是高场下超导腔表面局部磁场增强所致. 为研究高场下超导腔表面的电磁场特性，用单cell超导腔设计了腔表面峰值磁场的研究实验. 通过对单cell超导腔表面峰值磁场的测量，可以确定超导腔焊缝及iris附近表面是否存在缺陷，以便进一步进行腔的处理来改进腔的性能.     

Cold RF test and associated mechanical features correlation of a TESLA-style 9-cell superconducting niobium cavity built in China

The RF performance of a 1.3 GHz 9-cell superconducting niobium cavity was evaluated at cryogenic temperatures following surface processing by using the standard ILC-style recipe. The cavity is a TESLA-style 9-cell superconducting niobium cavity, with complete end group components including a higher order mode coupler, built in China for practical applications. An accelerating gradient of 28.6 MV/m was achieved at an unloaded quality factor of 4×10⁹. The morphological property of mechanical features on the RF surface of this cavity was characterized through optical inspection. Correlation between the observed mechanical features and the RF performance of the cavity is attempted.     

超导在加速器中的应用概况

文中简要回顾了世界上已建造的大型超导加速器,重点介绍未来的超导加速器方案,对超导新材料在加速器中的应用研究以及我国超导在加速器中的应用研究情况作了简要介绍.     

Investigation on the fabrication of the 3rd harmonic superconducting cavity for the SSRF storage ring

A third harmonic superconducting niobium cavity has been proposed for installation in the Shang-hai Synchrotron Radiation Facility (SSRF) storage ring to improve the Touschek lifetime. In order to investigate the feasibility of the superconducting cavity fabrication indigenously and the possibility to master the fabrica-tion techniques, cavities were fabricated from copper and niobium sheets by deep drawing and electron-beam welding, and a series of measurements, such as resonant frequency, shape dimensions and wall thickness, were carried out during this process. After analysis of various problems existing in the fabrication process, tech-nique improvements were proposed, and finally the precise shape as designed and resonant frequency within 1.2 MHz were achieved for the new completed cavities. In addition, full annealing was finally proved to be a good cure for niobium sheets' tearing up during deep drawing. By fabricating niobium cavities successfully, some problems to the next step were cleared. This paper introduces the process of cavity fabrication and its technique improvements towards forming, and the initial vertical test result of niobium cavity is also presented.     

Some superconducting and normal state properties of niobium nitride thin films

We have measured the temperature dependence of the resistance, the superconducting transition temperature, and the upper critical field of niobium nitride thin films. Our samples were made by sputtering in a nitrogen-argon ion beam. The pressure during deposition is typically one to two orders of magnitude lower than that of standard sputtering techniques.     

超导腔垂直测量系统中的磁屏蔽

简要介绍空间磁场对纯铌超导加速腔性能的影响,以及在超导腔垂直测量时对空间磁场进行有效屏蔽的方法.由于多数磁性材料对应力和温度变化非常敏感,而且国内缺乏在低温下相关磁屏蔽材料性能的数据,为此对8种国产铁磁和软磁材料在低温下的初始磁导率进行了测量,并给出了相应的测试结果.最后介绍了作者研制的1.3GHz超导腔垂直测量低温恒温器内置式磁屏蔽装置及其性能.     

Investigation on the fabrication of the 3rd harmonic superconducting cavity for the SSRF storage ring

A third harmonic superconducting niobium cavity has been proposed for installation in the Shanghai Synchrotron Radiation Facility （SSRF） storage ring to improve the Touschek lifetime. In order to investigate the feasibility of the superconducting cavity fabrication indigenously and the possibility to master the fabrica tion techniques, cavities were fabricated from copper and niobium sheets by deep drawing and electron-beam welding, and a series of measurements, such as resonant frequency, shape dimensions and wall thickness, were carried out during this process. After analysis of various problems existing in the fabrication process, technique improvements were proposed, and finally the precise shape as designed and resonant frequency within 1.2 MHz were achieved for the new completed cavities. In addition, full annealing was finally proved to be a good cure for niobium sheets＇ tearing up during deep drawing. By fabricating niobium cavities successfully, some problems to the next step were cleared. This paper introduces the process of cavity fabrication and its technique improvements towards forming, and the initial vertical test result of niobium cavity is also presented.