Dual-axes differential confocal microscopy with high axial resolution and long working distance

We discover that the slight transverse offset of a point detector results in a shift of the axial intensity response curve in a dual-axes confocal microscopy (DCM). Based on this, we propose a new dual-axes differential confocal microscopy (DDCM) with high axial resolution and long working distance, in which two point detectors are placed symmetrically about the collection axis. And a signal is obtained through the differential subtraction of two signals received simultaneously by the two point detectors. Theoretical analyses and preliminary experiments indicate that DDCM is feasible and suitable for the high precision tracing measurement of microstructures and surface contours.     

气相色谱-质谱法测定水中25种挥发性有机物及其在污水厂应急溯源中的应用

采用吹扫捕集-气相色谱-质谱法测定水中25种挥发性有机物的含量,并研究了其在污水厂应急溯源中的应用。25种挥发性有机物在一定的质量浓度范围内与其峰面积呈线性关系,方法的检出限(3.143s)在0.6~5.0μg·L-1之间。以空白样品为基体进行加标回收试验,所得回收率在91.6%~102%之间,测定值的相对标准偏差(n=6)在2.7%~4.6%之间。在一起污水厂冲击案例中,通过污水管网采样及污水样品分析,确定污染因子二氯甲烷,并根据二氯甲烷浓度变化快速锁定污染源头,确保污水厂出口水质达标。     

光学优化设计中一阶和二阶偏导数的解析求法

以复合函数的微分法则为基础,提出了光学设计中目标函数对结构参数一阶和二阶偏导数解析求导的方法,给出了相应的推导过程和计算实例。     

基于改进声线跟踪法的室内交通噪声动态模拟

对碰撞点的有效性判断是传统声线跟踪法的一个重要步骤,在计算复杂的室内空间问题时计算量较大,为解决这一问题采用了一种与空间剖分相结合的改进的声线跟踪法。将该方法与微观交通流仿真和车辆噪声排放模型进行结合,实现了道路交通噪声透过窗户在多连通室内空间传播的动态模拟。最后采用该方法对相同道路和交通流条件下不同建筑朝向的4种布局室内噪声进行动态模拟。分析了室内交通噪声的大小和分布与建筑物布局、窗户的朝向、窗户的形式和面积等因数之间的关系。结果表明:窗户正对道路的房间比窗户侧对道路的房间噪声高4～6 d B(A),房间内等效声级与窗户面积的对数成正比关系。     

An emerging NIR super-long persistent phosphor and its applications

Materials with the ability to persistently emit intense near-infrared (NIR) light after ceasing excitation are very useful in many fields. The persistent time is a vital parameter for successful applications. In this study, we developed an emerging NIR super-long persistent luminescent (PersL) material, Cr³⁺-activated magnetoplumbite oxide La(Zn/Mg)(Ga,Al)₁₁O₁₉:Cr³⁺, by doping Yb³⁺ as a new efficient electron trap and incorporating Al³⁺ to engineer the energy band. We show that fine control of the trap depth and density is the key underpinning for PersL enhancement. The title material emits intense PersL in the spectral range of 600–950 nm with a PersL time of more than 1,000 h. Furthermore, after undergoing such long-term decay, the NIR emission can be revived by photo-/thermo-stimulation. We demonstrate its potential uses in bioimaging, multilevel anti-counterfeiting, tracing, and positioning. This study provides insight into how energy band engineering manipulates electronic structures to achieve high-performance PersL. The new NIR persistent phosphor may be soon utilized in related applications.     

Topological pressure of continuous flows without fixed points

In this paper, we give the equivalent definitions of topological pressure for flows by using spanning sets, weakly spanning sets, strongly separated sets and tracing sets, respectively. We get an inequality between the topological pressures of Lipschitz conjugate flows, and prove that the topological pressure of expansive flows with tracing property can be described by its periodic orbits.     

粉状硝铵炸药示踪检测研究

用X射线荧光能谱法检测了含十二烷基苯磺酸铈（CDBS）和硬脂酸铈（CSA）的硝铵（AN）炸药（ANE）。根据含CDBS和CSA的AN炸药的典型X射线荧光能谱，提出了用稀土（XT）的Kd峰的逃逸峰作为检测AN炸药的特征峰，其值为6．11keV。考察了该逃选峰的信号强度（Is）与炸药中XT含量（x％）、探测距离（L）、探测时间（t）、炸药量（m）的关系，并列出相应的关系式，认为在XT含量不低于0．2％，检测时间不少于5s，AN炸药量不少于50g的情况下，该检测技术适合检测AN炸药。     

Pointwise Recurrent Dynamical Systems with Pseudo-orbit Tracing Property

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Prediction of the sound field into high-rise building facades due to its balcony ceiling form

This study presents the acoustic performance off tall building facades closed to roadway due to one of balcony configurations, namely ceiling, with an inclined form in terms of traffic noise reduction. Three inclined angles are tested (5,10, and 15°) with different balcony depths by using a Pyramid Tracing model developed by A. Farina. The results in terms of A-weighted sound pressure level reduction are expressed in free field into the balcony back wall. The protection level, defined as the difference in noise levels before and after inserting the proposed balcony form, has been used to assess the reduction offered by that configuration. A maximum reduction due to using these forms is obtained at higher floors and at balcony of 2 m depths and more. As a consequence of simulation results, it is found that the prediction of protection levels from 10th to 15th floor can be calculated from an empirical equation.