New progress on beam availability and reliability of PKU high intensity CW proton ECR ion source

The stability and reliability of an ion source and its beam availability are extremely significant for any accelerator,especially for those high current long term CW operation ones like ADS. Although the first high quality 306-hours continuous wave(CW) operating curve at 50 m A@35 ke V has been successfully obtained with a standard compact 2.45 GHz ECR ion source at Peking University(PKU), but the uncertainties that caused beam trips before are unacceptable during an accelerator real operation and should be eliminated. Meanwhile, no permission will be given when the beam power is upgraded from 50 m A@35 ke V to 50 m A@50 ke V. To improve the PKU CW proton source quality, several upgrades were done recently. After those improvements, a new long term CW proton beam experiment at 50 m A@50 ke V was carried out in June 2016. The total running time is 300.5 hours, including near 6 hours ion source preparation and 294 hours non-disturb continuous operation. Within the continuous 13 days operation, no beam-off happened, no spark was observed,no beam drop appeared, no interrupting action was needed, and only a few beam fluctuations caused by the air conditional failure occurred. Beam availability and reliability within the 294 hours is 100%. The root-mean-square(RMS) emittance of this 50 m A@50 ke V CW proton beam is about 0.186 π.mm.mrad. A careful inspection of the ion source was done after this long term operation and no obvious damage was found. The restart experimental results obtained after the ion source inspection prove the high repeatability of PKU PMECRIS. In addition, a 130-m A H+beam was obtained at 50 k V with duty factor of 10%(100 Hz/1 ms) with this source. Details will be presented in this paper.     

Beam transport design for a 1 MeV prototype dielectric wall accelerator

The beam transport design of a novel proton dielectric wall accelerator is introduced in this paper. The protons will be accelerated from 40 keV to nearly 1 MeV under an accelerating gradient that is as high as 20 MV/m. A consideration of the beam line as well as the transport simulation is presented. The influences of the injection timing jitter and the accelerating pulse timing jitter are also discussed.     

Understanding hydrogen plasma processes based on the diagnostic results of 2.45 GHz ECRIS at Peking University

Optical emission spectroscopy(OES), as a simple in situ method without disturbing the plasma, has been performed for the plasma diagnosis of a 2.45 GHz permanent magnet electron cyclotron resonance(PMECR) ion source at Peking University(PKU). A spectrum measurement platform has been set up with the quartz-chamber electron cyclotron resonance(ECR) ion source [Patent Number: ZL 201110026605.4] and experiments were carried out recently. The electron temperature and electron density inside the ECR plasma chamber have been measured with the method of line intensity ratio of noble gas. Hydrogen plasma processes inside the discharge chamber are discussed based on the diagnostic results. What is more, the superiority of the method of line intensity ratio of noble gas is indicated with a comparison to line intensity ratio of hydrogen. Details will be presented in this paper.     

Beam transport design for a 1 MeV prototype dielectric wall accelerator

The beam transport design of a novel proton dielectric wall accelerator is introduced in this paper. The protons will be accelerated from 40 keV to nearly 1 MeV under an accelerating gradient that is as high as 20 MV/m. A consideration of the beam line as well as the transport simulation is presented. The influences of the injection timing jitter and the accelerating pulse timing jitter are also discussed.     

低能质子束脉冲踢束器的物理设计

电子回旋共振(ECR)质子源产生的脉冲质子束脉宽通常在ms或亚ms量级,高梯度加速结构要求注入的质子束脉宽为100 ns或更短,需要一个脉冲踢束器将大部分不需要的束流踢开,留下所需的短脉冲质子束。设计的踢束器采用静电偏转方法,针对在研ECR质子源的束流参数,设计了脉冲踢束器的结构尺寸,使用ANSYS软件计算了踢束器的静电场分布情况,利用软件内置的CMATRIX宏提取了结构电容的数据,给出了对脉冲踢束电源的参数要求,讨论了踢束脉冲上升沿和产生的束流脉冲上升沿的对应关系。     

呋喃唑酮代谢物单克隆抗体制备及酶联免疫吸附分析方法

本研究针对呋喃唑酮代谢物(AOZ),设计合成了系列半抗原,进一步通过偶联牛血清白蛋白(BSA)免疫Balb/c小鼠、细胞融合、筛选和亚克隆等过程成功获得了源于新颖半抗原H3的具有高亲和力(亲和力常数6.68× 1010L/mol)和高特异性(与其它功能类似物交叉反应小于0.1％)抗AOZ单克隆抗体.同时,基于设计合成的系列同/异源半抗原/包被抗原,考察了不同结构包被原对ELISA方法灵敏度的影响.另外,采用最佳的特征结构异源包被原H5 -OVA,建立了以对硝基苯甲醛(p-NP)为衍生剂的AOZ间接竞争ELISA(icELISA)和直接竞争ELISA(deELISA)检测方法.结果表明:icELISA模式的AOZ检测IC50为0.503 μg/L,定量检测线性范围(IC20～IG80)为0.06～14.0 μg/L,检出限(IC10)达0.017 μg/L; dcELISA模式的AOZ检测IC50为1.19 μg/L,定量检测线性范围为0.14～23.6 μg/L,检出限为0.056 μg/L.两种方法对AOZ的检测灵敏度和定量线性范围均达到相关检测限量要求,可满足不同需求的实际样品检测.     

低能强流离子注入丁腈橡胶的表面改性(英文)北大核心CSCD

丁腈橡胶是一种广泛使用的合成橡胶,目前应用于各种非轮胎制品。离子注入被认为是一种提高丁腈橡胶表面特性的有效手段,比如降低摩擦系数、提高耐抗性等。最近,为了理解辐照效应对于硫化橡胶的功能特性如摩擦系数和硬度等的影响,利用北京大学离子源测试平台将N^+和H^+注入丁腈橡胶表面进行研究。离子注入完成以后,对丁腈橡胶表面的摩擦系数、硬度、耐热老化性能、摩擦特性以及耐磨损性能进行了分析。     

A fast emittance measurement unit for high intensity DC beam

A combined unit, which has the ability to measure the current and emittance of the high intensity direct current(DC)ion beam, is developed at Peking University(PKU). It is a multi-slit single-wire(MSSW)-type beam emittance meter combined with a water-cooled Faraday Cup, named high intensity beam emittance measurement unit-6(HIBEMU-6). It takes about 15 seconds to complete one measurement of the beam current and its emittance. The emittance of a 50-mA@50-kV DC proton beam is measured.     

高效液相色谱-串联质谱法测定多种农产品中杀草强的残留量

建立了采用高效液相色谱-串联质谱法(HPLC-MS/MS)检测多种农产品中杀草强残留量的方法。根据样品基质不同,分别采用25%丙酮水溶液(针对小麦、鱼、肉和肝脏样品)、1%乙酸酸化的25%丙酮水溶液(针对玉米和花生样品)、1%乙酸水溶液(针对金银花、姜粉、花椒粉和茶叶样品)及1%乙酸水溶液和二氯甲烷(针对苹果、菠萝、菠菜、胡萝卜和紫苏叶）进行提取,然后依次采用二氯甲烷萃取、PCX或ENVI-Carb固相萃取柱净化后,进行HPLC-MS/MS测定,外标法定量。在0.005～0.1 mg/kg范围内,杀草强的峰面积与其质量浓度有良好的线性关系,相关系数为0.9997。对上述15种不同种类的农产品进行添加回收,回收率为67.5%~98.1%,相对标准偏差为1.0%~9.8%。苹果、菠菜、紫苏叶、玉米、姜、鱼和肉等样品的定量限为0.01 mg/kg,茶叶、金银花、花椒粉的定量限为0.02 mg/kg。该方法的灵敏度、准确度和精密度均符合农药残留测定的技术要求。     

A miniaturized 2.45 GHz ECR ion source at Peking University

A miniaturized 2.45 GHz permanent magnet electron cyclotron resonance(PMECR) ion source, which has the ability of producing a tens-m A H+beam, has been built and tested at Peking University(PKU). Its plasma chamber dimension is Φ30 mm×40 mm and the whole size of the ion source is Φ180 mm×130 mm. This source has a unique structure with the whole source body embedded into the extraction system. It can be operated in both continuous wave(CW) mode and pulse mode. In the CW mode, more than 20 m A hydrogen ion beam at 40 k V can be obtained with the microwave power of 180 W and about 1 m A hydrogen ion beam is produced with a microwave power of 10 W. In the pulse mode, more than50 m A hydrogen ion beam with a duty factor of 10% can be extracted when the peak microwave power is 1800 W.