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使用CTAB作为软模板,水热处理柚子皮,再以碳化和KOH活化过程得到了分级多孔碳(HPC),这种分级多孔碳材料的比表面积高达1 813 m~2·g~(-1),相比于没有水热步骤制备的多孔碳(PC),拥有更加丰富的介孔结构和更大的比表面积。XPS分析结果表明HPC的氧掺杂量更高,会比PC贡献更大的赝电容。三电极测试体系中,HPC的比电容达到285 F·g~(-1)(0.5 A·g~(-1),1 mol·L~(-1)KOH)。同时,组装的两电极对称超级电容器拥有很好的倍率性能,循环12 000次充放电后,比电容依旧保留99%。HPC拥有这样优异的性能归结于较大的比表面积,高氧掺杂量和合理的孔径分布的协同作用。 相似文献
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The relation between the generalised Eshelby integral and the generalised BCS and DB modelsvspace1mm 下载免费PDF全文
The generalised BCS dislocation group model and the generalised DB atomic cohesive force zone model have obtained the same results on nonlinear fracture study of some one-, two- and three-dimensional quasicrystals. This work reveals some inherent connection between the two models, and finds that their common basis is the generalised Eshelby integral based on the generalised Eshelby energy--momentum tensor for quasicrystals. Further applications of the theory in solving nonlinear fracture problems of the materials are also discussed. 相似文献
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为了发现新型姜黄素类抗肿瘤先导化合物,通过1,3-偶极环加成反应合成了14个螺杂环单羰基姜黄素类似物.该反应利用无需加催化剂的"一锅煮"方法合成,具有环境友好的优点.所有化合物结构经ESI-MS、ESI-HRMS和1H NMR确认,通过X衍射确证B6的晶体结构为单斜晶系,该类化合物的合成具有良好的区域选择性和立体选择性.通过噻唑兰(MTT)法测定所有化合物对人胃癌细胞SGC-7901、神经胶质瘤细胞U251、人大细胞肺癌细胞株NCI-H460的增殖抑制活性,部分化合物表现出了较好的活性.其中B1、B6、B7和B11对三种肿瘤细胞均表现出较好的抗肿瘤活性,而对正常人肝细胞HL-7702显示了相对较低的细胞毒性.化合物B1和B7均能明显诱导凋亡相关蛋白含半胱氨酸的天冬氨酸蛋白水解酶3(caspase3)和多聚ADP-核糖聚合酶(PARP)的活化,诱导肿瘤细胞发生凋亡.所合成的螺杂环单羰基姜黄素类似物为新型的抗肿瘤化合物,该类化合物可能在靶向抗肿瘤药物研发方面具有较好的研究前景. 相似文献
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The relation between the generalised Eshelby integral and the generalised BCS and DB models 下载免费PDF全文
The generalised BCS dislocation group model and the generalised DB atomic cohesive force zone model have obtained the same results on nonlinear fracture study of some one-,two-and three-dimensional quasicrystals.This work reveals some inherent connection between the two models,and finds that their common basis is the generalised Eshelby integral based on the generalised Eshelby energy-momentum tensor for quasicrystals.Further applications of the theory in solving nonlinear fracture problems of the materials are also discussed. 相似文献
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介绍了采用CAN总线数据传输方式的系统中,光电编码器CAN总线接口的设计与应用。首先,设计了由单片机、独立CAN总线控制器SJA1000、CAN总线收发器TJA1050及高速光耦TLP113等构成的光电编码器CAN总线接口硬件电路;然后,介绍了光电编码器CAN总线接口的软件设计,包括初始化的设计、CAN总线报文接收及发送的设计;最后,通过周立功公司的“USBCAN1”型号CAN总线接口卡验证了该光电编码器CAN总线接口设计的可行性。实验中采用1米长的屏蔽双绞线作为传输介质,通信速率为800kbps;结果表明:带有CAN接口的光电编码器克服了传统的通信线路的缺点,具有更高的实时性、可靠性且通信速率高、传输距离长、抗干扰能力强,更加适用于自动化测量和控制系统。 相似文献
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A model on the coexisting phase of quasicrystal-crystal is proposed,with which we concretely investigate the interface effects for coexisting phases of one-dimensional orthorhombic quasicrystal-isotropic crystal and three-dimensional icosahedral quasicrystal-cubic crystal.The phason strain fields which play an important role in some processes are determined.Some factors affecting the strain fields,e.g.,the material constants of phonon,phason,phonon-phason coupling of the quasicrystal and the elastic modulus and the size of the crystal are also explored. 相似文献
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