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1 INTRODUCTION Substituted 1,2,4-triazines represent an important class of nitrogen-containing heterocycles. The 1,2, 4-triazine core is a versatile synthetic platform to access a wide range of condensed heterocyclic ring systems via intramolecular Diels-Alder reactions with a vast array of dienophiles[1~5]. In addition, 1,2, 4-triazines have been associated with diverse activi- ties such as antihypertension and inhibition of pla- telets[6] and antiinflammatory[7], and been a key com- po… 相似文献
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建立了同时检测化妆品中溴酸盐和碘酸盐的离子色谱-柱后衍生紫外检测器定量分析方法。样品用水提取,经RP柱净化,采用IonPac AS11-HC色谱柱分离,以EG40自动淋洗液发生器生成的KOH为淋洗液梯度洗脱,溴化钾、亚硝酸钠为衍生试剂,二极管阵列检测器检测,外标法定量。结果表明:该方法在2.0~1 000 mg/kg范围内线性关系良好(r≥0.999 8);加标回收率为84%~99%;相对标准偏差小于2%。方法简单、快速、选择性强,可用于化妆品中碘酸盐和溴酸盐的测定。 相似文献
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The title compound, ethyl 5-amino-1-[(5'-methyl-1'-t-butyl-4'-pyrazolyl)carbonyl] -3-methylthio-1H-pyrazole-4-carboxylate 5, has been synthesized by the treatment of 4 with ethyl 2-cyano-3,3-dimethylthioacrylate, and its crystal structure was determined by X-ray diffraction method. The crystal belongs to monoclinic, space group P21/c with a = 12.194(4), b = 12.909(4), c = 11.607(4) (A), β= 90.183(5)°, V = 1827.2(10) (A)3, Mr = 365.45, Z = 4, Dc = 1.328 g/cm3, μ = 0.203 mm-1, F(000) = 776, R = 0.0586 and wR = 0.1558. Preliminary bioassays indicated that the title compound shows fungicidal and plant growth regulation activities. 相似文献
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对于任意素数p,本文利用解析的方法、模p的勒让德符号的性质以及特征和的估计,研究了模p的连续二次剩余的三元数(简称3-CQR)以及连续二次非剩余的三元数(简称3-CQN)的分布性质.本文给出当p≡3或7 (mod 8)时3-CQR和3-CQN的个数S1(p)以及S2 (p)精确的计算公式,并且给出p≡1或5 (mod 8)时,S1 (p)以及S2(p)的渐近公式.类似地,本文研究了间隔为2的二次剩余的三元数并给出其个数的计算公式.作为应用,本文利用3-CQR构造了有限域Fp中9度的平方幻方. 相似文献
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本文以实验课教学为例就如何培养学生能力进行了探讨;从实验教材的处理和实验课的指导两个方面入手,注重培养学生的观察与分析能力、理论联系实际的能力和解决实际问题的能力,拓宽学生思维,夯实基本功。 相似文献