不同窑口古代青瓷的产地特征的中子活化分析

产地属性是科学鉴别遗址和墓葬中出土的古陶瓷烧制产地的重要依据.用仪器中子活化（INAA）有损分析了浙江寺龙口越窑、江西洪州窑和陕西耀州窑出土的古瓷碎片样品,通过实验数据的统计分析,结果表明3个窑口古瓷的元素组成具有各自的特征,它们之间具有可以区分的依据,寺龙口越窑与南方江西洪州窑的制胎原料关系较近,与北方陕西耀州窑的关系较远.这些试验结果将为古陶瓷地研究提供重要参数.Provenance characteristic is an important scientific parameter to identify ancient porcelain wares unearthed from sites and graves.The porcelain samples of Si Long Kou kiln of Zhejiang Province,Hong Zhou kiln of Jiangxi Province and Yao Zhou kiln of Shanxi Province have been analyzed with neutron activation analysis(NAA) in this paper.The experimental data were studied with statistic methods.The results show that the chemical compositions of porcelain body samples for three kilns were different. The difference was been able identified. The body materials of both Si Long Kou Yue kiln and Hong Zhou kiln of Jiangxi were similar. The samples of Yao Zhou kiln in north of China existed obvious difference.     

药物代谢转化研究及其进展

扼要地叙述了近年国内外药物代谢转化研究方法及代谢物分离分析新技术。     

历代洪州窑古瓷的元素组成特征的中子活化分析研究

对江西洪州窑从东汉晚期至晚唐五代8期400个瓷胎样品进行了中子活化分析, 分析结果显示碱金属元素Na和Rb、 碱土金属元素Ba及Fe等作为胎的助熔剂元素随年代的变化趋势相似, 都呈现出两头高中间低的U字形变化规律, 其中Fe作为呈色元素, 其含量的高低与瓷胎颜色的深浅是一致的. 分析结果还揭示洪州窑的发展与衰落以及窑址的不断变迁可能都与制瓷原料的发现与消耗有关. 对分析数据进行主成分分析, 可以将不同时期烧制的瓷胎样品大致分为5组: （1）东汉晚期东吴时期; （2）两晋和南朝时期; （3）隋代; （4）初唐和盛唐时期; （5）晚唐五代时期. 400 sherds were collected from Hongzhou Kiln covering 8 periods from Eastern Han to Late Tang Dynasty/the Five Dynastied and their bodies were analysed by NAA. The results show that the elemental contents in different samples are quite distinct, even for those in the same period. It means no single element can be used as “fingerprint” to distinguish the period. The curves of the contents of Na, Rb, Ba and Fe varying with time are very similar, like “U” shape. As a colorant element, the content of Fe is consistent with the color of the body. The higher content of Fe, the more dark of the body. The outcome of principal component analysis (PCA) indicate that most of the sherds can be classified into 5 groups: (1) Eastern Han & Eastern Wu; (2) Western Jin, Eastern Jin and Southern Dynasties; (3) Sui; (4) Early Tang and Middle Tang; (5) Late Tang & Five Dynasties.