SEPARATING SCN~- FROM DESULPHURIZATION WASTE SOLUTION OF COCKING PLANT BY D241 RESIN

1. INTRODUCTION In the process of coking plant, about 30%~35% sulfur is transformed to H2S and some other sulfide, which form impurity in coal gas together with NH3 and HCN. Only 0.1% H2S containing in air can lead to die, so it is very important to carry on desulphurization and decyanation with coal gas [1~3]. Currently desulphurization and decyanation craft technique have Dry Oxidation Technology, Wet Oxidation Technology and Liquid Absorption Technology [2] three main kinds. The…     

平面交叉玻璃波导型微透镜阵列光学性能研究

介绍了平面交叉玻璃光波导型半球形微透镜阵列的制作方法.利用积分形式的光线方程式讨论了半球形微透镜的光学特性,得到了半球形微透镜的光线轨迹方程式和焦距表示式,理论结果与实验数据是一致的.     

关于非光滑不变凸多目标规划的Wolfe型对偶

本文讨论定义在Banach空间上的,既具有等式约束又具有不等式约束的,非光滑(F,P)不变凸多目标规划的Wolfe对偶性,Mond-Weir型对偶性可类似讨论之。     

LARGE-SIGNAL SIMULATIONS OF A GYROTRON TRAVELING-WAVE AMPLIFIER WITH A MODE-SELECTIVE INTERACTION CIRCUIT

A self-consistent nonlinear theory is used to analyze the saturated performances of a Ka-band gyrotron traveling wave amplifier (gyro-TWA) operating at the fundamental with a mode-selective interaction circuit involving a tapered vane-slot mode converter. The amplifier is predicted to generate 140 kW saturated output power with 33.3% efficiency, a saturated gain of 33dB, and a 3dB bandwidth of 2.7 GHz (8%) for a 70 kV, 6A electron beam with a velocity ratio of 1.0 and an axial velocity spread of 5%.     

非本征型法布里-珀罗干涉仪光纤布拉格光栅应变温度传感器及其应用

介绍了光纤布拉格光栅非本征型法布里珀罗干涉仪集成复用传感器的结构、应变和温度同时监测的原理 ;观察到光纤布拉格光栅反射谱和非本征型法布里珀罗干涉仪干涉谱间的串扰 ,用 3dB带宽平均波长法减小了该串扰 ,提高了测量精度 ;将该传感器应用于三维编织复合材料的应变及温度同时监测。实验结果表明温度精度为± 1℃ ,应变精度为± 2 0 μ ,可满足实际应用的要求     

微型圆光栅刻划偏心量的控制

对微型圆光栅刻划偏心误差问题进行了讨论。提出了微型圆光栅刻划时偏心调试误差的公差范围。     

Studies of a new series of ion-pair complexes [Mo(dtc)_4][Ln(dtc)_4] (Ln=La-Er,exp.Pm)

A new series of ion-pair complexes [Mo(dtc)4][Ln(dtc)4] (Ln=La-Er, exp. Pm) were synthesized from MoCl5, LnCl3 and Nadtc in anhydrous methanol. The crystal structures of the four complexes, [Mo(dtc)4][Ln(dtc)4] (Ln=Nd, Sm, Ho and Er) have been determined by X-ray diffraction. Spectroscopic properties of all these complexes are also discussed here.     

Studies of some new bioactive acrylic esters

Four typical bioactive esters of acrylic monomers, N-p-acryloxybenzoyloxysuccinimides, 3-ac-ryloxy-4-oxo-3,4-dihydro-1,2,3-benzotriazines, N-acryloxy-5-norbornene-2,3-dicarboximides, and I-p-acryloxybenzoyloxybenzotriazoles, were Synthesized and polymerized as reactive polymers. Twelve new monomers were prepared by coupling acrylic acid, methacrylic acid, p-acryloxybenzoic acid, or p-methacryloxybenzoic acid with four N-hydroxy compounds such as N-hydroxysuccinimide (HOSu), 3-hydroxy-4-oxo-3,4-dihydro-1,2,3-benzotriazine (HOObt), N-hydroxy-5-norbornene-2,3-dicarboximide (HONB), and I -hydroxybenzotriazole (HOBT) in the presence of dicyclohexylcarbodimide. All monomers polymerized readily in solution with azobisisobutyronitrile (AIBN) as free radical initiator. The resulting reactive polymers with reactive ? OSu, ? OObt, ? ONB, or ? OBT group on the side chain are equally reactive toward n-butylamine at room temperature in the formation of corresponding polyacrylamides. Reactive polymers were used to immobilizetrypsin. It has been found that poly(N-p-methacryloxybenzoyloxy-5-norbornene-2,3-dicarboximide)-trypsin matrix had high activity around three times that of the poly(N-methacryloxy-5-norbornene-dicarboximide)-trypsin matrix. It is proposed that this activity may be due to the presence of a long spacer arm with a hydrophobic and rigid benzene ring between the ligand and matrix. The reactive poly(N-p-methacryloxybenzoyloxysuccinimide-p-methacryloxybenzoic acid) copolymer was used to immobilize the serum protein. This immobilized protein was a hopeful bioactive solid immunoadsorbent.     

An Efficient and Green Synthesis of 5-Oxo-5, 6, 7, 8-tetrahydro- 4H-benzo-[b]-pyran Derivatives Promoted by InCl_3·4H_2O Under Microwave Irradiation

Construction of tetrahydropyran rings has attracted a great deal of interests in organic synthesis in recent years1, since tetrahydropyran moiety constitutes a structural unit in a number of natural products2. In addition, tetrahydropyran derivatives possess wide range of biological activities and pharmacological properties, such as anticancer activity3 and antihypersensitivity4. Many methods for the preparation of such compounds have already been developed5. Among them, condensation of α, β…     

Synthesis and Characterization of a Novel Biomaterial： Maleic Anhydride-modified Poly（dl-lactic acid）

A novel modified poly(dl-lactic acid) (PDLLA) was obtained by covalently grafting of maleic anhydride onto the backbone of PDLLA, attempting to improve PDLLA‘s hydrophilicity and cell affinity and to provide reactive groups for further chemical modification. FTIR, ^13 C NMR and DSC were used to characterize the maleic anhydride-modified PDLLA.