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991.
In this paper the reaction of substituted β-nitrostyrene with O,O-dialkyl phosphite under cocatalysis of trimethylsilyl chloride (TMS-C1) and triethylamine (or other acidbinding agent) has been first studied and the new cyclization reaction leading to the formation of product Ⅱ, as a new class of derivatives of 1-hydroxyindoles, difficultly accessible or inaccessible with usual methods has been observed. In the related reaction it is surprising that when the Arbuzov rearrangement occurs under mild conditions, the addition, reduction and cyclization as a one-pot reaction take place simultaneously with the formation of products Ⅰ, Ⅱ, Ⅲ. By controlling the reaction conditions the products were formed almost in specificity, and thus the most interesting cyclic products Ⅱ_(a-h) containing phosphorus-carbon bond were obtained. Their structures were confirmed by elemental analysis, IR, ~1H or ~(31)p NMR and MS spectra. The crystal structure of representative compound Ⅱ_h was determined by X-ray diffract 相似文献
992.
993.
The total reaction cross sections (TRCSs) of^29S ^28Si have been measured at intermediate energies. An obvious enhancement in TRCS of ^29S is observed as compared with its neighbouring nuclei. The TRCSs of ^29S ^28Si arecal culated with the modified Glauber theory in the optical limit and few-body approaches. The different factor d as a possible measure of halo appearance is deduced from the experimental and theoretical data. It is well accepted that ^27p is a proton halo nucleus. Although not as anomalous as ^27p, the different factor d of ^29S is obviously larger than that of its neighbouring isotones of N = 13. This result indicates that a moderate proton halo may exist in ~9S nucleus. We calculate the total reaction cross sections for ~9S with the modified Glaubertheory as a function of incident energy and compare the results with those for 2rSi which is a core nucleus 0f29S.The measured TRCSs of 27Si4-2SSi can be described to be satisfactory by the modified Glauber theory of theoptical limit approach. Although a diffused nuclear density distribution is used, the theories still inadequatelypredict the experimental TRCSs of 29S4-2SSi, which further indicates the possibility of proton halo in 29S. 相似文献
994.
GMPLS网络中约束最短路径优先算法研究 总被引:4,自引:0,他引:4
针对GMPLS网络中求解最短路径问题,提出了一种具有共享风险链路约束的启发式约束最短路径优先路由算法,对该算法的有效性和可靠性进行了比较全面的仿真测试,仿真结果显示此算法提高了网络资源的利用率,减少了网络的阻塞,同时降低了链路失效时的风险,提高了网络的强壮性和可靠性. 相似文献
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996.
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998.
Based on modern differential geometry, the symplectic structure of a Birkhoffiansystem which is an extension of conservative and nonconservative systems is analyz ed. Anone-dimensional damped vibration is taken as an ilhustrative example and an integralinvariant of Poincaré's type is found. 相似文献
999.
1000.