费托反应本征动力学中合成气分压对反应速率的影响

利用高通量动力学反应器测量了本征条件下钴基费托催化剂上反应物消耗速率rCO和产物生成速率rCH4随固定床床层的分布,并考察了它们在不同入口分压(p0CO,p0H2)条件下的变化.结果表明,入口氢碳比(H/C)0=p0H2/p0CO为影响速率的敏感外部变量,反应速率随(H/C)0的增加而加快;而合成气总压p0H2+CO则...     

非水溶剂热法制备(001)面暴露的F/TiO2纳米晶及其光催化活性

采用非水体系溶剂热法制备了(001)面暴露的锐钛矿相F/TiO2纳米光催化剂.结果表明,F的掺杂对TiO2纳米单晶的形成影响很大.一方面,F离子作为晶面导向剂稳定(001)晶面,形成(001)面暴露的锐钛矿相TiO2;另一方面,F离子也起到稳定剂作用,抑制纳米粒子的快速生长.以光催化降解甲基橙为模型反应比较了不同F/T...     

琥乙红霉素分子印迹聚合物微球的制备及表征

以琥乙红霉素为模板分子,甲基丙烯酸为功能单体,乙二醇二甲基丙烯酸酯为交联剂,采用悬浮聚合法制备得到了平均粒径约为60μm的琥乙红霉素分子印迹聚合物微球(MIPs),并用扫描电镜对其表面形貌进行了表征。考察了琥乙红霉素分子印迹聚合物的印迹效果,研究了琥乙红霉素分子印迹聚合物的动力学吸附特性。比较了MIPs对琥乙红霉素及其它3种抗生素的吸附情况。结果表明,制备得到的琥乙红霉素分子印迹聚合物微球对琥乙红霉素具有最好的吸附能力,显示出MIPs具有高的选择性。     

频移反馈Nd∶YLF激光软阈值实验与模拟计算

实验和模拟计算均表明：在无注入种子激光的频移反馈Ｎｄ∶ＹＬＦ激光系统中，不存在软阈值，而当注入种子激光时，出现软阈值特性，实验还发现：随着种子激光功率增大，软阈值变得更加明显。     

Particle-core coupling in 141Nd

High-spin states in 141Nd have been studied using in-beam γ-ray spectroscopic techniques via the 130Te(16O, 5nγ)141Nd reaction. The level scheme of 141Nd has been extended up to an excitation energy of 7614.5 kev including 12 new γ rays deexciting 15 new levels. According to particle-vibrator coupling and semi-empirical shell model calculations, the level structure of 141Nd can be well interpreted by coupling an h11/2 neutron-hole to the respective excited states in 142Nd core.     

Parameter analysis of a photonic crystal fiber with raised-core index profile based on effective index method

Photonic crystal fibers (PCFs) with a stepped raised-core profile and one layer equally spaced holes in the cladding are analyzed. Using effective index method and considering a raised step refractive index difference between the index of the core and the effective index of the cladding, we improve the characteristic parameters such as numerical aperture and V-parameter, and reduce its bending loss to about one tenth of a conventional PCF. Implementing such a structure in PCFs may be one step forward to achieve low loss PCFs for communication applications.     

MgxB2起始成分对不可逆场和临界电流密度的影响

我们用固相反应法成功合成了MgrB2（0．5≤x≤1．3）系列样品，并对其结构，临界电流密度（Jc）和不可逆场（Hirr）进行了研究．实验结果表明，随着x增大晶格常数α逐渐增大，而晶格常数c在x=0．9左右达到最大值．所有x〉0．5的样品在零场下的Jc值都在10^6A／cm^2左右．然而在高磁场下，Mg缺位的样品的Jc值要比Mg富足的样品的Jc值大．20K时．Mg0．8B2样品的不可逆场达到最大值5．2T，比MgB2样品要高出0．8T．研究表明，高磁场下Hirr和Jc的增大可能与MgB4纳米粒子的形成有关．     

Amplification effect on stimulated Brillouin scattering in the S-band forward G652 fiber Raman amplifier

The amplification effects on forward and backward stimulated Brillouin scattering (SBS) lines in the forward pumped S-band distributed G652 fiber Raman amplifier (FRA) have been studied. There is a pump threshold power of Stokes backward stimulated Brillouin scattering (B-SBS) line in the forward pumped G652 FRA, it is about 1 mW. The Stokes B-SBS lines are amplified by FRA and fiber Brillouin amplifier (FBA). The gain of amplification is given as Ga = GR · GB where GR is Raman gain and GB is Brillouin gain. In experimental work, the saturation gain of the first order Stokes backward SBS line is about 58 dB and the saturation gain of 25-km G652 forward FRA is about 25 dB, so the gain of FBA is about 33 dB. The forward stimulated Brillouin scattering (F-SBS) is generated and amplified in S-band G652 FRA. The stimulated threshold powers of the forward first order Stokes SBS (SB1-), second order Stokes SBS (SB2-), and third order SBS (SB3-) in the forward pumped FRA are 2.3, 1.6, and 1.6 mW, respectively. In experimental work, the saturation gains of SB1-, SB2-, and SB3- are about 38, 62, and 60 dB, respectively. The saturation Raman gain of 25-km G652 forward FRA is about 8.8 dB, so the Brillouin gains of SB1-, SB2-, and SB3- are about 29.2, 53.2, and 51.2 dB, respectively. The forward and backward cascaded SBS lines have been observed.     

HL-2A装置电子回旋传输系统

近年来，电子回旋共振加热和驱动在许多装置上得到应用，例如：Tore Supra。JT-60U和Heliotron J，与其它加热和驱动方法相比，它具有以下优点。电子回旋波能以能量集中的高斯模式注入，产生高度集中的功率沉积，能进行理想的MHD不稳定性控制。