Silica-based microcavity fabricated by wet etching

Silica whispering gallery mode(WGM) microcavities were fabricated by the buffered oxide etcher and potassium hydroxide wet etching technique without any subsequent chemical or laser treatments. The silicon pedestal underneath was an octagonal pyramid, thus providing a pointed connection area with the top silica microdisk while weakly influencing the resonance modes. The sidewalls of our microdisks were wedge shaped, which was believed to be an advantage for the mode confinement. Efficient coupling from and to the 60 μm diameter microdisk structure was achieved using tapered optical fibres, exhibiting a quality factor of 1.5×10~4 near a wavelength of 1550 nm. Many resonance modes were observed, and double transverse electric modes were identified by theoretical calculations. The quality factor of the microdisks was also analysed to deduce the cavity roughness. The wet etching technique provides a more convenient avenue to fabricate WGM microdisks than conventional fabrication methods.     

Lectin法分析uNK细胞在人妊娠母胎界面的分布变化

通过Lectin法分析uNK细胞在人妊娠早、晚期母胎界面的分布变化。结果发现:(1)在妊娠早期的蜕膜中,uNK细胞主要有两种形式,一种是成熟uNK细胞,细胞体积较大,胞浆和胞膜呈现强烈的棕黄色染色,分布于蜕膜的血管中。另一种是未成熟uNK细胞,细胞体积较小,胞核呈现黄色染色,分布于蜕膜细胞之间。(2)在妊娠早期的绒毛组织中,uNK主要是未成熟uNK,分布于绒毛间质之间。(3)与妊娠早期蜕膜的uNK细胞数相比,至妊娠晚期,蜕膜的uNK细胞数量明显减少(P<0.01)。(4)在妊娠晚期,绒毛组织不表达uNK细胞。结论:uNK细胞主要分布于子宫蜕膜组织,且随着妊娠的进展,其表达数量明显下降。这种时空性的表达变化可能与其在调控滋养层细胞的侵袭、血管重建及免疫耐受方面密切相关。     

GaN基蓝光VCSEL的制备及光学特性

利用金属有机物气相沉积技术(MOCVD)在(0001)蓝宝石衬底上生长了Ga N基垂直腔面发射激光器(VCSEL)的多量子阱腔层结构。X射线衍射测量显示该多量子阱具有良好周期结构和平整界面。运用键合及激光剥离技术将该外延片制作成VCSEL,顶部和底部反射镜为极高反射率的介质膜分布布拉格反射镜(DBR)。在室温、紫外脉冲激光的泵浦条件下,观察到了VCSEL明显的激射现象,峰值波长位于447.7 nm,半高宽为0.11 nm,自发辐射因子约为6.0×10-2,阈值能量密度约为8.8 m J/cm2。在大幅度降低制作难度的情况下,得到目前国际最好结果同样数量级的激射阈值。降低器件制作难度有利于制备的重复性,有利于器件的产品化。     

Influence of barrier thickness on the structural and optical properties of InGaN/GaN multiple quantum wells

The structural and optical properties of InGaN/GaN multiple quantum wells(MQWs) with different barrier thicknesses are studied by means of high resolution X-ray diffraction(HRXRD), a cross-sectional transmission electron microscope(TEM), and temperature-dependent photoluminescence(PL) measurements. HRXRD and cross-sectional TEM measurements show that the interfaces between wells and barriers are abrupt and the entire MQW region has good periodicity for all three samples. As the barrier thickness is increased, the temperature of the turning point from blueshift to redshift of the S-shaped temperature-dependent PL peak energy increases monotonously, which indicates that the localization potentials due to In-rich clusters is deeper. From the Arrhenius plot of the normalized integrated PL intensity, it is found that there are two kinds of nonradiative recombination processes accounting for the thermal quenching of photoluminescence,and the corresponding activation energy(or the localization potential) increases with the increase of the barrier thickness.The dependence on barrier thickness is attributed to the redistribution of In-rich clusters during the growth of barrier layers,i.e., clusters with lower In contents aggregate into clusters with higher In contents.     

激光诱导p-GaN掺杂对发光二极管性能改善的分析

采用激光诱导掺锌的方法提高了常规GaN基外延片p-GaN层的空穴浓度,并将它制备成小功率白光发光二极管(LED).对其光电性能做了详细的测量并进行了加速老化实验和分析.结果表明,与常规LED相比,经过激光诱导p-GaN层掺锌LED的光电性能获得了明显改善:正向工作电压VF从3.33V降到3.13V,串联电阻从30.27Ω降到20.27Ω,室温下衰退系数从1.68×10-4降到1.34×10-4,老化1600h后的反向漏电流从超过0.2μA降为不超过0.025μA,器件的预测寿命延长了41%.器件光电性能改善的主要原因是激光诱导掺锌使LED的p-型欧姆接触改善和热阻降低所致.     

12C6+束辐照引起的实验猪皮肤急性损伤反应的研究

探讨了正常皮肤对重离子辐照急性损伤反应的耐受性, 为重离子治癌临床应用提供安全性检测的实验依据。实验前10 min, 实验猪肌肉注射复方氯胺酮1.2 mg/kg进行麻醉, 然后在兰州重离子研究装置（HIRFL）辐照终端利用12C6+束照射, 辐照剂量分别为0, 12, 21和27 Gy, 辐照分3次完成, 剂量率约为1.2 Gy/min, Bragg峰区照射, 辐照后每隔7 d对照射野拍照并活检取样, 做HE组织病理学观察。不同剂量12C6+离子束辐照实验猪皮肤后, 皮肤外观反应随辐照剂量增大而加快, 表现为肿胀和色素沉积等; 皮肤组织结构的变化明显, 上皮细胞排列紊乱、 萎缩、 空泡变性; 基本恢复正常所需时间也越长, 且都存在明显的剂量效应关系。结果表明, 辐照剂量范围为0—27 Gy时, 重离子对正常皮肤的辐照是安全的。The tolerance of the normal skin to the acute radiation injury reaction induced by heavy ion beams has been studied experimentally. The experimental pigs were injected with 1.2 mg/kg ketamine in 10 min before irradiation and were irradiated with 0, 12 , 21 and 27 Gy 12C6+ ion at a dose rate of 1.2 Gy/min at the Heavy Ion Research Facility in Lanzhou（HIRFL）. The total radiation dose was finished by 3 times at Bragg Peak Region of Heavy Ion Beams.The radiation fields of skin were taken photo and performed biopsy. The contaneous tissues of radiation fields were stained by HE and examined histopatholo gical changes every seven days after irradiation. The results indicated that the cutaneous appearance reaction became more faster with radiation dosage rising and presented with swollen, melanin forming and so on after irradiated by the carbon ions at different dosage. The Pathological examination showed noticeable changes in histological and structural of experimental pigs skin, such as atrophy, vacuolation, denaturation and arranged irregularly in epithelial cells. Furthermore, the time for return to normality became longer with the increasing of radiation dosage. All indexes demonstrated correlation between the does and effects. It is concluded that the irradiation of heavy ion beams to normal skin is security when the radiation dose range is about 0—27 Gy.     

硅基GaN微腔制作及其激射特性(特邀)

提出了一种新的Si衬底上GaN微盘谐振腔的制备方式,避免了传统Si基GaN器件中晶体质量较差以及外延层较厚对器件性能的影响.本工作中GaN的外延生长使用蓝宝石衬底,随后将外延层转移至硅衬底上进行微盘谐振腔的制备.外延生长时靠近衬底侧的GaN富缺陷层可使用减薄抛光的方式去除,并且通过简单湿法刻蚀二氧化硅牺牲层即可实现Ga...