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排序方式: 共有9043条查询结果,搜索用时 62 毫秒
991.
YUAN KaiHua & QIU ZhiPing School of Aeronautic Science Engineering Beijing University of Aeronautics Astronautics Beijing China 《中国科学:物理学 力学 天文学(英文版)》2010,(2)
The flutter instability of stiffened composite panels subjected to aerodynamic forces in the supersonic flow is investigated. Based on Hamilton's principle,the aeroelastic model of the composite panel is established by using the von Karman large deflection plate theory,piston theory aerodynamics and the quasi-steady thermal stress theory. Then,using the finite element method along with Bogner-Fox-Schmit elements and three-dimensional beam elements,the nonlinear equations of motion are derived. The effect of... 相似文献
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The aim of this work was to develop a method for determining seven quinolones (ciprofloxacin, danofloxacin, enrofloxacin, sarafloxacin, difloxacin, oxolinic acid and flumequine) in chicken muscle by LC coupled to MS. Two ionisation techniques, ESI and atmospheric pressure chemical ionisation (APCI) were compared using standard solutions. LOD and LOQwere determined under the optimised conditions for the two sources. The ESI was found the best for the purpose. The optimised method (LC-ESI-MS) was validated for the simultaneous analysis of the quinolones regulated by European Community in spiked chicken tissues, using norfloxacin as internal standard. Recoveries obtained varied in the range 60-109%. This method was compared with LC-UV method established previously. 相似文献
995.
Higashi T Takayama N Nishio T Taniguchi E Shimada K 《Analytical and bioanalytical chemistry》2006,386(3):658-665
A practical procedure for determining estrogens in biological fluids has been studied using liquid chromatography–electron
capture atmospheric pressure chemical ionization–mass spectrometry combined with derivatization. Among the commercially available
reagents (4-nitrobenzoyl chloride, 2,4-dinitrofluorobenzene, 4-nitrobenzenesulfonyl chloride and 4-nitrobenzyl bromide), 4-nitrobenzenesulfonyl
chloride was of the most practical use; it rapidly and quantitatively reacted with estrogens and increased the detection responses
by 8–23 times. The derivatization method allowed the reproducible and accurate quantification of serum and urine estrone and
estradiol of a pregnant woman, which is useful for diagnosis of the fetoplacental function, with small amounts (10 μl) of
sample and a simple pretreatment procedure.
Tatsuya
Higashiis Associate Professor of the Laboratory of Clinical Analytical Sciences (Professor Kazutake Shimada’s research group) at
the Graduate School of Natural Science and Technology of Kanazawa University. He received the Japan Society for Analytical
Chemistry Award for Young Scientists in 2003 and the Pharmaceutical Society of Japan Award for Young Scientists in 2006. His
current research interests are the development of methods for increasing sensitivity in LC-MS to detect and characterize trace
amounts of biologically active steroids, such as estrogens, androgens and neuroactive steroids. 相似文献
996.
Leppington F. G.; Broadbent E. G.; Butler G. F. 《IMA Journal of Applied Mathematics》2006,71(6):940-955
** Email: f.leppington{at}ukonline.co.uk
Two thin elastic plates, which may have different physical parameters,occupy the parallel regions 0 < x < a, 0 < y < b,z = d and 0 < x < a, 0 < y < b, z = 0, ina Cartesian coordinate system, where the separation distanced is much less than the dimensions a and b. The plates are simplyconnected to a structure that occupies the rest of the region d < z < 0. The side walls (x = 0 or a, 0 <y < b, d < z < 0 and y = 0 or b, 0 < x <a, d < z < 0) are taken to be acoustically soft;the surfaces z = d and z = 0, outside the rectangularregions occupied by the plates, are taken to be acousticallyhard. Light compressible fluid (air) is in each of the half-spacesoutside the plates and in the rectangular region between them.A sound field is induced by a high-frequency plane wave. Allowanceis made for a small element of damping in the fluid trappedbetween the plates, as well as damping in the plates. Estimatesare derived for the transmitted power, averaged over a frequencyband and with respect to all incidence directions, in the asymptoticlimits of small fluid loading and high frequency. For the casewhere the two plates have identical physical properties, detailedasymptotic estimates are given for the form of the peaks inthe transmitted power, at a discrete set of operating frequencies,both above and below the plates' coincidence frequency. 相似文献
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既有高速铁路进一步提速受限,构建低真空管道运行超高速列车的发展趋势日益明显.运用滑移网格技术,建立动车组列车和低真空管道的三维耦合模型,考虑管道气体的瞬态压缩效应,分析低真空管道横截面积、动车组列车运行速度、管道环境温度和环境压力对车体表面压力的影响.研究表明,低真空管道横截面积、动车组列车运行速度、管道环境温度和环境... 相似文献
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对背面有热流输入的矩形毛细微槽群横截面上的气液分界面形状进行了理论分析,在一定条件下对Wayner蒸发模型进行简化,根据等壁温条件推出蒸发薄液膜区域热流密度近似为定值,通过流体动力学理论推导出了微槽横截面薄液膜区域液膜厚度变化的关系式,并与Wayner蒸发模型的计算结果进行了比较。进一步提出了全新的交界线区域长度的判定方法,根据蒸发薄液膜区域总换热量计算得到蒸发薄液膜区域的长度,交界处接触角,以及固有弯月面区域的曲率半径,从而最终得出了微槽横截面整个气液分界面的形状曲线,理论分析表明:槽宽、热流密度、过热度等因素对蒸发薄液膜区域长度、接触角以及固有弯月面曲率半径等参数有较大的影响。 相似文献