非对称空间外差光谱仪自适应频率跟踪处理方法

非对称空间外差光谱技术是一种新型的超高分辨率遥感探测技术,要求后期的数据处理技术也具有相应的超高准确度.从数字信号处理的角度,提出了一种自适应的频率跟踪处理方法,根据信号的空间频率来插值补偿信号的相位偏移,并且递归迭代出最接近真实值的相位信息.经仿真实验对比验证表明,在噪声干扰强度不大的条件下,相较于传统傅里叶变换方法,本文算法对信号频率和相位提取的准确度提高了约100倍以上,能够有效降低非对称空间外差光谱技术的系统误差.     

相移阴影莫尔条纹正交化解调技术

提出一种基于克莱姆正则化分析法的三帧自标定相移阴影莫尔三维轮廓技术.该技术首先采用移动光栅的方法获得相移条纹图,然后通过不同帧相移条纹图相减去除条纹图背景,进而结合克莱姆正交化法和最小二乘法,发展了一种相位解调方法,提取了测量相位.以五步Harlharan算法为参考,用不同算法对同一物体表面进行测量.结果表明,相对于典型的三步相移法和主量分析方法,提出的方法测量得到的相位误差最小(0.5rad),且简化了测量过程.     

一种新的USED CARS相位匹配实现技术

相位匹配是相干反斯托克斯拉曼散射(CARS)测温的关键技术之一,针对现有非稳腔空间增强探测(USED)相位匹配方式中存在的背景辐射大、光路调试不灵活以及斯托克斯光利用率低的不足,提出了一种新的USED CARS相位匹配实现方案：即设计一个与斯托克斯光斑大小相当、呈45°斜角的斜反镜,用于反射全部斯托克斯光,并以斜反镜代替传统USED CARS中的环反镜,让泵浦光从斜反镜后方射入,从而形成USED相位匹配方式。新的USED CARS相位匹配方案中：由于斜反镜面积相对于环反镜大为减小,使得因反射而进入光路的背景辐射大幅降低;斜反镜本身可作为光路调节元件,因而增加了光路调试灵活度;斯托克斯光被斜反镜全部反射用于产生CARS信号,提高了其利用效率。基于平面火焰炉稳态火焰开展的测温实验结果表明：新的USED CARS相位匹配方案不但克服了传统USED CARS中存在的不足,而且具有更小的标准差,是一种更为有效的相位匹配方法。     

无规共聚物P(MEO2MA-co-OEGMA)的合成及其在水溶液中温度诱导相转变行为

利用原子转移自由基聚合(ATRP)方法,由单体2-(2-甲氧基乙氧基)甲基丙烯酸乙酯(MEO₂MA)和寡聚(乙二醇)甲基醚甲基丙烯酸酯(OEGMA, M_n = 500 g·mol^-1)合成了无规共聚物P(MEO₂MA-co-OEGMA).并采用动态光散射(DLS)、紫外光谱及透射电子显微镜(TEM)等技术考察聚合物在水溶液中的温度响应性聚集行为,获得其在水溶液中的最低临界溶解温度(LCST)及其随组成的变化规律.结果表明,该聚合物具有良好且可逆的温度响应行为,这主要归因于聚合物与水分子之间氢键作用,及其分子本身疏水作用之间为了保持一种微妙的动态平衡而自发对聚集形态进行的“自我调整”,从而达到新的热力学平衡状态的结果.该聚合物的LCST与聚合物中单体OEGMA所占的摩尔比例呈线性关系,可以通过改变单体的摩尔配比实现对聚合物LCST的调控.     

Effect of phase interactions on crystal stress evolution over crystal orientation space under elastoplastic deformation of two-phase polycrystalline solids

It has been known for decades that crystal stress directions move toward the vertices of the single crystal yield surface (SCYS) during plastic flow of polycrystalline solids to satisfy the deformation compatibility among crystals. The alignment of crystal stress with a SCYS vertex is affected not only by plastic anisotropy, but also by other factors such as elastic anisotropy, loading direction, and grain interactions. Among the factors contributing to the degree of alignment, the effect of phase interactions on the crystal stress evolution during plastic flow has not been extensively investigated. In this research, the effect of phase interactions on the crystal stress direction evolution is investigated using simulations of an elastoplastically deforming two-phase (Cu/Fe) polycrystalline solid calibrated to a neutron diffraction experiment. By mapping the simulated crystal stresses over the crystal orientation space, crystal-orientation-dependent nonuniform partitioning of the crystal stress between phases can be observed. An analysis of the distribution of angles between the SCYS vertex and the crystal stress based on the simulation of the two-phase material shows that the crystal stress evolution pattern during plastic flow is strongly affected by phase interactions. These interactions result in low alignment and greater dispersion angles between the crystal stresses and SCYS vertices, particularly in the strong phase.     

Bifurcations of stationary solutions with triple junctions in phase separation problems — A new view of bifurcation analysis

Investigated here are bifurcations of stationary solutions with triple junctions to the curvature-driven motion of curves, which arises in phase separation problems. We demonstrate that, when seen from a new perspective, typical bifurcations under perturbations of domain shape can be analyzed using only elementary geometry.     

On the application of the critical minimum energy subspace method to disordered systems

We discuss the recent application to strongly disordered systems of the Critical Minimum Energy Subspace (CrMES) method, used to limit the energy subspace of the Wang-Landau sampling. We compare with our results on the 3D random field Ising model obtained by a multi-range Wang-Landau simulation over the whole energy range. We point out some problems that may arise when applying the CrMES scheme to models having a complex free energy landscape.     

Automated phase correction via maximization of the real signal

Due to improved quantification capabilities and enhanced signal-to-noise ratio (SNR), phase-corrected real reconstruction in magnetic resonance imaging is superior to the common magnitude reconstruction, especially at low SNR. This requires the development of an automated phase-correction algorithm. Existing methods are not well suited for multiple unconnected regions of very low SNR. For this situation, a method based on the real-signal maximization is implemented, in which the experimental image phase is approximated by a three-dimensional polynomial of up to third order. The presented implementation was successfully applied to data originating from different samples and pulse sequences.     

Detector area expansion at iNSE neutron spin echo spectrometer

Expansion of a detection area is an effective method to increase the measurement efficiency of a neutron spin echo (NSE) spectrometer as well as other spectrometers. For this purpose, we installed a new π/2 spin flipper and Fresnel coil of iNSE spectrometer at JRR-3, Tokai, Japan, for wide-area data acquisition. In this study, we propose a data reduction method to correct the phase inhomogeneity due to the path difference of neutrons on the large detection area. This method can convert many NSE signals at small areas to one NSE signal at a large area with taking the phase offset due to the phase inhomogeneity into account. The measurement efficiency increased by approximately one order of magnitude as a result of the detection area expansion.     

First principles calculation of L21+A2 coherent equilibria in the Fe–Al–Ti system

By combining first-principles density functional total energy calculations and statistical mechanics the ground state and the phase equilibria at finite temperatures of the ternary system Fe–Al–Ti have been investigated. Total energy calculations have been performed by means of the Wien 2k code to establish the ground state energetic. A cluster expansion method was therewith used to describe solid solutions. At several chosen finite temperatures the cluster variation method in the irregular tetrahedron approximation was employed in order to calculate the iron rich ternary bcc equilibria. It is confirmed that there are two kinds of phase separations of the bcc phase, A2+L2₁ and B2+L2₁.