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991.
We report the construction, operation and performance of a transmission spectrometer for the visible to the IR (up to 3.5 μm wavelength) to measure crystals up to a temperature of 1400 °C. The spectral resolution is almost comparable to that of a commercial spectrometer. The performance of the spectrometer and some problems are demonstrated by spectra of YAG : Nd at different temperatures. (© 2003 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim) 相似文献
992.
993.
994.
建立了碱消解-火焰原子吸收光谱法测定土壤中六价铬的方法。讨论了pH值对六价铬测定的影响。干扰实验的结果表明同等含量的三价铬对六价铬测定无干扰。实验对比了无背景校正、氘灯背景校正、塞曼背景校正三种工作方式,分别对低、中、高三个水平土壤六价铬标准物质进行了测定,结果表明,低含量的土壤样品用塞曼背景校正方式测定的结果更准确,最终选择了塞曼背景校正的工作方式。方法的线性范围0.1~2.0mg/L,线性相关系数R为0.999 8,相对标准偏差(RSD)为1.1%;当取样量5g,定容体积100mL时,方法检出限为0.20mg/kg,加标回收率为84.8%~86.9%,能满足日常测定需求。 相似文献
995.
The formation of microelectrostatic fields in biopolymers causes the adsorption of stain molecules in protein. The interactions between the dye alkali blue 6B (AB6B) and four proteins, bovine serum albumin (BSA), human γ-globulin (γ-G), horse myoglobin (Mb) and ovalbumin (OVA), were studied by the microphase adsorption/spectral correction technique. It was observed that the interactions obey the Langmuir isothermal adsorption. The Langmuir equilibrium constants of all the aggregates were determined. Interestingly, the adsorption of AB6B has no relation to the array sequence of amino acid residues, and an electrostatic field consists of constant amino acid residues. The novel method has been applied satisfactorily to the determination of the total protein content in two different samples.
996.
997.
Radiative Heat Transfer in a Resistance Heated Floating Zone Furnace: A Numerical Study with FIDAPTM
This paper presents a numerical study of radiative heat transfer in a floating zone (FZ) furnace which was performed by using the commercial finite element program FIDAPTM. This resistance furnace should provide a temperature higher than the melting temperature of silicon (i.e. Tmax ≈ 1500 °C) and a variable temperature gradient at the liquid/solid interface (≥ 25 K/cm). Due to the high working temperatures, heat radiation plays the dominant role for the heat transfer in the furnace. For this reason, the quality of view factors used in the wall‐to‐wall model was carefully inspected with energy‐balance checks. A numerical model with two control parameters is applied to study the influence of material and geometrical parameters on the temperature field. In addition, this model allows us to estimate the internal thermal conditions which were used as thermal boundary conditions for partial 3D simulations. The influences of an optical lens system on the radial symmetry of the temperature field were examined with these partial 3D simulations. Furthermore, we used the inverse modeling method to achieve maximum possible temperature gradients at the liquid/solid interface according to the limitation of maximum available power and the maximum stable height of a melt zone. 相似文献
998.
The prediction of the flow field in a novel spiral casing has been accomplished. Hydraulic turbine manufacturers are considering the potential of using a special type of spiral casing because of the easier manufacturing process involved in its fabrication. These special spiral casings are known as plate‐spirals. Numerical simulation of complex three‐dimensional flow through such spiral casings has been accomplished using a finite element method (FEM). An explicit Eulerian velocity correction scheme has been deployed to solve the Reynolds‐average Navier–Stokes equations. The simulation has been performed to describe the flow in high Reynolds number (106) regimes. For spatial discretization, a streamline upwind Petrov–Galerkin (SUPG) technique has been used. The velocity field and the pressure distribution inside the spiral casing reveal meaningful results. Copyright © 2000 John Wiley & Sons, Ltd. 相似文献
999.
D.I. Savytskii M. Berkowski L.O. Vasylechko J. Fink‐Finowicki A.O. Matkovskii 《Crystal Research and Technology》2000,35(1):53-63
For La1‐xNdxGaO3 crystals the La‐Nd substitution leads to decrease of spontaneous strains and for composition with x≈0.32 the six possible twin states of orthorhombic phase (m3mFmmm) may be degenerated in three twin states inhered in m3mF4/mmm species when a distorted perovskite pseudocell becomes tetragonal. The {110} and {112} reflection twins and axial twins with compositional planes close to (211) and (21‐1) (S‐walls) were identified in La1‐xNdxGaO3 (x=0.07, 0.12, 0.20) solid solutions crystals. All observed twins are typical for crystals with GdFeO3 type perovskite‐like structure. It has been shown that for x≤0.2 and x≥0.5 orientations of S‐walls weakly depend on La/Nd ratio, whereas in the range of 0.2<x<0.5 they depend strongly on the solid solution composition. The tilt angle between two twin states across twin boundary in La1‐xNdxGaO3 (x<0.6) solid solutions is smaller than that between two twins in pure LaGaO3 or NdGaO3. 相似文献
1000.
That from us as X‐ray Rotation‐Tilt Technique (XRT Method) designated procedure principle represents a world innovation and overcomes essential disadvantages of comparable diffraction techniques known up to now. Starting from the origin and the informational content of the XRT interferences a realization of a special equipment and selected examples of some first applications are presented. 相似文献