A VARIATIONAL EXPECTATION-MAXIMIZATION METHOD FOR THE INVERSE BLACK BODY RADIATION PROBLEM

The inverse black body radiation problem, which is to reconstruct the area temperature distribution from the measurement of power spectrum distribution, is a well-known ill-posed problem. In this paper, a variational expectation-maximization （EM） method is developed and its convergence is studied. Numerical experiments demonstrate that the variational EM method is more efficient and accurate than the traditional methods, including the Tikhonov regularization method, the Landweber method and the conjugate gradient method.     

Catalyst-free and solvent-free method for the synthesis of quinoxalines under microwave irradiation

A facile procedure for the synthesis.of quinoxalines is being reported starting from benzil and 1,2-diaminobenzene. Thereactions were carried out catalyst-free, solvent-free and under microwave irradiation conditions in high yield (84-98%) with short time (3-6 rain) and environmental benign, as well as convenient operation. The structures of all the compounds have been confirmed on the basis of their IR, 1H NMR, and/or 13C NMR, mass spectral data.     

电解分离基体—原子吸收光谱法测定氧化铜光谱标样中Pb,Ni,Zn,Fe

用电解法分离基体铜,电解液经浓缩后直接火焰原子吸收光谱法测定。方法简便、准确。回收率为98—103％。测定0.000x—0.000x％含量的样品。其变异系数为1.8—6.9％。     

高温超导材料YBa2Cu3O7-δ在可见光区的电场调制光反射光谱

本文报道了用调制光谱手段对YBa₂Cu₃O_7-δ化合物所进行的光学测量和研究。从对可见光区调制光谱结构的分析和讨论表明调制光谱可以用于研究超导体化合物的电子态结构。从而提出了又一种研究高温超导材料光学特性的新的测试手段。 关键词：     

Polymeric complex micelle loaded with axially substituted silicon（IV） phthalocyanine

A novel axially substituted silicon(IV) phthalocyanine, namely di-pyridyloxy axially substituted silicon(IV) phthalocyanine 2 was synthesized and characterized by UV/vis, IR, elemental analysis, MS as well as ¹H NMR spectroscopy. Hydrophobic 2 was encapsulated by amphiphilic triblock copolymer poly[N^ε-(benzyloxycarbonyl-lysine]-poly(ethylene glycol)-poly[N^ε-(benzyl oxycarbonyl) (PLL(Z)-b-PEG-b-PLL(Z)) to form hydrophobic 2-loaded polymeric complex micelle (PIC) (2-loaded PIC). Atom force microscopy (AFM) image showed that 2-loaded PIC formed a spherical nanocarrier with approximately 35-50 nm in diameter. The fluorescence intensity and lifetime of 2-loaded PIC was significantly enhanced by the incorporation 2 into PIC nanocarrier.     

基于"CS-IF"矩阵的顾客满意度测评指标体系研究

测评指标体系是顾客满意度测评的核心.本文介绍了一种基于"CS-IF"矩阵的顾客满意度测评指标体系研究方法,更加准确、有效得指导企业改进服务短板,持续提升顾客满意度,并以A省移动公司近期某阶段的满意度测评为例介绍了此方法的应用.     

添加KCl对银胶光吸收的影响

本文研究了添加KCl对两种银胶光吸收谱的影响,并与添加吡啶的情形进行了比较。结果表明KCl的加入,由于造成银颗粒表面的覆盖层而使整个光谱区的光吸收增加,消弱了原银颗粒的等离振子共振吸收,同时因银胶发生链状凝聚,原等离振子共振吸收峰发生劈裂和红移。讨论了这些变化对表面增强喇曼散射强度的影响。 关键词：     

Ce-5%La合金表面氧化过程研究

采用拉曼光谱原位分析、扫描探针显微镜、扫描电镜和X射线能谱研究了Ce-5%（质量分数）La合金在空气中的氧化过程。结果表明,Ce-5%La合金在空气中极易氧化,氧化层由外及里存在氧浓度梯度,Ce^3＋和Ce^4＋所对应的拉曼谱峰强度变化情况反映了Ce-5%La合金在空气中的氧化过程具有两个显著阶段,表面剥离氧化物主要为CeO2。