改性松香键合二氧化硅高效液相色谱固定相的制备及其对三七总皂苷的分离

三七中发挥药效的主要成分为三七皂苷R1、人参皂苷Rg1、人参皂苷Re、人参皂苷Rb1和人参皂苷Rd,用于贫血、冠心病、高血压、脑卒中后遗症等疾病的治疗,但其化学成分多且难分离.将氢化松香丙烯酸羟乙酯(HRHA)通过巯基-烯点击化学反应键合到烷基化硅胶表面,制备出一种新型的改性松香键合二氧化硅高效液相色谱固定相(SiO2...     

广义Carmichael数

设n是一个合数,Z_n表示模n的剩余类环,r(x)∈Z_n[x]是一个首一的k(>0)次不可约多项式。本文引入n是k阶摸r(x)的Carmichael数的定义,全体这样的数记为集C_(k,r)(x),由此给出k阶Carmichael数集:C_k={∪C_(k,r)(x)|r(x)过全体Z_n上的首一k次不可约多项式}。显然C_1表示通常的Carmichael数集。作者得到了n∈C_(k,r(x))的一个充要条件,进而得到n∈C_k的一个充要条件及n∈C_2的一个更易计算的充要条件,还证明了C_1(?)C_2以及|C_2|=∞。     

弱闭T(N)-模的预零化子的等距映射

本文刻划了弱闭T(N)-模的预零化子间的等距映射.设u,W分别为由左连续序同态N→~N和N→~N所确定的弱闭T(N)-模, u(?),W(?)分别为u,W的预零化子,Φ为由u(?)到W(?)上的线性等距映射.若(0)*=(0)#=(0),dim(0)+≠1且min{dim(H(?)~H),dim(He(?)^H)}≥2,则存在酉算子Ui,Vi(i=1,2),使得Φ(A)=U1AV*1或Φ(A)=U2A*V2*.     

Acyclic edge coloring of triangle-free 1-planar graphs

A proper edge coloring of a graph G is acyclic if there is no 2-colored cycle in G. The acyclic chromatic index of G, denoted by χ a(G), is the least number of colors such that G has an acyclic edge coloring. A graph is 1-planar if it can be drawn on the plane so that each edge is crossed by at most one other edge. In this paper, it is proved that χ a(G) ≤Δ(G) + 22, if G is a triangle-free 1-planar graph.     

Synthesis and Esterification of 3‐Ferrocenyl Acrylic Acid in Ionic Liquid

3‐Ferrocenyl acrylic acid, synthesized from ferrocenecarboxaldehyde and propandioic acid in water‐insoluble ionic liquid (1‐butyl‐3‐methylimidazolium hexafluorophosphate, [BMIM]PF₆) at 85 °C in high yield, was transformed to a series of 3‐ferrocenyl acrylate of alcohols and phenols in water‐soluble ionic liquid (1,3‐dimethylimidazolium dimethylphosphate, [DMIM]Me₂PO₄) at room temperature in the presence of dicyclohexylcarbodiimide (DCC) and 4‐dimethylaminopyridine (DMAP).     

Two-dimensional electron transport in AlGaN/GaN heterostructures

We present a theoretical study of electron transport properties of two-dimensional electron gas in AlGaN/GaN heterostructures. By assuming a drifted Fermi–Dirac distribution and taking into account all major scattering mechanisms, including polar optical and acoustic phonons, background impurities, dislocation and interface roughness, the momentum- and energy-balance equations derived from Boltzmann equation are solved self-consistently. The dependence of the electron drift velocity and electron temperature as a function of the applied electric field are obtained and discussed.     

殷钢中零热胀系数的微观机制

18 97年 ,瑞士物理学家Ｃ .Ｅ .Ｇｕｉｌａｕｍｅ发现了一种奇妙的合金———在室温附近的一个很宽的温度范围内 ,合金的热膨胀系数几乎等于零 .这种合金的组成是 6 5%Ｆｅ和 35%Ｎｉ;呈面心立方结构 ,它的中文名字叫殷钢 ,英文名字是ｉｎｖａｒ,意思是体积不变(ｉｎｖａｒｉａｂｌｅ) .与ｉｎｖａｒ类似 ,Ｇｕｉｌａｕｍｅ还发展了所谓ｅｌｉｎｖａｒ合金 ,加热时合金的弹性 (ｅｌａｓｔｉｃｉｔｙ)不变 ,因而被用于制造钟表游丝 .192 0年 ,Ｇｕｉｌａｕｍｅ因上述发现被授予诺贝尔物理奖 .今天 ,殷钢最重要的应用是 :用来制造彩色电视机显…     

Durable antimicrobial cotton fabric fabricated by carboxymethyl chitosan and quaternary ammonium salts

Cellulose - In this article, carboxymethyl chitosan (CMC) and (3-carboxypropyl) trimethylammonium chloride (CPTC) were used as raw materials to prepare an antibacterial cotton fabric with excellent...