2-碘-N-甲基苯磺酰胺的合成新方法和分子结构

选用新方法合成了2-碘—N-甲基苯磺酰胺，通过^1H NMR,^13C NMR,^13C DEPT NMR(Distortionless Enhancement by Polarization Transfer NMR)和MS确证的其结构。     

Numerical Calculation and Analysis of Track Etching Process

Heavy ion irradiated polymers can be chemically etched to form track membrane with pores in the micro and sub-micro ranges. It has been reported that pore growth during etching can be related to track structures. A latent track has a track core inside and a track halo surrounding the track core. By single track etching it is observed that etching in the track core is much faster than in the track halo where the etching rate is even lower tlian that of bulk material. For multi-track etching, no such stages can be seen by the conductance measurements.     

CO、H_2及HO_2在Co/SiO_2催化剂上吸附的原位红外光谱

用原位IR研究了CO在Co/SiO_2催化剂上的吸附,并考察了吸附的CO与H_2、H_2O的相互作用。CO在Co/SiO_2上的吸附显示出四种不同的吸收峰。2002、2027cm~(-1)归属于端基CO吸附;2120cm~(-1)归属于CO在钴离于上的吸附;1870cm~(-1)为CO的桥式吸附;1720cm~(-1)则为多中心吸附。当温度高于370K时,吸附的CO会完全脱附。H_2与吸附的CO相互作用可削弱CO吸收峰的强度,并逐步在低波数(1980cm~(-1))处产生一个小肩。水与吸附的CO相互作用产生一种甲酸基物种(1585、1390cm~(-1))。该物种被认为是Kòlbel-Engelhardt反应的中间体。     

α-FUZZY PAIRWISE RETRACT OF L-VALUED PAIRWISE STRATIFICATION SPACES

The notion of a fuzzy retract was introduced by Rodabaugh (1981). The notion of a fuzzy pairwise retract was introduced in 2001. Some weak forms and some strong forms of α-continuous mappings were introduced in 1988 and 1997. The authors extend some of these forms to the L-fuzzy bitopological setting and construct various α-fuzzy pairwise retracts. The concept of weakly induced spaces in the case L = [0,1] was introduced by Martin (1980). Liu and Luo (1987) generalized this notion to the case that L is an arbitrary F-lattice and introduced the notion of induced L-fts. Several results are obtained, especially, for L-valued pairwise stratification spaces.     

复合多层介质在可变温度和集中荷载作用下的位移和应力

研究了多层介质中的热弹性位移和应力.多层介质具有不同厚度,各层又具有不同的弹性性质,最上层表面上作用热荷载和集中荷载.假设各层分别是均匀、各向同性弹性材料,各层相关的位移分量是轴对称的,对称轴为各层表面的垂线.因此,各层应力函数满足无体力的单一方程.利用积分变换法求解了该方程,对由任意多个层数构造的多层介质,给出了其相应层数基础热弹性位移和应力的解析表达式.并对3层介质和4层介质时的数值结果进行了比较.     

15C的中子晕结构研究

实验测量了83A MeV ^14,15C的核反应总截面(σ_R)及¹⁵C产生^14,15C和¹⁴C产生¹³C的动量分布(P_//). 分析得到了¹⁵C产生¹⁴C和¹³C的动量分布半高宽(FWHM)分别为71±9MeV/c和223±28MeV/c, 而¹⁴C产生¹³C的FWHM为195±21MeV/c. 从¹⁵C和¹⁴C产生¹³C的FWHM与Goldhaber模型的预言基本一致. 而¹⁵C产生¹⁴C的FWHM却要比该模型计算小得多. 同时观测到¹⁵C的σ_R比相邻核有反常增加. 在Glauber模型框架中, 对实验测得的P_//和σ_R进行了探讨. P_//和σ_R的分析结果同时显示¹⁵C的最后一个中主要处于s_1/2态, 具有中子晕结构.     

PROMOTION EFFECT OF PYRIDINE FOR THE DIRECT ELECTROCHEMISTRY OF CYTOCHROME C AT GOLD ELECTRODES

It was found for the first time that the compounds with only one functional group, such as pyridine, can show the promotion effect for the electrochemical reaction of cytochrome C at gold electrodes.     

Residual stress profiling of an aluminum alloy by laser ultrasonics

A residual-stress profile along the thickness of an aluminum alloy sheet is determined by laser-ultrasonic technique. Surface acoustic waves are generated by a Nd:YAG pulse laser and detected by a Heterodyne interferometer on a lateral free surface of the sheet. The distribution of residual stress is determined by measuring the relative variation of the wavevelocities at different location of the sample along its thickness. This technique is validated by three different residual stress profiles obtained experimentally.     

OSCILLATION FOR NONAUTONOMOUS NEUTRAL DYNAMIC DELAY EQUATIONS ON TIME SCALES

The article is concerned with oscillation of nonautonomous neutral dynamic delay equations on time scales. Sufficient conditions are established for the existence of bounded positive solutions and for oscillation of all solutions of this equation. Some results extend known results for difference equations when the time scale is the set Z of positive integers and for differential equations when the time scale is the set R of real numbers.     

STABLE SOLUTION OF TIME DOMAIN INTEGRAL EQUATION METHODS USING QUADRATIC B-SPLINE TEMPORAL BASIS FUNCTIONS

This paper is concerned with stable solutions of time domain integral equation （TDIE） methods for transient scattering problems with 3D conducting objects. We use the quadratic B-spline function as temporal basis functions, which permits both the induced currents and induced charges to be properly approximated in terms of completeness. Because the B-spline function has the least support width among all polynomial basis functions of the same order, the resulting system matrices seem to be the sparsest. The TDIE formula-tions using induced electric polarizations as unknown function are adopted and justified. Numerical results demonstrate that the proposed approach is accurate and efficient, and no late-time instability is observed.