基于粗糙模糊集的聚类决策及应用

对基于粗糙模糊集的聚类问题进行了研究.首先,定义了粗糙模糊值与粗糙模糊集的相似度,给出了粗糙模糊集相似度的一般表达式;然后利用该公式构建了模糊相似矩阵,进而给出了粗糙模糊集的一种聚类方法;最后以实际算例说明了这种思想.     

大规模集成电路抗辐射性能无损筛选方法

空间辐射环境会对电子器件产生辐射损伤。由于商用器件性能普遍优于抗辐射加固器件,所以从商用器件中筛选出抗辐射性能优异的器件将在一定程度上提高空间电子系统的可靠性。结合数学回归分析与物理应力实验的方法,研究了集成电路抗辐射性能无损筛选技术。通过不同的外界能量注入及总剂量辐照实验,探究电路典型参数的应变情况与电路耐辐射性能的关系,并确定其辐射敏感参数;建立预测电路抗辐射性能的多元线性回归方程,并对应力条件下的回归方程进行辐照实验验证。结果显示,物理应力实验与数学回归分析结合的筛选方法减小了实验值与预测值的偏差,提高了预估方程的拟合优度和显著程度,使预估方程处于置信区间。     

Estimation of enhanced low dose rate sensitivity mechanisms using temperature switching irradiation on gate-controlled lateral PNP transistor

The mechanisms occurring when the switched temperature technique is applied, as an accelerated enhanced low dose rate sensitivity(ELDRS) test technique, are investigated in terms of a specially designed gate-controlled lateral PNP transistor(GLPNP) that used to extract the interface traps(Nit) and oxide trapped charges(Not). Electrical characteristics in GLPNP transistors induced by ~(60)Co gamma irradiation are measured in situ as a function of total dose, showing that generation of Nit in the oxide is the primary cause of base current variations for the GLPNP. Based on the analysis of the variations of Nit and Not, with switching the temperature, the properties of accelerated protons release and suppressed protons loss play critical roles in determining the increased Nit formation leading to the base current degradation with dose accumulation. Simultaneously the hydrogen cracking mechanisms responsible for additional protons release are related to the neutralization of Not extending enhanced Nit buildup. In this study the switched temperature irradiation has been employed to conservatively estimate the ELDRS of GLPNP, which provides us with a new insight into the test technique for ELDRS.     

在科研活动中培养学生的实践能力

为了培养学生的创新能力 ,开放了酶工程研究室。目的是与实验教学相结合 ,让各年级学生在科研活动中锻炼自己的实际动手能力 ,培养学生的创新意识、独立解决实际问题和进行科学实验的能力 ,巩固和加深相关的理论知识     

纳米氧化铪的制备与热膨胀性

制备了尺寸为4 nm的HfO2纳米颗粒,并借助X射线原子对分布函数方法,研究了尺寸约4 nm和体相HfO2颗粒的晶格热膨胀。结果表明,在纳米尺度的HfO2中,晶格沿a,c轴的热膨胀性增大,b轴热膨胀性稍微减小,体积热膨胀性增大。同时纳米HfO2晶格热膨胀的各向异性比体相大。该现象是由于尺寸效应导致结构畸变变大,尤其是次近邻Hf-O-Hf键角减小,随后升温过程中该畸变发生热弛豫趋向恢复至平衡位置导致的。     

典型模拟电路低剂量率辐照损伤增强效应的研究与评估

采用变剂量率和变温两种辐照方法,对4款典型模拟电路的低剂量率辐照损伤特性及变化规律进行了研究与评估,分析了两种辐照方法下其辐照敏感参数的变化,比较了不同辐照方式下器件的退化程度,讨论了这两种实验室加速评估低剂量率辐照损伤方法的机理.结果显示,变剂量率辐照可以较快地预测实际低剂量率下的辐照损伤趋势,且在较低的总剂量下能够给出不太保守的估计,但其预测的总剂量受到器件退化速度的影响;变温辐照加速评估方法能够保守地估计其低剂量率下的辐照损伤,其评估范围不仅可达1000 Gy(Si),且可将评估时间缩短为12 h左右.研究结果表明,双极电路的低剂量率辐照损伤增强效应与感生的界面态密度和氢化的氧空位缺陷有关,辐照时剂量率和温度的改变会促进界面态的生长,抑制界面态的钝化作用,从而激发器件的辐照损伤潜能.     

Simulation of Synergism Effect Using Temperature Switching Irradiation on Bipolar Comparator

The synergism effect of total ionizing dose(TID) on a single event transient(SET) in a bipolar comparator is investigated. Experimental results show that the shapes of the SET are considerably influenced by the TID accumulated in low dose rates. The variation tendency of SET shapes can be accurately simulated by temperature switching irradiation. The mechanism of this synergism effect is also analyzed in brief via the operating schematic of a comparator. After the accumulation of 100 krad(Si), the lower tendency of negative SET can be attributed to the degeneration of . The change tendency of a positive SET, either lower or higher, is dependent on the load condition that limits the output range of the comparator.     

快速溶剂萃取-气相色谱-三重四极杆质谱法测定沉积物中的酞酸酯

建立了快速溶剂萃取(ASE)-气相色谱-三重四极杆质谱(GC-MS/MS)测定沉积物中酞酸酯的方法。样品用二氯甲烷-丙酮(体积比为1:1)混合溶剂在100 ℃、103.4 MPa (1500 psi)条件下经快速溶剂萃取、以5 mL/min的速率经凝胶渗透色谱(GPC)净化去除大分子干扰物后,采用GC-MS/MS分析测定。采用内标法定量,17种酞酸酯的检出限为0.05～0.40 μg/kg;回收率为50.5%～107.9%,相对标准偏差为3.5%～13.9%。采用替代物基体加入法对方法的性能进行了验证,3种替代物的回收率为65.3%～95.8%。该方法快速、灵敏度高,能同时准确定性定量测定17种酞酸酯。     

NbN/AlN/NbN超导隧道结的制备工艺

研究了在MgO基片上制备NbN/AlN/NbN结的工艺,NbN和AlN的制备分别采用直流磁控溅射和交流磁控溅射。为了得到良好特性的隧道结,首先要在高真空反应室里沉积三层膜结构,经过光刻和反应离子刻蚀,得到底电极和桥区的三层结构图形。再经过第二步光刻和刻蚀,仅保留底电极最下层的NbN,得到结区的三层结构图形,并覆盖AlN绝缘层。经过Lift-off工艺,洗去结区上的光刻胶,最后沉积上电极。使用四端子方法对制备的隧道结进行了一系列测量,特别是在高频(THz)下的响应。     

Thermal and redox dual responsive poly(<Emphasis Type="SmallCaps">L</Emphasis>-glutamate) with oligo(ethylene glycol) side-chains

A series of poly(L-glutamate)s grafted with oligo(ethylene glycol) (OEG) side-chains through the thioether linkages (PALG _n -g-EG _x , x = 2, 3 and 4) were prepared by ring-opening polymerization (ROP) of γ-allyl-L-glutamate N-carboxyanhydride (ALG-NCA) and thiol-ene photoaddition. The chemical structures and physical properties were characterized by ¹H-NMR, Fourier transform infrared (FTIR), circular dichroism (CD), etc. The PALG _n -g-EG _x samples with x = 3 and 4 displayed lower critical solution temperature (LCST) in water due to the presence of OEG units. The clouding point (CP) of polypeptides can be finely tuned by changing the side chain structures, molecular weights and sample concentrations. In addition, the thioether linkages in the side chains offer additional redox-responsive properties. The influence of both OEG units and thioether linkages on the LCST behavior was systematically investigated. This work provides an efficient way to prepare multi-stimuli responsive materials with highly tunable properties.