表面粗糙度的变波矢光散射测量方法的研究

提出了表面粗糙度变波矢光散射测量方法，通过散射光强中心亮点光能量的参数ｌｎ，Ｅ随变化的线性关系来确定粗糙度ｗ，对６块粗糙度不同的硅片背面样品进行了实验测量。     

Ordered supramolecular assembly of bis[3,4,12,13,21,22,30,31-octa(dodecylthio)-2,3-naphthalocyaninato]erbium at the air/water interface

The supramolecular assembly of bis[3, 4, 12, 13, 21, 22, 30, 31-octa(dodecylthio)-2, 3-naphthalocyaninato] erbium complex (Er[Nc(SC12H25)8]2) was fabricated at the air/water interface by Langmuir monolayer technique. Surface pressure-area isotherm indicates that stable monolayer is formed. The monolayer morphology on mica was investigated by atomic force microscopy (AFM). Columnar domains of ca. 100 nm ×(20-30) nm appearing in the micrograph have ordered orientation. Polarized UV-vis spectra and small-angle X-ray diffraction pattern show that the macrocycles tilt in the monolayer. The orientation angle of the naphthalocyanine ring with respect to the substrate was found to be ca. 54°. Each monolayer is ca. 3.53 nm thick. The columnar domain comprises 4-6 rows of columnar supramolecular assemblies where the molecules stack face-to-face.     

角分辩的光散射轮廓及自仿射分形表面的粗糙指数的实验研究

建立了反射式随机表面的光散射特件实验测量系统,利用多幅平均及叠加连接的方法,得出入射角在45°～85°之间不同值时的光散射轮廓.结果表明,随着表面入射角的增加,光散射轮廓的半峰全宽逐渐减小.并且当入射角的增加到一定值时,光散射轮廓出现中央亮斑.由数学上的对称F降函数,推导出光散射轮廓的半峰全宽随散射光波矢的变化关系,从实验测得角分辩的的光散射轮廓中提取了自仿射分形随机表面的粗糙指数.与原子力显微镜测量得到的粗糙指数进行比较,两者符合得很好.     

低温磁控溅射有机衬底和玻璃衬底ZnO:Al透明导电膜的结构及特性

利用射频磁控溅射法在有机薄膜衬底和7059玻璃衬底上制备出了具有良好附着性的低电阻率的ZnO:Al透明导电膜,对在低温（25～210℃）下制备薄膜的结构和光电特性进行了比较研究. 铝掺杂的氧化锌薄膜是多晶膜,具有六角纤锌矿结构,最佳取向为（002）方向.薄膜的最低电阻率分别为1.0×10^-3和8.4×10^-4Ω·cm,在可见光区的平均透过率分别达到了72%和85%.     

变孔径像面散斑平均光强标定随机表面的理论与实验

采用随机表面的高斯相关模型和统计光学原理,推导出弱散射体在4f系统中的像面上光强的表达式.在此基础上提出了均方偏差粗糙度和横向相关长度的标定方法,该方法用理论结果对实验测量的像面散斑平均光强随滤波孔半径的关系曲线进行拟合,同时测量出被测样品表面的两个统计量.实验上制作了高斯相关随机表面样品,对其表面参数进行了测量,与AFM所测结果符合得较好,这表明该方法具有较高的精度. 关键词： 弱散射体 像面散斑 平均光强     

弱散射屏的像面散斑自相关函数特性的实验研究

在对随机弱散射屏进行表面参数的原子力显微镜测量和建立了门积分取样平均的随机光强自相关函数测量系统的基础上,对弱散射屏在严格像面和离焦像面上产生的散斑自相关函数进行了测量。发现在严格像面上,散斑平均颗粒的大小随表面粗糙度增加而减小,且光强自相关函数次极大的相关间隔宽度随粗糙度增加而减小;而次极大的超伏随粗糙度的增大而增大;在离焦像面上,离焦量的增加使光强的自相关函数下降变得平滑,并使极小值点和次极大点变得不明显或者消失。     

气/液界面上双萘菁夹心化合物有序超分子结构的组装

研究了气/液界面上双(八-十二烷硫基)萘菁铒{Er[Nc(SC₁₂H₂₅)₈]₂}形成的Langmuir单层膜中的超分子结构. 表面压-面积(π -A)等温线表明该化合物形成了稳定的单层膜. 将其沉积在云母片上, 用原子力显微镜(AFM)进行观察, 表明分子形成了取向高度有序的结构, 聚集体特征长度在100 nm左右(有的长达300 nm), 宽为20~30 nm.用紫外-可见光谱、偏振紫外-可见光谱、小角X射线衍射等对 LB膜进行了研究, 发现分子大环平面与基片平面夹角为54°, 每层厚度为3.53 nm. 研究表明形成的超分子结构由4~6列以面对面堆积形成的柱状体构成.     

Correlation and fractal properties of speckles in the extremely deep Fresnel diffraction region

Based on the Kirchhoff approximation and the theoretical analysis of the random light fields,the speckle intensity distributions in the extremely deep Fresnel diffraction region are simulated.The fractal property of the speckles as well as the relation between the speckle intensity distribution and the corresponding random surface is investigated.We design a microscope system to detect experimentally the speckles in the extremely deep Fresnel diffraction region,and the experimental results prove the conclusions drawn from our simulations.     

Experimental study of regional fractal speckle produced in large angle scattering

Using the interference of speckle and the spherical reference wave,we extract the real and the imaginary parts of the complex amplitudes of the speckle in large angle scattering.By calculating the spatial correlation functions of intensity,we find that the speckle has a property of regional fractality,i.e.the fractal exponent equals 1 in a small spatial region and it becomes less than 1 in a bigger region.The empirical analytic expression of the intensity correlation function is gained.The probability density distributions of the intensities and the complex amplitudes show that the regional fractal speckle still obeys zero-mean circular complex Gaussian statistics.     

旋转孔径白光散斑照相法的研究

本文报道利用旋转孔径法进行白光散斑照相,研测动态问题.其不仅具有旋转孔径激光散斑照相的优点,而且最突出的优点是能走出实验室,到现场进行动态测量研究.