钛光度分析的某些进展

综述了光度法测定钛近 5年来研究的某些进展 ,涉及经典光度法、动力学光度法、计算光度法及流动注射光度法测钛 ,引文 6 0篇。     

国内动力学光度法测定碘研究的某些进展

本文综述了国内光度法测定碘研究的某些进展,分别从催化氧化动力学,阻抑动力学、非动力学光度法和催化荧光光度法等几个类别进行归纳,并从反应介质、检出限、线性范围和应用等方面进行叙述.     

国内光度法测定亚硝酸根进展

对国内近年来(2000—2009年)亚硝酸根的光度法测定进展作了回顾,主要涉及亚硝酸根的光度测定中应用普通分光光度法、流动注射光度法、催化光度法和荧光光度法等内容,引用文献88篇。     

环境样品中痕量铝的现代光度分析研究新进展

论文综述和评论了近年来环境样品中痕量铝的光度分析研究新进展。重点论述了现代光度分析法测定环境样品中铝的研究新进展 ,内容包括 :胶束增溶分光光度法、双波长分光光度法、导数分光光度法、催化光度法、固相光度法、流动注射光度法。对普通光度法和胶束增溶光度法的反应体系、测定条件、摩尔吸收系数 (ε)或检出限、线性范围及其应用进行了归纳总结 ,评述了各种光度法测定的优劣 ,展望了光度法测定痕量铝的发展前景     

罗丹明B在无机分析中的应用

本文从分光光度法、荧光光度法、散射三个方面系统的综述了近年来罗丹明B在无机分析中的应用情况及研究进展,引用文献49篇。     

催化动力学光度法测定痕量铜的研究进展

本文探讨和论述了近年来催化动力学光度法测定痕量铜的研究进展，比较了催化光度法与原子吸收法、萃取光度法的优缺点；介绍了催化动力学光度法的原理；评述了催化褪色光度法、催化显色光度法、催化荧光光度法等的研究进展，探讨和展望了催化动力学光度法未来的研究方向和发展前景，包括：1．对传统显色剂改性或合成新的高灵敏度、高选择性显色剂；2．活性剂增敏研究；3．加强相关催化机理的研究和探讨。全文参考文献29篇。     

DAN荧光法等3种测定蛹虫草菌丝体中硒含量的方法比较

通过DAN荧光法,3,3-二氨基联苯胺分光光度法和邻苯二胺紫外分光光度法测定蛹虫草菌丝体中硒的含量,对测得结果进行统计分析,并对其检出限、回收率进行比较研究.研究结果表明,DAN荧光法、3,3-二氨基联苯胺分光光度法和邻苯二胺紫外分光光度法中,硒含量相对标准偏差分别是2.5%,9.2%和6.1%;线性回归系数都大于0....     

杂多酸(蓝)分光光度法在测定痕量元素中的研究进展

杂多酸能被还原为有颜色的杂多蓝,结合分光光度法,可对痕量元素进行准确的分析。目前,杂多酸分光光度法作为一种分析技术,具有精度高、操作简便、分析速度快等优点,在痕量分析领域得到了迅速发展。文章综述了杂多酸在测定痕量元素P, As, Si和V中的应用及研究进展。方法主要包括钼蓝法、杂多酸-碱性染料法、荧光分光光度法、流动注射分光光度法、原子吸收分光光度法、激光热透镜分光光度法等,并对这些方法进行了比较分析。     

催化动力学光度法测定痕量Fe(Ⅲ)的研究进展

论文探讨和论述了近年来催化动力学光度法测定痕量铁的研究进展。具体探讨和评述内容包括:比较催化光度法与原子吸收法、萃取光度法的优缺点;介绍催化动力学光度法的原理;评述催化褪色动力学光度法研究进展、催化显色动力学光度法研究进展、阻抑显色催化动力学光度法研究进展、阻抑褪色催化动力学光度法研究进展;包括指示反应及其条件、方法的检出限、干扰情况、测定范围、应用等。论文还探讨和展望了催化动力学光度法未来的研究方向和发展前景。内容包括:①对传统显色剂改性或合成新的高灵敏度、高选择性显色剂;②活性剂增敏研究;③加强相关催化机理的研究和探讨;④开展酶催化动力学光度法研究。     

国内银的分析测定研究进展（一）——国内光度法测定银的研究进展

归纳总结了国内主要刊物上所发表的光度法测定银的研究和应用情况。主要包括普通吸光光度法,催化光度法,共振散射法,和化学发光法,并进一步提出了建议和设想。     

Propagation of Helmholtz-Gauss beams in weak turbulent atmosphere

Based on the Rytov approximation of light propagation in weak turbulent atmosphere,the closed-form expressions of field and average irradiance of each one of the four fundamental families of Helmholtz-Gauss (HzG)beams:cosine-Gauss beams,stationary Mathieu-Gauss beams,stationary parabolic-Gauss beams,and Bessel-Gauss beams,which are propagating in weak turbulent atmosphere,are obtained.The results show that the field and average irradiance can be written as the product of four factors:complex amplitude depending on the z-coordinate only,a Ganssian beam.a factor of complex phase perturbation induced by atmospheric turbulence,and a complex scaled version of the transverse shape of the non-diffracting beam.The effect of weak atmospheric turbulence on irradiance distribution of the HzG beam can be ignored.     

Investigation on characteristics of self-organization in Mach-Zehnder erbium-doped fiber laser cavity

The characteristics of coherent coupling in Mach-Zehnder erbium-doped fiber laser cavity are experimentally studied. By virtue of a seemly controlling of length difference between two interferometric arms, the obtained comb-like spectrum of interferometer resonator with a period of 0.06 nm commendably agrees with the theory of self-organization coherence. The coherent output exits from the output mirror of a fiber Bragg grating with 4.5% reflectivity. A high coherent combining efficiency of 94% is obtained. Investigation on characteristics of the leak power opens out self-organization mechanism in Mach-Zehnder composite cavity.     

Synergistic effects on iodine release in potassium iodide solution by combination of ultrasound and visible light irradiations

Iodine release in potassium iodide solution has been investigated under the irradiations of ultrasound and visible light respectively and simultaneously. We have observed that the amount of iodine liberated under the combined irradiation of ultrasound and visible light is larger than the sum of that under the respective irradiations of ultrasound and visible light, indicating a synergistic effect of ultrasound and visible light irradiations. Based on the investigation of the reaction kinetics of iodine liberated, we have ascribed the synergistic effect to the perfect stirring of the photochemical reactor induced by the applying simultaneous ultrasound. The ideal stirring can result in the homogenization of the primary light effect in the whole reaction medium, which induces the acceleration of the photochemical reaction. On behavior of our knowledge, there are few reports on the investigations of utilizing the combination of ultrasonic energy and light energy to accelerate the reaction yield and rate as well as the kinetics of the reaction.     

Effect ofγ-radiation on the spectral luminescence characteristics of impure cadmium tungstate crystals

Results of a study of the effect of γ-radiation on the spectral luminescence properties of cadmium tungstate crystals doped with silver, bismuth, and molybdenum cations are presented. Spectral characteristics of the nondnnnoped crystals are briefly described. Absorption and photo and X-ray luminescence spectra of the crystals taken before and after exposure to γ-radiation (5.5·10⁴ Gy) are compared. It is found that the spectral characteristics of the crystals doped with silver, bismuth, and molybdenum cations do not change markedly after the exposure. The relation between the type of impurity-induced defects, individual characteristics of the impurity cations, and the character of the effect of γ-radiation on the spectral luminescence properties of impure crystals is analyzed (preliminarily). Translated from Zhurnal Prikladnoi Spektroskopii, Vol. 64, No. 1, pp. 55–60, January–February, 1997.     

A study on the best irradiation dose of X-ray for Hep-2 cells by Fourier transform infrared spectroscopy

Fourier transform infrared spectroscopy (FTIR) was employed to study the human epidermis larynx carcinoma cell lines (Hep-2) which were irradiated by different doses of X-ray.The results show that (1) the irradiation of X-ray damages the structure of the CH3 groups of the thymine in DNA,which restrains the reproduction of Hep-2 cells effectively,(2) the 8 Gy dose of X-ray irradiation changes the framework and the relative contents of some proteins,lipids and the nucleic acid molecules intercellular in the greatest degree,and (3) the 8 Gy dose of X-ray irradiation is the best irradiation dose for lowering the degree of the cancerization of Hep-2 cells according to the criteria for the degree of the cancerization reported recently.Meanwhile,the apoptosis of these cells were detected by using flow cytometry (FCM) primarily.It shows that the apoptotic ratio of the Hep-2 cells depends on the irradiation dose to some extent,but is not linearly.And the apoptotic ratio of the 12 Gy dose group is the maximum (20.36%),but the apoptotic ratios of the 2 to 8 Gy dose groups change little.     

Experimental study on SC RF cavities by using China large grain niobium for ILC

Large grain niobium has the potential of simplifying the production sequence and consequently reducing the cost of the superconducting RF cavities for ILC.To investigate the feasibility of fabrication and the possibility to achieve high gradient by large grain cavities,two 1.3 GHz cavities were made of China large grain niobium and a series of vertical tests were carried out following several different surfaces treatment procedures.Two cavities have both reached the high gradient of more than 43 MV/m repeatedly and the maximum accelerating field of 47.9 MV/m has been achieved by China large grain niobium.This paper introduces the features of the fabrication and surface treatments on the large grain cavities and presents the preliminary results of the research.     

Analysis of Laser-generated Rayleigh wave on viscoelastic materials

In order to understand the viscoelasticity of material, this research has been conducted to study the propagation characteristics of viscoelastic Rayleigh wave theoretically. A model is presented for the pulsed laser generation of ultrasound on viscoelastic medium surface. Referred to the Kelvin model, the frequency equation and the normal displacement of viscoelastic Rayleigh wave were derived, the influence of the viscoelastic modulus on dispersion and attenuation was discussed. From the theoretical calculation, it is shown that the effect of viscoelasticity on the attenuation of Rayleigh wave is more than that on its dispersion. In the case of a weak viscosity, the attenuation of viscoelastic Rayleigh wave is directly proportional to viscosity modulus; the effect of shear viscosity on the attenuation is much more than that of bulk viscosity. The transient response of viscoelastic Rayleigh wave was also simulated using Laplace and Hankel inversion transform, which are showed in good agreement with the theoretic predictions. The model provides a useful tool for the determination of viscoelastic parameters of medium.     

Testifying experiment of the multi-pulse phenomena of capillary discharge soft-X-ray laser

In a capillary discharge experiment for the neon-like argon lasing, we have proposed an experimental scheme to verify that the multi-spike of X-ray diode (XRD) signal is a multi-pulse laser or is a reflection of the laser pulse in the XRD.The ceramic capillary has an inner diameter of 3mm and a length of 200mm.At the gas pressure of 28Pa and discharge current of 27kA, stable lasing has been realized.The experimental results prove that the multi-spike of XRD signal is a reflection of the electromagnetic signal produced by the laser pulse in the XRD.The improved electrocircuit scheme of the XRD to minimize the reflection phenomena is also found.     

Harmonic operation of high gain harmonic generation free electron laser

In high gain harmonic generation (HGHG) free electron laser (FEL), with the right choice of parameters of the modulator undulator, the dispersive section and the seed laser, one may make the spatial bunching of the electron beam density distribution correspond to one of the harmonic frequencies of the radiator radiation, instead of the fundamental frequency of the radiator radiation in conventional HGHG, thus the radiator undulator is in harmonic operation (HO) mode. In this paper, we investigate HO of HGHG FEL.Theoretical analyses with universal method are derived and numerical simulations in ultraviolet and deep ultraviolet spectral regions are given. It shows that the power of the 3rd harmonic radiation in the HO of HGHG may be as high as 18.5% of the fundamental power level. Thus HO of HGHG FEL may obtain short wavelength by using lower beam energy.     

Radiative spectra of thermal electromagnetic noise induced by planar realistic dielectrics

Spectral characteristics of stochastic fields and their spatial derivatives in various planar structures composed by lossy materials described by realistic dielectric functions are numerically calculated based on solutions to the problems of multipolar electromagnetic fields in a plane layered geometry. A displacement of the maximum of the spectral power densities for spatial derivatives of fluctuating fields to the high-frequency domain, a resonant increase in the density of states of the fluctuating fields at the frequencies of interface excitations and interference modes for the radiative part of the spectra, the influence of geometry on the density of states, and other peculiarities are found by numerical calculations and graphically demonstrated. Interpretations of the above effects are provided.