| ICP-AES测定铝锭中八种杂质元素 |
| |
| 引用本文： | 钟志光,卞群洲,刘崇华,卢焯冬,贺柏龄.ICP-AES测定铝锭中八种杂质元素[J].光谱实验室,1999,16(6):684-687. |
| |
| 作者姓名： | 钟志光 卞群洲 刘崇华 卢焯冬 贺柏龄 |
| |
| 作者单位： | 广东出入境检验检疫局,510623 |
| |
| 摘 要： | 本文研究了名对铁、锰、铜、锌、镁、钛、硅、镓等分析元素的干扰情况，采用了基体匹配法进行基体干扰校正，采用干扰系数法扣除杂质元素间光谱干扰引起的分析偏差，从而确定了铝锭中八种杂质元素同时测定的最佳工作条件，并用实际样品把本方法与化学法的测定进行对比，结果令人满意。方法回收率在９２．９％－１０５％之间，精密度在０．８２％－２．３２％之间，该方法快速、简便、可靠，适用于进出口铝锭的日常检验。
|
| 关 键 词： | 电感耦合等离子体原子发射光谱 铝锭 基体匹配法 干扰系数法 |
| 修稿时间： | 1999-07-30 |
Simultaneous Determination of 8 Impurity Elements in Aluminium Ingot by ICP-AES |
| |
| ZHONG Zhi-Guang,BIAN Qun-Zhou,LIU Chong-Hua,LU Zhuo-Dong,HE Bai-Ling.Simultaneous Determination of 8 Impurity Elements in Aluminium Ingot by ICP-AES[J].Chinese Journal of Spectroscopy Laboratory,1999,16(6):684-687. |
| |
| Authors: | ZHONG Zhi-Guang BIAN Qun-Zhou LIU Chong-Hua LU Zhuo-Dong HE Bai-Ling |
| |
| Abstract: | With matrix match technique and interference factor method, a new method has been developed for simultaneous determination of 8 impurities (Fe,Mg,Cu,Zn,Ti,Si,Mn,Ga) in aluminium ingot by ICP AES . The satisfactory results of comparative test of real sample with chemistry method were obtained. The recovery rates are between 92.9% and 105%.The precision is in the range of 0.82%-2.32%. This method is rapid ,accurate and convenient for operation. This will be of great practical significance in spectral analysis of impurities in import and export aluminium ingot in daily inspection. |
| |
| Keywords: | ICP AES Aluminium Ingot Matrix Match Method Interference Factor Method |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
