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原子吸收光谱法测定水泥中的钠、钾、镁和铁
引用本文:张晓,李蓉仑,张安琪.原子吸收光谱法测定水泥中的钠、钾、镁和铁[J].光谱实验室,2012,29(2):741-744.
作者姓名:张晓  李蓉仑  张安琪
作者单位:中铁二院工程集团有限责任公司工程测试中心,成都市金牛区通锦路3号,610000
摘    要:对火焰原子吸收光谱法测定水泥中的钠、钾、镁和铁的方法进行研究。在选定的最佳仪器条件下,测定钠、钾、镁和铁的RSD分别为1.81%、1.05%、2.68%、1.12%。水泥样品中钠、钾、镁和铁的回收率分别为102.0%—104.0%、98.4%—100.4、98.0%—102.0%、98.0%—100.3%。方法操作简单,测试快速,结果准确稳定。

关 键 词:火焰原子吸收光谱法  水泥        

Determination of Sodium, Potassium, Magnesium and Iron in Cement by AAS
ZHANG Xiao , LI Rong-Lun , ZHANG An-Qi.Determination of Sodium, Potassium, Magnesium and Iron in Cement by AAS[J].Chinese Journal of Spectroscopy Laboratory,2012,29(2):741-744.
Authors:ZHANG Xiao  LI Rong-Lun  ZHANG An-Qi
Institution:ZHANG Xiao LI Rong-Lun ZHANG An-Qi(Engineering Test Center of China Railway Eryuan Engineering Group Co.,Ltd,Chengdu 610000,P.R.China)
Abstract:The method for the determination of sodium,potassium,magnesium and iron in cement by atomic absorption spectrometry(AAS) was studied.Under the optimum experimental conditions,the RSDs of sodium,potassium,magnesium and iron were respectively 1.81%,1.05%,2.68% and 1.12%.The recoveries of sodium,potassium,magnesium and iron were respectively 102.0%—104.0% and 98.4%—100.4%,98.0%—102.0% and 98.0%—100.3%.The method has simple operation and rapid determination with accurate and stable results.
Keywords:AAS  Cement  Sodium  Potassium  Magnesium  Iron
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